Preparation and Characterization of Hydroxyapatite Coatings on Ti6Al4V Alloy by a Sol‐Gel Method

Journal of the American Ceramic Society - Tập 82 Số 1 - Trang 27-32 - 1999
Wenjian Weng1, J.L. Baptista2
1Department of Materials Science and Engineering Zhejiang University, Hangzhou 310027, People's Republic of China
2Department of Ceramics and Glass Engineering, University of Aveiro, Aveiro 3810, Portugal

Tóm tắt

Hydroxyapatite coatings on Ti6Al4V substrates were prepared by a sol–gel method, and characterized by X‐ray diffraction, scanning electron microscopy, and infrared reflection spectroscopy. The coatings obtained at 500°C in air had a hydroxyapatite phase, some of which was carbonated hydroxyapatite, and had a dense and smooth morphology. When the coatings were treated in a simulated body fluid, the coatings had an increase in large hydroxyapatite grains, and a rough and porous morphology. The adhesive strength of the coatings was more than 14 MPa.

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Tài liệu tham khảo

Park J. B., 1992, Biomaterials—An Introduction, 2, 10.1007/978-1-4757-2156-0

10.1142/9789814317351_0012

10.1007/BF00120414

10.1002/jbm.820271205

10.1111/j.1151-2916.1996.tb08561.x

10.1007/BF00701082

LeGeros R. Z., 1995, Ceramic Transactions, 173

10.1007/BF00713445

Brinker C. J., 1992, Sol–Gel Science: The Physics and Chemistry of Sol–Gel Processing, 841

10.2109/jcersj.98.1255

W.WengandJ. L.Baptista “Synthesis of Ca Phosphates by PO(OH)x(OBut)3‐xand CaO2C2H4 ”J. Sol–Gel Sci. Technol. in press.

10.1016/S0022-3093(05)80586-1

10.1016/S0955-2219(96)00215-4

10.1111/j.1151-2916.1995.tb08435.x

T.Zhu “Preparation and Application of Lead Titanate Based Thin Films by Sol–Gel Processing”;Ph.D Dissertation.Zhejiang University Hangzhou People's Republic of China 1997.

10.1007/BF00355120