A New Standard Substance for Calibration of Circular Dichroism: Ammonium d-10-Camphorsulfonate

Takashi Takakuwa1, Toshio Konno2, Hiroshi Meguro3
1Application Laboratory, Japan Spectroscopic Co. Ltd., Ishikawa-cho, Hachioji, Japan
2Faculty of Education, Niigata University, Igarashi-Ninocho, Niigata, Japan
3Department of Food Chemistry, Faculty of Agriculture, Tohoku University, Tsuzumidori-Amamiya, Sendai 980, Japan

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Tài liệu tham khảo

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The two recrystallizations were sufficient for CSA as starting reagents from Tokyo Kasei Co., Aldrich Chemical Co. and Baker Chemical Co.

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This reagent was prepared by a method similar to ours and was purified from ethanol. However, the [θ], [M] and [α]D agreed with ours (less than 0.1 % of error).