Modification of Multiresidue QuEChERS Protocol to Minimize Matrix Effect and Improve Recoveries for Determination of Pesticide Residues in Dried Herbs Followed by GC-MS/MS
Tóm tắt
Từ khóa
Tài liệu tham khảo
Attallah ER, Barakat DA, Maatook GR, Badawy HA (2012) Validation of a quick and easy (QuEChERS) method for the determination of pesticides residue in dried herbs. J Food Agric Environ 10(1):755–762
Anastassiades M, Lehotay SJ, Stajnbaher D, Schenck FJ (2003a) Fast and easy multiresidue method employing acetonitrile extraction/partitioning and “dispersive solid-phase extraction” for the determination of pesticide residues in produce. J AOAC Int 86(2):412–431
Anastassiades M, Mastovska K, Lehotay SJ (2003b) Evaluation of analyte protectants to improve gas chromatographic analysis of pesticides. J Chromatogr A 1015:163–184
CA Codex Alimentarius (2016) Food and Agriculture Organization of the United Nations. https://www.fao.org/fao-who-codexalimentarius/codex-home/en/ . Accessed 22 August 2016
Chen L, Song F, Liu Z, Zheng Z, Xing J, Liu S (2012) Multi-residue method for fast determination of pesticide residues in plants used in traditional Chinese medicine by ultra-high-performance liquid chromatography coupled to tandem mass spectrometry. J Chromatogr A 1225:132–140
Dai R, Ren X, He X, Huo Y (2011) Convenient analytical method for quantitative determination of 23 pesticide residues in herbs by gas chromatography–mass spectrometry. B Environ Contam Tox 86:559–564
Du B, Li X, Liu H (2007) Determination of organochlorine pesticide residues in herbs by capillary gas chromatography. Life Sci J 4(1):40–42
Du G, Xiao Y, Yang HR, Wang L, Song YL, Wang YT (2012) Rapid determination of pesticide residues in herbs using selective pressurized liquid extraction and fast gas chromatography coupled with mass spectrometry. J Sep Sci 35:1922–1932
EC Regulation No 396/2005 Of the European Parliament and of the Council of 23 February 2005 on maximum residue levels of pesticides in or on food and feed of plant and animal origin and amending Council Directive 91/414/EEC. Off J Eur Union L 70/1, 16.3.2005, with later amendments. https://eur-lex.europa.eu/legal-content/EN/TXT/PDF/?uri=CELEX:32005R0396&from=en . Accessed 04 May 2017
EFSA European Food Safety Authority (2015) Scientific report of EFSA. The 2013 European Union report on pesticide residues in food. EFSA J 13(3):4038. https://www.efsa.europa.eu/sites/default/files/scientific_output/files/main_documents/4038.pdf . Accessed 22 August 2016
EP 8.0 European Directorate for the Quality of Medicines and HealthCare (2014) European Pharmacopoeia, 8th edition, European Directorate for the Quality of Medicines and HealthCare, Strasbourg, France
Ferrer C, Lozano A, Agüera A, Girón AJ, Fernández-Alba AR (2011) Overcoming matrix effects using the dilution approach in multiresidue methods for fruits and vegetables. J Chromatogr A 1218(42):7634–7639
Ghani SBA (2014) Determination of multiclass pesticides in dry herbs using GC-ECD. J Appl Sci Agr 9(3):955–959
Gondo TT, Obuseng VC, Mmualefe LC, Okatch H (2016) Employing solid phase microextraction as extraction tool for pesticide residues in traditional medicinal plants. J Anal Methods Chem. https://doi.org/10.1155/2016/2890219
Hajou RM, Afifi FU, Battah AH (2004) Comparative determination of multi-pesticide residues in Pimpinella anisum using two different AOAC methods. Food Chem 88:469–478
Hajslova J, Holadova K, Kocourek V, Poustka J, Godula M, Cuhra P, Kempny M (1998) Matrix-induced effects: a critical point in gas chromatographic analysis of pesticide residues. J Chromatogr A 80:283–295
Ho YM, Tsoi YK, Leung KSY (2013) Highly sensitive and selective organophosphate screening in twelve commodities of fruits, vegetables and herbal medicines by dispersive liquid–liquid microextraction. Anal Chim Acta 775:58–66
Hu Y, Wan L, Zhang J, Yang F, Cao J (2012) Rapid determination of pesticide residues in Chinese materia medica using QuEChERS sample preparation followed by gas chromatography–mass spectrometry. Acta Pharm Sin B 2(3):286–293
Hwang BH, Lee MR (2000) Solid-phase microextraction for organochlorine pesticide residues analysis in Chinese herbal formulations. J Chromatogr A 898:245–256
Kaczyński P, Łozowicka B, Jankowska M, Hrynko I (2016) Rapid determination of acid herbicides in soil by liquid chromatography with tandem mass spectrometric detection based on dispersive solid phase extraction. Talanta 152:127–136
Kinsella B, O’Mahony J, Malone E, Moloney M, Cantwell H, Furey A, Danaher M (2009) Current trends in sample preparation for growth promoter and veterinary drug residue analysis. J Chromatogr A 1216:7977–8015
Kwon H, Lehotay SJ, Geis-Asteggiante L (2012) Variability of matrix effects in liquid and gas chromatography–mass spectrometry analysis of pesticide residues after QuEChERS sample preparation of different food crops. J Chromatogr A 1270:235–245
Lehotay SJ, Mastovská K, Lightfield AR (2005a) Use of buffering and other means to improve results of problematic pesticides in a fast and easy method for residue analysis of fruit and vegetables. J AOAC Int 88(2):615–629
Lehotay SJ, Mastovská K, Yun SJ (2005b) Evaluation of two fast and easy methods for pesticide residue analysis in fatty food matrixes. J AOAC Int 88(2):630–638
Lehotay SJ, Son K, Kwon H, Koesukwiwat U, Fu W, Mastovska K et al (2010) Comparison of QuEChERS sample preparation methods for the analysis of pesticide residues in fruits and vegetables. J Chromatogr A 1217(16):2548–2560
Li W, Liu Y, Duan J, Saint CP, Mulcahy D (2015) The role of methanol addition to water samples in reducing analyte adsorption and matrix effects in liquid chromatography-tandem mass spectrometry. J Chromatogr A 1389:76–84
Liu XQ, Li YF, Meng WT, Li DX, Sun H, Tong L, Sun GX (2016) A multi-residue method for simultaneous determination of 74 pesticides in Chinese material medica using modified QuEChERS sample preparation procedure and gas chromatography tandem mass spectrometry. J Chromatogr B 1015–1016:1–12
Lozano A, Rajski Ł, Belmonte-Valles N, Uclés A, Uclés S, Mezcua M, Fernández-Alba AR (2012) Pesticide analysis in teas and chamomile by liquid chromatography and gas chromatography tandem mass spectrometry using a modified QuEChERS method: validation and pilot survey in real samples. J Chromatogr A 1268:109–122
Lozano A, Rajski Ł, Uclés A, Belmonte-Valles N, Mezcua M, Fernández-Alba AR (2014) Evaluation of zirconium dioxide-based sorbents to decrease the matrix effect in avocado and almond multiresidue pesticide analysis followed by gas chromatography tandem mass spectrometry. Talanta 118:68–83
Łozowicka B, Jankowska M, Rutkowska E, Hrynko I, Kaczynski P, Micinski J (2013) The evaluation of a fast and simple pesticide multiresidue method in various herbs by gas chromatography. J Nat Med 68:95–111
Łozowicka B, Ilyasova G, Kaczynski P, Jankowska M, Rutkowska E, Hrynko I, Mojsak P, Szabunko J (2016) Multi-residue methods for the determination of over four hundred pesticides in solid and liquid high sucrose content matrices by tandem mass spectrometry coupled with gas and liquid chromatograph. Talanta 151:51–61
Matyjaszczyk E (2011) Selected aspects of plant protection in Poland, five years on from EU accession. Outlook Agr 40(2):119–123
Nantia EA, Moreno-González D, Manfo FPT, Gámiz-Gracia L, García-Campaña AM (2017) QuEChERS-based method for the determination of carbamate residues in aromatic herbs by UHPLC-MS/MS. Food Chem 216:334–341
Nguyen TD, Lee KJ, Lee MH, Lee GH (2010) A multiresidue method for the determination 234 pesticides in Korean herbs using gas chromatography mass spectrometry. Microchem J 95:43–49
PPDB Pesticide Properties Database (2016) University of Hertfordshire. https://sitem.herts.ac.uk/aeru/ppdb/en/index.htm . Accessed 22 August 2016
Rao MM, KumarMeena A, Galib E (2011) Detection of toxic heavy metals and pesticide residue in herbal plants which are commonly used in the herbal formulations. Environ Monit Assess 181:267–271
Qian G, Rimao H, Feng T, Wu X, Xuede L, Haiqun C, Yanhong S, Jun T (2010) A multiresidue method for 20 pesticides in Radix paeoniae Alba of Chinese herb by gas chromatography with electron-capture detection. B Environ Contam Tox 84:779–783
Sadowska-Rociek A, Surma M, Cieślik E (2013) Application of QuEChERS method for simultaneous determination of pesticide residues and PAHs in fresh herbs. B Environ Contam Tox 90(4):508–513
Sanchez-Brunette C, Albero B, Martin G, Tadeo JL (2005) Determination of pesticide residues by GC–MS using analyte protectants to counteract the matrix effect. Anal Sci 12:1219–1296
SANTE (2015) Document No. SANTE/11945/2015. Guidance document on analytical quality control and method validation procedures for pesticides residues analysis in food and feed. https://ec.europa.eu/food/plant/docs/plant_pesticides_mrl_guidelines_wrkdoc_11945_en.pdf . Accessed 22 August 2016
Sarkhail P, Yunesian M, Ahmadkhaniha R, Sarkheil P, Rastkari N (2012) Levels of organophosphorus pesticides in medicinal plants commonly consumed in Iran. Daru 20:9
Słowik-Borowiec M (2015) Validation of a QuEChERS-based gas chromatographic method for multiresidue pesticide analysis in fresh peppermint including studies of matrix effects. Food Anal Method 8(6):1413–1424
Storelli MM (2014) Evaluation of toxic metal (Hg, Cd, Pb), polychlorinated biphenyl (PCBs), and pesticide (DDTs) levels in aromatic herbs collected in selected areas of southern Italy. Environ Sci Pollut R 21(2):946–953
Tong H, Tong Y, Xue J, Liu D, Wu X (2014) Multi-residual pesticide monitoring in commercial Chinese herbal medicines by gas chromatography–triple quadrupole tandem mass spectrometry. Food Anal Method 7(1):135–145
Tuzimski T (2011) Determination of analytes in medical herbs extracts by SPE coupled with two-dimensional planar chromatography in combination with diode array scanning densitometry and HPLC-diode array detector. J Sep Sci 34(1):27–36
Van De Steene JC, Mortier KA, Lambert WE (2006) Tackling matrix effects during development of a liquid chromatographic–electrospray ionisation tandem mass spectrometric analysis of nine basic pharmaceuticals in aqueous environmental samples. J Chromatogr A 1123:71–81
Walorczyk S, Drożdżyński D, Kierzek R (2015) Two-step dispersive-solid phase extraction strategy for pesticide multiresidue analysis in a chlorophyll-containing matrix by gas chromatography-tandem mass spectrometry. J Chromatogr A 1412:22–32
Wan YQ, Mao XJ, Yan AP, Shen MY, Wu YM (2010) Simultaneous determination of organophosphorus pesticides in Chinese herbal medicines by microwave-assisted extraction coupled with dispersive-solid phase extraction and gas chromatography. Biomed Chromatogr 24:961–968
Wang Y, Jin HY, Ma SC, Lu J, Lin RC (2011) Determination of 195 pesticide residues in Chinese herbs by gas chromatography–mass spectrometry using analyte protectants. J Chromatogr A 1218:334–342
Zrostlíková J, Hajšlová J, Godula M, Maštovská K (2001) Performance of programmed temperature vaporizer, pulsed splitless and on-column injection techniques in analysis of pesticide residues in plant matrices. J Chromatogr A 937:73–86