Direct transesterification of all classes of lipids in a one-step reaction.
Tóm tắt
Từ khóa
Tài liệu tham khảo
Thomas, 1981, Hydrogenated oils and fats: the presence of chemicallymodified fatty acids in human adipose tissue, Am. J. Clin. Nutr., 34, 877, 10.1093/ajcn/34.5.877
Wolff, 1984, Plasma and red blood cell fatty acid composition in children with protein-calorie malnutrition, Pediatr. Res., 18, 162, 10.1203/00006450-198402000-00010
Haan, 1979, Analysis of fatty acids from human lipids by gas chromatography, J. Chromatogr., 162, 261, 10.1016/S0378-4347(00)81513-3
MacGee, 1974, Preparation of methyl esters from the saponifiable fatty acids in small biological specimens for gas-liquid chromatographic analysis, J. Chromatogr., 100, 35, 10.1016/S0021-9673(00)86037-9
Shimasaki, 1977, Direct transesterification of lipids in mammalian tissue for fatty acid analysis via dehydration with 2, 2'-dimethoxypropane, J. Lipid Res., 18, 540, 10.1016/S0022-2275(20)41672-4
Gerhardt, 1977, Rapid microdetermination of fatty acids in biological materials by gasliquid chromatography, J. Chromatogr., 143, 335, 10.1016/S0378-4347(00)80980-9
Penttila, 1984, Simultaneous measurement of free and esterified fatty acids by gas chromatography from normal and type IV hyperlipoproteinaemic sera, Ann. Clin. Res., 16, 13
Lillington, 1981, A rapid and simple method for the esterification of fatty acids and steroid carboxylic acids prior to gas-liquid chromatography, Clin. Chim. Acta., Ill, 91, 10.1016/0009-8981(81)90425-3
Folch, 1957, A simple method for the isolation and purification of total lipids from animal tissues, J. Biol. Chem., 226, 497, 10.1016/S0021-9258(18)64849-5
Klein, 1980, The use of 13-methyl-tetradecanoic acid as an indicator of adipose tissue turnover, Lipids., 15, 572, 10.1007/BF02534181
Lepage, 1984, Improved recovery of fatty acid through direct transesterification without prior extraction or purification, J. Lipid Res., 25, 1391, 10.1016/S0022-2275(20)34457-6
MacGee, 1981, Preparation of sphingolipid fatty acid methyl esters for determination by gas-liquid chromatography, J. Chromatogr., 205, 281, 10.1016/S0021-9673(00)82656-4
Gurr, 1975, 138
Morrison, 1964, Preparation of fatty acid methyl esters and dimethylacetals from lipids with boron fluoride-methanol, J. Lipid Res., 5, 600, 10.1016/S0022-2275(20)40190-7
Ohlrogge, 1981, Human tissue lipids: occurrence of fatty acid isomers from dietary hydrogenated oils, J. Lipid Res., 22, 955, 10.1016/S0022-2275(20)37333-8
Goetz, 1982, Capillary gas chromatographic analysis of human skin surface lipids after microsampling on ground-glass platelets, J. Chromatogr., 233, 19, 10.1016/S0378-4347(00)81727-2
Rogiers, 1977, The application of an improved gasliquid chromatographic method for the determination of the long chain nonesterified fatty acid pattern of blood plasma in children, Clin. Chim. Acta., 78, 227, 10.1016/0009-8981(77)90310-2
Christie, 1982, A simple procedure for rapid transmethylation of glycerolipids and cholesteryl esters, J. Lipid Res., 23, 1072, 10.1016/S0022-2275(20)38081-0
Bitman, 1981, Two-stage, one-dimensional thin-layer chromatographic method for separation of lipid classes, J. Liq. Chromatogr., 4, 1007, 10.1080/01483918108059601
Putnam, 1982, The effect of variations in dietary fatty acids on the fatty acid composition of erythrocyte phosphatidylcholine and phosphatidylethanolamine in human infants, Am. J. Clin. Nutr., 36, 106, 10.1093/ajcn/36.1.106
Nelson, 1975, Isolation and purification of lipids from animal tissues, 1
Yunker, 1981, Simultaneous quantitation of biliary cholesterol, bile acids, and phospholipids (as fatty acids), by gas-liquid chromatography, with campesterol as internal standard, Clin. Chem., 27, 1779, 10.1093/clinchem/27.10.1779
Bolton, 1978, A simplified procedure for the analysis of cholesterol, phospholipids and bile salts in human bile, Clin. Chim. Acta., 83, 177, 10.1016/0009-8981(78)90222-X