Quality control of the traditional herbs and herbal products: a review

Nazim MD, Aslam M, Khatoon R, Asif M, Chaudhary SS (2018) Physico-chemical standardization of Hansraj (Adiantum capillus-Veneris). J Drug Delivery Therapeut 8(6-s):195–203

Marchese A, Barbieri R, Coppo E, Orhan IE, Daglia M, Nabavi SF, Izadi M, Abdollahi M, Nabavi SM, Ajami M (2017) Antimicrobial activity of eugenol and essential oils containing eugenol: a mechanistic viewpoint. Crit Rev Microbiol 43(6):668–689. https://doi.org/10.1080/1040841X.2017.1295225

Deogade MS, Prasad KS (2019) Standardization of wild Krushnatulasi (Ocimum tenuiflorum Linn) Leaf. Int J Ayurvedic Med 10(1):52–61

Liu C, Guo DA, Liu L (2018) Quality transitivity and traceability system of herbal medicine products based on quality markers. Phytomedicine 44:247–257

Steinhoff B (2019) Quality of herbal medicinal products: State of the art of purity assessment. Phytomedicine 60:153003. https://doi.org/10.1016/j.phymed.2019.153003

Rashid S, Zafar M, Ahmad M, Lone FA, Shaheen S, Sultana, Shinwari MI (2018) Microscopic investigations and pharmacognostic techniques used for the standardization of herbal drug Nigella sativa L. Microsc Res Tech 81(12):1443–1450

Zhang J, Wider B, Shang H, Li X, Ernst E (2012) Quality of herbal medicines: challenges and solutions. Complement Ther Med 20(1-2):100–106. https://doi.org/10.1016/j.ctim.2011.09.004

Fernandes FH, Salgado HR (2016) Gallic acid: review of the methods of determination and quantification. Crit Rev Anal Chem 46(3):257–265. https://doi.org/10.1080/10408347.2015.1095064

Guimarães GP, Santos RL, Brandão DO, de Oliveira Cartaxo-Furtado NA, de Medeiros Cavalcanti AL, Macedo RO (2018) Thermoanalytical characterization of herbal drugs from Poincianella pyramidalis in different particle sizes. J Therm Anal Calorim 131(1):661–670

Cuinica LG, Macêdo RO (2018) Thermoanalytical characterization of plant drug and extract of Urtica dioica L. and kinetic parameters analysis. J Therm Anal Calorim 133(1):591–602

Liu Y, Yang L, Ma C, Zhang Y (2019) Thermal behavior of sweet potato starch by non-isothermal thermogravimetric analysis. Materials 12(5):699

Malucelli LC, Massulo T, Magalhães WL, Stofella NC, Vasconcelos EC, Carvalho Filho MAS, Murakami FS (2018) Thermal and chemical characterization of Dicksonia sellowiana extract by means of thermal analysis. Rev Bras 28(5):626–630

Toma CC, Tita B, Olah NK, Statti G (2018) Investigation of thermal behavior of Nigellae sativae semen from different types of extracts. Studia Universitatis Babes Bolyai Chemia 63(2)

Brandão DO, Guimarães GP, Santos RL, Júnior FJ, Silva KM, Souza FS, Macêdo RO (2016) Model analytical development for physical, chemical, and biological characterization of Momordica charantia vegetable drug. J Anal Methods Chem. https://doi.org/10.1155/2016/7528297

Alves R, Reis TV, Silva LC, Storpírtis S, Mercuri LP, Matos JD (2010) Thermal behavior and decomposition kinetics of rifampicin polymorphs under isothermal and non-isothermal conditions. Braz J Pharmaceut Sci 46(2):343–351. https://doi.org/10.1590/S1984-82502010000200022

Correia LP, Procópio JV, Santana CP, Pinto MF, Moura EA, Santos AF, Macêdo RO (2015) Herbal medicine physical quality evaluation by thermal analysis using adapted Ozawa method. J Therm Anal Calorim 122(1):207–214. https://doi.org/10.1007/s10973-015-4638-5

Neethu Kannan B, Gayathri Devi V, Anitha John LG, Natarajan M, Kanagarajan A (2019) Pharmacognostic evaluation and HPTLC fingerprinting of Pirantai Vatakam, a Siddha formulation. J Phytopharmacol 8(2):33–37

Do T, Santi I, Reich E (2019) A harmonized HPTLC method for identification of various caffeine containing herbal drugs, extracts, and products, and quantitative estimation of their caffeine content. J Liq Chromatogr Relat Technol 42(9-10):274–281

Tomar V, Beuerle T, Sircar D (2019) A validated HPTLC method for the simultaneous quantifications of three phenolic acids and three withanolides from Withania somnifera plants and its herbal products. J Chromatogr B 1124:154–160

Chewchida S, Vongsak B (2019) Simultaneous HPTLC quantification of three caffeoylquinic acids in Pluchea indica leaves and their commercial products in Thailand. Rev Bras 29(2):177–181

Frommenwiler DA, Kim J, Yook CS, Tran TTT, Cañigueral S, Reich E (2018) Comprehensive HPTLC fingerprinting for quality control of an herbal drug–the case of Angelica gigas root. Planta Med 84(06/07):465–474

Shawky E, El Newehy NM, Beltagy AM, Abd-Alhaseeb MM, Omran GA, Harraz FM (2018) Fingerprint profile and efficacy-associated markers of Nigella sativa oil for geographical origin determination using targeted and untargeted HPTLC-multivariate analysis. J Chromatogr B 1087:108–117

Pundarikakshudu K, Sharma AK, Bhatt CJ, Kanaki NS (2019) Development and validation of a high-performance thin-layer chromatographic (HPTLC) method for simultaneous quantification of Reserpine, Atropine, and Piperine in Sarpagandha Ghanvati, a classical ayurvedic preparation. J AOAC Int 102(4):1021–1026. https://doi.org/10.5740/jaoacint.18-0382

Abhimanyu KK, Ravindra CS, Avanapu RS (2017) A validated HPTLC method for the quantification of friedelin in Putranjiva roxburghii Wall extracts and in polyherbal formulations. Bull Faculty Pharm Cairo Univ 55(1):79–84. https://doi.org/10.1016/j.bfopcu.2016.11.002

Mangal AK, Tewari D, Shantha TR, Bansal S, Mangal M (2018) Pharmacognostical standardization and HPTLC fingerprinting analysis of Crocus sativus L

Laila O, Murtaza I, Abdin MZ, Ahmad S, Khan MS (2019) Development and validation of a high-performance thin-layer chromatography based method for the quantification of trigonelline in fenugreek (Trigonella foenum-graecum) seeds. JPC J Planar Chromatography-ModernTLC 32(2):95–102. https://www.researchgate.net/deref/http%3A%2F%2Fdx.doi.org%2F10.1556%2F1006.2019.32.2.3

Tomar V, Beeurle T, Sircar D (2019) A validated HPTLC method for the simultaneous quantifications of three phenolic acids and three withanolides from Withania somnifera plants and its herbal products. J Chromatogr B. https://doi.org/10.1016/j.jchromb.2019.06.009

Alam P, Kamal YT, Alqasoumi SI, Foudah AI, Alqarni MH, Yusufoglu HS (2019) HPTLC method for simultaneous determination of ascorbic acid and gallic acid biomarker from freeze dry pomegranate juice and herbal formulation. Saudi Pharmaceut J 27(7):975–980. https://doi.org/10.1016/j.jsps.2019.07.006

Hamburger M (2019) HPLC-based activity profiling for pharmacologically and toxicologically relevant natural products–principles and recent examples. Pharm Biol 57(1):328–334

Hemdan A, Tawakol SM (2018) HPLC–UV chromatographic methods for detection and quantification of undeclared withdrawn synthetic medications in counterfeit herbal medicines with confirmation by HPLC–PDA and mass spectrometry. Chromatographia 81(5):777–783

Walters NA, de Villiers A, Joubert E, de Beer D (2017) Improved HPLC method for rooibos phenolics targeting changes due to fermentation. J Food Compos Anal 55:20–29

Nag M, Kar A, Chanda J, Mukherjee PK (2019) RP-HPLC analysis of methanol extract of Viscum articulatum–a plant from Ayurveda. J Ayurveda Integrative Med. https://doi.org/10.1016/j.jaim.2018.02.135

Raclariu AC, Paltinean R, Vlase L, Labarre A, Manzanilla V, Ichim MC, de Boer H (2017) Comparative authentication of Hypericum perforatum herbal products using DNA metabarcoding, TLC and HPLC-MS. Sci Rep 7(1):1–12

Gitea D, Vicas S, Gitea MA, Nemeth S, Tit DM, Pasca, B.,& Iovan, C. (2018) HPLC screening of bioactives compounds and antioxidant capacity of different hypericum species. Rev Chim 69(2):305–309

Govindarajan R, Tejas V, Pushpangadan P (2019) High-performance liquid chromatography (HPLC) as a tool for standardization of complex herbal drugs. J AOAC Int 102(4):986–992

Sánchez-Camargo ADP, Parada-Alonso F, Ibáñez E, Cifuentes A (2019) Recent applications of on-line supercritical fluid extraction coupled to advanced analytical techniques for compounds extraction and identification. J Sep Sci 42(1):243–257

Liu TT, Cheong LZ, Man QQ, Zheng X, Zhang J, Song S (2019) Simultaneous profiling of vitamin D metabolites in serum by supercritical fluid chromatography-tandem mass spectrometry (SFC-MS/MS). J Chromatogr B 1120:16–23

Zhong Y (2019) Electronic nose for food sensory evaluation. In: Evaluation technologies for food quality. Woodhead Publishing, pp 7–22

Murcia-Morales M, Cutillas V, Fernández-Alba AR (2019) Supercritical fluid chromatography and gas chromatography coupled to tandem mass spectrometry for the analysis of pyrethroids in vegetable matrices: a comparative study. J Agric Food Chem 67(46):12626–12632

Huang Y, Wang T, Fillet M, Crommen J, Jiang Z (2019) Simultaneous determination of amino acids in different teas using supercritical fluid chromatography coupled with single quadrupole mass spectrometry. J Pharmaceut Anal 9(4):254–258

Varhan Oral E, Tokul-Ölmez Ö, Yener İ, Firat M, Tunay Z, Terzioğlu P et al (2019) Trace elemental analysis of allium species by inductively coupled plasma-mass spectrometry (ICP-MS) with multivariate chemometrics. Anal Lett 52(2):320–336

Rao JC, Naidu BG, Sarita P, Srikanth S, Raju GN (2019) Elemental analysis of Pterocarpus santalinus by PIXE and ICP-MS: chemometric approach. J Radioanal Nucl Chem 322(1):129–137

Tokalıoğlu Ş, Dokan FK, Köprü S (2019) ICP-MS multi-element analysis for determining the origin by multivariate analysis of red pepper flakes from three different regions of Turkey. LWT 103:301–307

Kumar V, Singh S, Singh A, Subhose V, Prakash O (2019) Assessment of heavy metal ions, essential metal ions, and antioxidant properties of the most common herbal drugs in Indian ayurvedic hospital: for ensuring quality assurance of certain ayurvedic drugs. Biocatalysis Agric Biotechnol 18:101018

Gonçalves DA, de Souza ID, Rosa ACG, Melo ESP, Goncalves AMB, de Oliveira LCS, do Nascimento VA (2019) Multi-wavelength calibration: determination of trace toxic elements in medicine plants by ICP OES. Microchem J 146:381–386

Marchetti L, Pellati F, Graziosi R, Brighenti V, Pinetti D, Bertelli D (2019) Identification and determination of bioactive phenylpropanoid glycosides of Aloysia polystachya (Griseb. et Moldenke) by HPLC-MS. J Pharm Biomed Anal 166:364–370

Nanjappan S, Paul D, Bolla L (2018) Assessing herb–drug interactions of herbal products with therapeutic agents for metabolic diseases: analytical and regulatory perspectives. Stud Nat Prod Chem 59:283–322

Zhou J, Cai H, Tu S, Duan Y, Pei K, Xu Y, Zhou Q (2018) Identification and analysis of compound profiles of sinisan based on ‘individual herb, herb-pair, herbal formula’ before and after processing using UHPLC-Q-TOF/MS coupled with multiple statistical strategy. Molecules 23(12):3128

Zhang A, Sun H, Wang X (2018) Mass spectrometry-driven drug discovery for development of herbal medicine. Mass Spectrom Rev 37(3):307–320

Gomathi D, Kalaiselvi M, Ravikumar G, Devaki K, Uma C (2015) GC-MS analysis of bioactive compounds from the whole plant ethanolic extract of Evolvulus alsinoides (L.) L. J Food Sci Technol 52(2):1212–1217

Saito K, Kaneko S, Furuya Y, Asada Y, Ito R, Sugie KI, Yanagawa Y (2019) Confirmation of synthetic cannabinoids in herb and blood by HS-SPME-GC/MS. Forensic Chem 13:100156

Huertas-Pérez JF, Ernest M, Badoud F (2019) Quantification of folpet and phthalimide in tea and herbal infusions by LC–high-resolution MS and GC–MS/MS. Food Additives Contaminants Part A 36(1):109–119

Taha SM, Gadalla SA (2017) Development of an efficient method for multi residue analysis of 160 pesticides in herbal plant by ethyl acetate hexane mixture with direct injection to GC-MS/MS. Talanta 174:767–779

Rutkowska E, Łozowicka B, Kaczyński P (2018) Modification of multiresidue QuEChERS protocol to minimize matrix effect and improve recoveries for determination of pesticide residues in dried herbs followed by GC-MS/MS. Food Anal Methods 11(3):709–724

Abraham A, Samuel S, Mathew L (2018) Phytochemical analysis of Pathyashadangam kwath and its standardization by HPLC and HPTLC. J Ayurveda Integrative Med 11(2):153–158