On-line chiral analysis using the kinetic method

Analyst, The - Tập 141 Số 8 - Trang 2441-2446
Ryan M. Bain1,2,3, Xin Yan1,2,3, Shannon A. Raab1,2,3, Stephen T. Ayrton1,2,3, Tawnya G. Flick4,5, R. Graham Cooks6,7,1,3
1Department of Chemistry, Purdue University, West Lafayette, IN USA
2Purdue University
3West Lafayette
4Amgen Inc., Thousand Oaks, CA USA
5Thousand Oaks
6Center for Analytical Instrumentation Development
7Center for Analytical Instrumentation Development, Purdue University, West Lafayette, IN,USA

Tóm tắt

Chiral analysis of constituents in solution-phase reaction mixtures can be performed by tandem mass spectrometry using the kinetic method to determine the enantiomeric excess (ee).

Từ khóa


Tài liệu tham khảo

Cooks, 1977, J. Am. Chem. Soc., 99, 1279, 10.1021/ja00446a059

McLuckey, 1981, J. Am. Chem. Soc., 103, 1313, 10.1021/ja00396a001

Nourse, 1991, Int. J. Mass Spectrom. Ion Processes, 106, 249, 10.1016/0168-1176(91)85022-E

Wong, 1997, J. Am. Soc. Mass Spectrom., 8, 68, 10.1016/S1044-0305(96)00154-7

Schroeter, 1998, Eur. J. Org. Chem., 565, 10.1002/(SICI)1099-0690(199804)1998:4<565::AID-EJOC565>3.0.CO;2-J

Burinsky, 1984, J. Am. Chem. Soc., 106, 2770, 10.1021/ja00322a007

Denault, 1998, J. Am. Soc. Mass Spectrom., 0305, 1141, 10.1016/S1044-0305(98)00092-0

Eberlin, 1994, J. Am. Chem. Soc., 116, 2457, 10.1021/ja00085a028

Yang, 1995, J. Mass Spectrom., 30, 807, 10.1002/jms.1190300605

Lioe, 2007, Int. J. Mass Spectrom., 267, 220, 10.1016/j.ijms.2007.02.038

Bouchoux, 2009, J. Phys. Chem. A, 113, 6666, 10.1021/jp902438a

Jarrold, 1987, J. Chem. Phys., 86, 3876, 10.1063/1.451948

Hanley, 1988, J. Phys. Chem., 5803, 10.1021/j100331a052

Boand, 1983, J. Am. Chem. Soc., 105, 2203, 10.1021/ja00346a600

Wright, 1982, Int. J. Mass Spectrom. Ion Phys., 42, 115, 10.1016/0020-7381(82)80057-0

Riffet, 2012, Int. J. Mass Spectrom., 316–318, 47, 10.1016/j.ijms.2011.12.014

O'Hair, 1992, Int. J. Mass Spectrom. Ion Processes, 117, 23, 10.1016/0168-1176(92)80083-D

Bortolini, 2011, Steroids, 76, 596, 10.1016/j.steroids.2011.02.028

Smith, 1996, Phosphorus, Sulfur Silicon Relat. Elem., 119, 49, 10.1080/10426509608043464

Ma, 1998, J. Mass Spectrom., 33, 943, 10.1002/(SICI)1096-9888(1998100)33:10<943::AID-JMS703>3.0.CO;2-B

Augusti, 2004, J. Mass Spectrom., 39, 558, 10.1002/jms.625

Yang, 1995, J. Mass Spectrom., 30, 184, 10.1002/jms.1190300128

Stöckigt, 1995, Int. J. Mass Spectrom. Ion Processes, 149–150, 1, 10.1016/0168-1176(95)04223-8

Gozzo, 2001, J. Mass Spectrom., 36, 1140, 10.1002/jms.219

Cheng, 1993, J. Am. Chem. Soc., 115, 4844, 10.1021/ja00064a052

Cerda, 1996, J. Am. Chem. Soc., 118, 11884, 10.1021/ja9613421

Cerda, 1998, J. Am. Chem. Soc., 120, 2437, 10.1021/ja972417j

Cooks, 1995, Mass Spectrom. Rev., 13, 287, 10.1002/mas.1280130402

Bouchoux, 2012, Mass Spectrom. Rev., 31, 391, 10.1002/mas.20349

Schröder, 2012, Methods Phys. Chem., 1, 63, 10.1002/9783527636839.ch3

Renaud, 2012, Eur. J. Mass Spectrom., 18, 223, 10.1255/ejms.1173

Wu, 2012, J. Pharm. Biomed. Anal., 69, 133, 10.1016/j.jpba.2012.04.022

Bouchoux, 2004, J. Mass Spectrom., 39, 986, 10.1002/jms.680

Bosesl, 2016, ARAC, 9

Young, 2007, Int. J. Mass Spectrom., 267, 199, 10.1016/j.ijms.2007.02.036

Fago, 2001, Angew. Chem., Int. Ed., 40, 4051, 10.1002/1521-3773(20011105)40:21<4051::AID-ANIE4051>3.0.CO;2-4

Paladini, 2003, Int. J. Mass Spectrom., 228, 349, 10.1016/S1387-3806(03)00129-5

Wu, 2003, J. Mass Spectrom., 38, 386, 10.1002/jms.450

Tao, 2001, Anal. Chem., 73, 1692, 10.1021/ac001150v

Augusti, 2002, Chem. Commun., 2242, 10.1039/b204421h

Augusti, 2002, Anal. Chem., 74, 3458, 10.1021/ac020135i

Nagy, 2015, J. Am. Soc. Mass Spectrom., 677, 10.1007/s13361-014-1072-z

Krogh, 2014, J. Mass Spectrom., 49, 1205, 10.1002/jms.3447

Ma, 2012, TrAC, 35, 50

Eberlin, 2007, Eur. J. Mass Spectrom., 13, 19, 10.1255/ejms.837

Ingram, 2015, Chem. Sci., 7, 39, 10.1039/C5SC02740C

Domingos, 2004, J. Org. Chem., 69, 7898, 10.1021/jo048737k

Yan, 2014, Angew. Chem., Int. Ed., 126, 6041, 10.1002/ange.201310493

Fang, 2010, J. Am. Chem. Soc., 132, 15525, 10.1021/ja107709w

Takats, 2004, Anal. Chem., 76, 4050, 10.1021/ac049848m

Ranc, 2008, Eur. J. Mass Spectrom., 14, 411, 10.1255/ejms.978

Wu, 2003, Anal. Chem., 75, 678, 10.1021/ac0260948

Yuchun, 2000, Int. J. Pharm., 196, 21, 10.1016/S0378-5173(99)00438-X