Experimental Measurement of the Saddle Node Region in a Distillation Column Profile Map by Using a Batch Apparatus

Castillo, 1998, Homogeneous azeotropic distillation. 1. Design procedure for single-feed columns at nontotal reflux, Ind Eng Chem Res, 37, 987, 10.1021/ie970480b Chronis, 1997, 1, 187 Doherty, 1985, Design and synthesis of homogeneous azeotropic distillation. 3. The sequence of columns for azeotropic and extractive distillation, Ind Eng Chem Fundam, 24, 474, 10.1021/i100020a012 Doherty, 1978, On the dynamics of distillation processes, I-VII, Chem Eng Sci, 34 King, 1980 Koehler, 1995, A review on minimum energy calculations for ideal and non ideal distillation, Ind Eng Chem Res, 34, 1003, 10.1021/ie00043a001 Modise, 2005, Can the operating leaves of a distillation column really be expanded?, Ind Eng Chem Res, 44, 7511, 10.1021/ie0488086 Nikolaev, 1979, Utilization of functional operation for determining the region of continuous rectification, Theor Found Chem Eng, 13, 418 Petlyuk, 1978, Rectification of zeotropic, azeotropic, and continuous mixtures in simple and complex infinite columns with finite reflux, Theor Found Chem Eng, 12, 671 Sandler, 1999 Tapp, 2003, An experimental simulation of distillation column concentration profiles using a batch apparatus, Chem Eng Sci, 58, 479, 10.1016/S0009-2509(02)00469-4 Tapp, 2004, Column profile maps. 1. Derivation and Interpretation, Ind Eng Chem Res, 43, 364, 10.1021/ie030165r Wahnschafft, 1992, The product composition regions of single-feed azeotropic distillation columns, Ind Eng Chem Res, 31, 2345, 10.1021/ie00010a014