Food ScienceNutrition and DieteticsBiotechnologyAgronomy and Crop Science
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Journal of the Science of Food and Agriculture publishes peer-reviewed original research, reviews, and perspectives in these areas, with particular emphasis on interdisciplinary studies at the agriculture/ food interface. The journal focuses on hypothesis-driven research studies suitable for an international audience. Studies of local products or descriptive studies are discouraged.
AbstractSpray‐dried coconut milk powder prepared with additions of skim milk and dextrin was stored in packages for 6 months at room temperature (30°C and 80% RH). The packaging materials used were aluminum laminate (vacuum and air packed) and polypropylene. The sorption isotherm of the powder showed that the monolayer of water molecules was complete when the relative humidity was 27% which corresponded to a moisture content of 5%. Measurements of water activity, moisture content, peroxide value and solubility index indicated that lipid oxidation is the limiting factor in the stability of the powder. Its maximum shelf‐life was 4 months when air or vacuum packaged in aluminum laminates and 1 1/2 months in polypropylene.
AbstractThe dissolution of two finely ground potassium feldspar rocks (KFR). from Malawi and Sri Lanka, was examined in four indigenous acid soils using open‐leaching and closed‐incubation systems. Increases in fractions of soil potassium (K), compared to the control, indicated that the extent of dissolution of KFR was usually substantially enhanced in the leaching system. Because the leaching system represents the field situation more closely, it is the most appropriate for assessing the dissolution of potassium feldspar rocks (KFR) in soils and their potential as direct‐application K fertilisers.
AbstractThe brown acidic pigments and the yellow neutral pigments of black tea are provisionally named thearubigins and theaflavins respectively. These and other substances characteristic of black tea are formed during the fermentation process, mainly as the result of the enzymic oxidation of (—)‐epigallocatechin and (—)‐epigallocatechin gallate. It is probable that the theaflavins are intermediates in thearubigin formation.
C J Powell, Michael N. Clifford, Shaun C Opie, Michael A. Ford, Alastair H. F. Robertson, Cohn L. Gibson
AbstractReverse‐phase HPLC of liquors prepared from a Lattakari Assam black tea was used to assess the contribution of black tea phenolic pigments to ‘tea cream’, a precipitate which forms routinely following caffeine complexation of the phenols when a strong infusion of black tea cools. In this study caffeine was added back to tea liquor fractions and reconstituted decaffeinated whole tea liquor, and the extent to which the theaflavins, thearubigins and flavonol glycosides were removed from solution in the form of insoluble complexes was monitored by HPLC. The poorly characterised thearubigins are shown to be the principal (≈ 86%) pigmented phenolic components of ‘tea cream’. Theaflavins (≈ 12%) and flavonol glycosides (≈ 2%) were also present. Evidence is presented for a synergistic interaction between theaflavins and thearubigins during cream formation. The use of caffeine precipitation is proposed as an aid to the fractionation and quantification of phenols including thearubigins in black tea liquors.
E. A. H. Roberts, Reed A. Cartwright, M. Oldschool
AbstractMethods are described for the fractionation of the complex mixture of phenolic substances and their oxidation products occurring in manufactured tea. Products of oxidation detected include two fractions, S I and S II, responsible for the greater part of the colour intensity of a tea infusion, and nine unidentified substances, A, B, C, D, P, Q, X, Y and Z. S I and S II have been obtained almost free from other contaminants. They have acidic properties, and mean molecular weights of the order 600. They are probably mixtures of dimers, each dimer consisting of two oxidized flavanol units. X and Y have no acidic properties and are also distinguished from S I and S II by several characteristic colour reactions. P may be an anthocyanidin.
Shaun C Opie, Alastair H. F. Robertson, Michael N. Clifford
AbstractA reverse phase, gradient elution HPLC method has been developed to separate black tea thearubigin compounds. Using diode array spectroscopy, spectral data are provided for the major pigment peaks. The analytical method has been used to monitor the formation of the thearubigin compounds during black tea fermentation. In‐vitro model fermentation systems using partially purified tea polyphenol oxidase and mixtures of six pure catechins have also been analysed. Data are presented to relate many of the thearubigins in black tea liquors to their catechin precursors. Manipulation of the in‐vitro model system conditions will be used to prepare various thearubigins for further structural studies.
AbstractThe sorption of iodide by several soil component materials was examined over a range of pH values and compared with sorption by a surface soil. A compost, prepared from grass roots which had been allowed to decompose for 24 weeks, sorbed substantial amounts of iodide from solution and showed changes in sorption, due to pH and drying, similar to those shown by the soil. Freshly precipitated hydrated ferric oxide also sorbed substantial amounts of iodide from solutions of pH < 5.5 but the amount decreased to zero as the pH approached 7. Sorption by freshly precipitated hydrated aluminium oxide was impossible to assess at pH < 5 owing to its solubility but at pH 5.5 to 7.5 its sorption was similar to that of ferric oxide. No sorption of iodide was detected by kaolinite, montmorillonite, chalk or limestone.Drying markedly reduced the capacity for iodide sorption of the compost and soil and had a smaller effect on the ferric and aluminium oxides.