New Frontiers in Application of FTIR Microscopy for Characterization of Cultural Heritage Materials

Springer Science and Business Media LLC - Tập 374 - Trang 1-32 - 2016
S. Prati1, G. Sciutto1, I. Bonacini1, R. Mazzeo1
1Chemistry Department, Microchemistry and Microscopy Art Diagnostic Laboratory (M2ADL), University of Bologna, Ravenna, Italy

Tóm tắt

We present an overview of recent advances in the application of Fourier Transform Infrared (FTIR) microscopy for analysis of complex, multicomponent, and multilayer samples such as those typically encountered in the field of heritage materials. This technique is particularly useful since it allows identification and localization of both organic and inorganic (if IR active) compounds. New improvements have been possible thanks to the introduction of ad hoc sample preparation methods to obtain either thin or cross sections that allow both avoidance of contamination from organic embedding resin and improvement of the quality of the acquired spectra. Moreover, integrated use of spectra registered in the near-infrared (NIR) and mid-infrared (MIR) regions allows better comprehension of cross section composition. Data interpretation has been improved thanks to the development of chemometric methods for elaboration of hyperspectral data. A new and very promising field is the development of enhanced FTIR methods for detection of trace components in microextracts. These systems, allowing detection of extractable organic compounds from about 0.1 mg of sample, will be extremely useful in the future for analysis of natural and synthetic colorants, varnishes extracted, for instance, from cotton swabs used during cleaning of paintings, and organic residues on archeological remains.

Tài liệu tham khảo

Derrick MR, Stulik DC (1999) Infrared spectroscopy in conservation science. The Getty Conservation Institute, Los Angeles Casadio F, Toniolo L (2001) J Cult Herit 2:71–78 Gettens RJ (1952) Sci Am 187:22–27 Low MJD, Baer NS (1977) Stud Conserv 22:116–128 Messerschmidt RG, Harthcock MA (1988) Infrared microspectroscopy. Theory and applications. Marcel Dekker, New York Prati S, Jospeh E, Sciutto G, Mazzeo R (2010) Acc Chem Res 6:792–801 Gillard RD, Hardman SM (1994) Stud Conserv 39:187–192 Bruni S, Cariati F, Casadio F, Toniolo L (1999) Vibr Spectrosc 20:15–25 Dannenberg H, Forbes JW (1960) Anal Chem 32:365–370 Griffiths P, De Haseth JA (2007) Fourier transform infrared spectrometry, 2nd edn. Wiley, New Jersey Miliani C, Rosi F, Daveri A, Brunetti BG (2012) Appl Phys A 106:295–307 Rosi F, Federici A, Brunetti BG, Sgamellotti A, Clementi S, Miliani C (2011) Anal Bioanal Chem 39:3133–3145 Van der Weerd J, Brammer H, Boon JJ, Heeren RMA (2002) Appl Spectrosc 56:276–283 Reffner JA, Martoglio PA (1995) In: Huecki HJ (ed) Practical guide to infrared microspectroscopy. Marcel Dekker, New York Lewis L, Sommer AJ (1999) Appl Spectrosc 53:375–380 Lewis EN, Treado PJ, Reeder RC, Story GM, Dowrey AE, Marco C, Levin IW (1995) Anal Chem 67:3377–3381 Chan KLA, Kazarian SG (2003) Appl Spectrosc 57:381–389 Joseph E, Prati S, Sciutto G, Ioele M, Santopadre P, Mazzeo R (2010) Anal Bioanal Chem 396:899–910 Howard M (2001) In: Raghavachari R (ed) Near-infrared applications in biotechnology, Marcel Dekker, New York Pasquini C (2003) J Braz Chem Soc 14:198–219 Blanco M, Coello J, Iturriaga H, Maspoch S, de la Pezuela C (1998) Analyst 123:135–150 Cruz Sarraguça M, Almeida Lopez J (2009) Vibr Spectrosc 49:204–210 Reid LM, O’Donnell CP, Downey G (2006) Trends Food Sci Tech 17:344–353 Karoui R, de Baerdemaeker J (2007) Food Chem 102:621–640 Lachenal G (1995) Vibr Spetrosc 9:93–100 Rosi F, Daveri A, Doherty B, Nazzareni S, Brunetti BG, Sgamellotti A, Miliani C (2010) Appl Spectrosc 64:956–963 Bacci M, Magrini D, Picollo M, Vervat M (2009) J Cult Herit 10:275–280 Vagnini M, Miliani C, Cartechini L, Rocchi P, Brunetti BG, Sgamellotti A (2009) Anal Bioanal Chem 395:2107–2118 Milani C, Rosi F, Burnstock A, Brunetti BG, Sgamellotti A (2007) Appl Phys A 89:849–856 Rosi F, Daveri A, Miliani C, Verri G, Benedetti P, Piqué F, Brunetti BG, Sgamellotti A (2010) Anal Bioanal Chem 385:2097–2106 Trafela T, Strlic M, Kolar J, Lichtblau DA, Anders M, Pucko Mencigar D, Pihlar B (2007) Anal Chem 79:6319–6323 Nevin A, Comelli D, Osticioli I, Toniolo L, Valentini G, Cubeddu R (2009) Anal Bioanal Chem 395:2139–2149 Dooley KA, Lomax S, Zeibel JG, Miliani C, Ricciardi P, Hoenigswald A, Loew M, Delaney JK (2013) Analyst 138:4838–4848 Poli T, Chiantore O, Giovagnoli A, Piccirillo A (2012) Anal Bioanal Chem 402:2977–2984 Sciutto G, Prati S, Bonacini I, Oliveri O, Mazzeo R (2014) Microchem J 112:87–96 Prati S, Sciutto G, Mazzeo R, Torri C, Fabbri D (2011) Anal Bioanal Chem 399:3081–3091 Laurie AP (1914) The pigments and mediums of the old masters. Macmillan, London Gettens RJ (1936) Tech Stud Field Fine Arts 5:18–22 Plesters J (1956) Stud Conserv 2:110–157 Derrick M, Souza L, Kieslich T, Florsham H, Stulik D (1994) Am Instit Conserv 33:227–245 Pilc J, White R (1995) Natl Gallery Tech Bull 16:73–84 Cotte M, Checroun E, Mazel V, Solé A, Richardin P, Taniguchi Y, Walter P, Susini J (2009) E-Preserv Sci 6:1–9 Van der Weerd J, Heeren RMA, Boon JJ (2004) Stud Conserv 29:193–210 Tsang JS, Cunningham RH (1991) J Am Inst Conserv 30:163–177 Echard JP, Bertrand L, von Bohlen A, Le Hô AS, Paris C, Bellot-Gurlet L, Soulier B, Lattuati-Derieux A, Thao S, Robinet L, Lavédrine B, Vaiedelich S (2010) Angew Chem Int Ed 49:197–201 Janssens K, Alfeld M, Van der Snickt G, De Nolf W, Vanmeert F, Radepont M, Monico L, Dik J, Cotte M, Falkenberg G, Miliani C, Brunetti BG (2013) Annu Rev Anal Chem 6:399–425 Beltran V, Salvadó N, Butí S, Cinque G, Wehbe K, Pradell T (2015) Anal Chem 87:6500–6504 Salvadò N, Pradell T, Pantos E, Papiz MZ, Molera J, Seco M, Vendrell-Saz M (2002) J Synch Rad 9:215–222 Salvadò N, Butì S, Cotte M, Cinque G, Pradell T (2013) Appl Phys A 111:47–57 Salvadò N, Butì S, Nicholson J, Emerich H, Labrador A, Pradell T (2009) Talanta 79:419–428 Cotte M, Susini J (2008) J Anal At Spectr 23:820–828 Pouyet E, Lluveras-Tenorio A, Nevin A, Saviello D, Sette F, Cotte M (2014) Anal Chim Acta 822:51–59 Bertrand L, Robinet L, Cohen SX, Sandt C, Le Hô A, Soulier B, Lattuati-Derieux A, Echard J (2010) Anal Bioanal Chem 399:3025–3032 Echard JP, Cotte M, Dooryhee E, Bertrand L (2008) Appl Phys A 92:77–81 Mazzeo R, Joseph E, Prati S, Millemaggi A (2007) Anal Chim Acta 599:107–117 Prati S, Sciutto G, Catelli E, Ashashina A, Mazzeo R (2013) Anal Bioanal Chem 405:895–905 Prati S, Rosi F, Sciutto G, Mazzeo R, Magrini D, Sotiropoulou S, Van Bos M (2012) Microchem J 103:79–89 Ogura K, Kamidaira M, Asahina S, Erdman N (2007) Microsc Microanal 13:1518–1519 Boon JJ, Asahina S (2006) Microsc Microanal 12:1322–1323 Boon JJ, van der Horst J (2008) In: J Townsend (ed) Proceedings of the ICOMCC paintings working group meeting on grounds. Archetype, London De Fonjaudran CM, Nevin A, Piqué F, Cather S (2008) Anal Bioanal Chem 392:77–86 Jäegers E, Jäegers E (1999) Brit Mus Occas Pap 135:37–42 Muros V, Hirx J (2004) JAIC 43:75–89 Hopfe V, Korte EH, Klobes P, Griihlert W (1993) J Mol Struct 293:245–248 Chalmers JM, Everall NJ, Ellison S (1996) Micron 27:315–328 Prati S, Rosi F, Sciutto G, Oliveri P, Catelli E, Miliani C, Mazzeo R (2013) Microchem J 110:314–319 Treado PJ, Morris MD (1993) Microscopic and spectroscopic imaging of the chemical state. Marcel Dekker, New York Krishnan K, Powell JR, Hill SL (1995) In: Humecki HJ (ed) Practical guide to infrared microspectroscopy. Marcel Dekker, New York Wold S (1972) Kem Tidskr 84:34–37 Oliveri P, Casolino MC, Forina M (2010) Adv Food Nutr Res 61:57–117 Romero-Pastor J, Cardell C, Yebra-Rodríguez Á, Rodríguez-Navarro AB (2013) J Cult Herit 14:509–514 Sarmiento A, Pérez-Alonso M, Olivares M, Castro K, Martínez-Arkarazo I, Fernández LA, Madariaga JM (2011) Anal Bioanal Chem 399:3601–3611 Rosi F, Miliani C, Clementi C, Kahrim K, Presciutti F, Vagnini M, Manuali V, Daveri A, Cartechini L, Brunetti BG, Sgamellotti A (2010) Appl Phys A 100:613–624 Rosi F, Burnstock A, Van den Berg KJ, Miliani C, Brunetti, Navas N, Romero-Pastor JB, Manzano E, Cardell C (2008) Anal Chim Acta 630:141–149 Miliani C, Rosi F, Borgia I, Benedetti P, Brunetti BG, Sgamellotti A (2007) Appl Spectrosc 61:293–299 Rosi F, Miliani C, Federici A, Brunetti BG, Sgamellotti A, Clementi S (2010) Anal Bioanal Chem 399:3133–3145 Spring M, Ricci C, Peggie DA, Kazarian S (2008) Anal Bioanal Chem 392:37–45 Sciutto G, Oliveri P, Prati S, Quaranta M, Lanteri S, Mazzeo R (2013) Anal Bioanal Chem 405:625–633 Valcárcel M, Cárdenas S (2005) Trends Anal Chem 24:67–74 Vlasov Y, Legin A, Rudnitskaya A, Di Natale C, D’Amico A (2005) Pure Appl Chem 77:1965–1983 Fearn T (2009) NIR News 20:16–17 Savitzky A, Golay MJE (1964) Anal Chem 36:1627–1639 Taavitsainen VM, Brown SD, Tauler R, Walczak B (eds) (2009) Comprehensive chemometrics. Elsevier, Amsterdam Hartstein A, Kirtley JR, Tsang JC (1980) Phys Rev Lett 15:201–204 Osawa M, Matsuda N, Yoshii K, Uchida I (1994) Phys Chem 98:12702–12707 Osawa M (2001) Top Appl Phys 81:163–187 Fasasi A, Griffiths PR, Pan HB, Wai CM (2011) Appl Spectrosc 7:741–745 Yang J, Griffiths PR (2007) Anal Bioanal Chem 388:109–119 Osawa M, Ikeda M (1991) J Phys Chem 95:9914–9919 Bjerke AE, Griffiths PR, Theiss W (1991) Anal Chem 71:1967–1974 Aroca R, Price B (1997) J Phys Chem 101:6537–6540 Hahn F, Melendres CA (2001) Electrochim Acta 46:3525–3534 Seelenbinder JA, Brown CW, Pivarnik P, Rand AG (1999) Anal Chem 71:1963–1966 Aroca F, Ross J, Domingo C (2004) Appl Spectrosc 58:324–338 Masson JF, Murray-Méthot MP, Live LS (2010) Analyst 135:1483–1489 Saito Y, Wang JJ, Smith DA, Batchelder DN (2002) Langmuir 18:2959–2961 Sockalingum GD, Beljebbar A, Morjani H, Angiboust JF, Manfait M (1998) Biospectroscopy 4:71–78 Wanzenböck HD, Mizaikoff B, Weissenbacher N, Kellner R (1998) Fresen J Anal Chem 362:15–20 Polubotko AM (1993) Phys Lett A 173:424–432 Badilescu S, Ashrit PV, Truong VV, Badilescu L (1989) Appl Spectrosc 43:549–551 Milosevic M, Berets SL, Fadeev AY (2003) Appl Spectrosc 57:724–727 Milosevic M (2012) Internal reflection and ATR spectroscopy. Wiley, New Jersey Mulcahy ME, Berets SL, Milosevic M, Michl J (2004) J Phys Chem B 108:1519–1521 Milosevic M, Milosevic V, Berets SL (2007) Appl Spectrosc 61:530–536 Christie RM (2001) Colour chemistry. RSC Paperbacks, London Zhang X, Laursen RA (2005) Anal Chem 77:2022–2025 van Bommel MR, Vanden Berghe I, Wallert AM, Boitelle R, Wouters J (2007) J Chromatogr A 1157:260–272 Gulmini M, Idone A, Diana E, Gastaldi D, Vaudan D, Aceto M (2013) Dyes Pigments 98:136–145 Lee J, Kim MH, Lee KB, van Elslande E, Walter P, Lee Y (2014) Surf Interface Anal 46:312–316 Vandenabeele P, Moens L (2012) J Raman Spectrosc 43:1545–1550 Casadio F, Leona M, Lombardi JR, van Duyne RP (2010) Acc Chem Res 43:782–791 Casadio F, van Duyne RP (2013) Analyst 138:7276–7278 Leona M, Decuzzi P, Kubic TA, Gates G, Lombardi JR (2011) Anal Chem 83:3990–3993 Lofrumento C, Ricci M, Platania E, Becucci M, Castellucci E (2013) J Raman Spectrosc 44:47–54 Pozzi F, Lombardi JR, Bruni S, Leona M (2012) Anal Chem 84:3751–3757 Canamares MV, Garcia-Ramos JV, Gomez-Varga JD, Domingo C, Sanchez-Cortes S (2007) Langmuir 23:5210–5215 Prati S, Quaranta M, Sciutto G, Bonacini I, Litti L, Meneghetti M, Mazzeo R (2014) Herit Sci 2:28 Amendola V, Meneghetti M (2007) J Mater Chem 17:4705–4710 Blumich B, Casanova F, Perlo J, Presciutti F, Anselmi C, Doherty B (2010) Acc Chem Res 43:761–770 Targowski P, Iwanicka M (2012) Appl Phys A 106:265–277