Stepwise Synthesis and Spectral Characteristics of meso-trans-Diphenyldi(1-naphthyl)tetrabenzoporphin and Its Zinc Complex

Pleiades Publishing Ltd - Tập 39 - Trang 1183-1187 - 2003
N. E. Galanin1, E. V. Kudrik1, G. P. Shaposhnikov1
1Ivanovo State Chemico-technological University, Ivanovo, Russia

Tóm tắt

A reaction of phthalimide with phenylacetic acid in the presence of zinc oxide furnished 3-oxoisoindolenyl-3'-oxoisoindolinylidene-1,1'-benzylidine which at heating with 1-naphthylacetic acid in the presence of zinc oxide provided zinc meso-trans-diphenyldi(1-naphthyl)tetrabenzoporphin complex. Proceeding from this compound a meso-trans-diphenyldi(1-naphthyl)tetrabenzoporphin was prepared. The spectral characteristics of compounds obtained were studied.

Tài liệu tham khảo

Kopranenkov V.N., Dashkevich S.N., and Luk'yanets E.A., USSR Inventor's Certificate no. 889675, 1981; SSSR Byull. Izobr., no. 46, 10. Maslyukov, A.P., Kopranenkov, V.N., Kopylova, E.M., and Goncharova, L.S., USSR Inventor' 765281; SSSR Byull. Izobr., 1980, no. 35, 147. Yasuike, M., Yamaoka, T., Ohno, O., Sakuragi, M., and Ichimura, K., Inorg. Chim. Acta, 1991, vol. 184, p. 191. Luk'yanets, E.A., Dashkevich, S.N., and Kobayashi, Nagao, Zh. Obshch. Khim., 1993, vol. 63, p. 1411. Cheng, R., Chen, Y., Wang, S., and Cheng, C., Polyhedron, 1993, vol. 12, p. 1353. Maw-Rong, Lee, Sue-Tsung, Liou, Ru-Jen, Cheng, J. Am. Soc. Mass. Spectrom., 1997, no. 8, p. 62. Ichimura, K., Sakuragi, M., Morii, H., Yasuike, M., Toba, Y., and Fukui, M. Inorg. Chim. Acta, 1991, vol. 186, p. 95. Kudrik, E.V., Islyaikin, M.K., and Frantseva, S.V. Zh. Obshch. Khim., 1997, vol. 67, p. 1202. Galanin, N.E., Kudrik, E.V., and Shaposhnikov, G.P., Zh. Obshch. Khim., 2000, vol. 70, p. 1379.