A New Standard Substance for Calibration of Circular Dichroism: Ammonium d-10-Camphorsulfonate
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T. Konno, H. Meguro, T. Murakami and M. Hatano, Chem. Lett., 1981, 953.
K. Tsuzimura, T. Konno, H. Meguro, M. Hatano, T. Murakami, K. Kashiwabara, K. Saito, Y. Kondo and T. M. Suzuki, Anal. Biochem., 81, 167 (1977).
A. J. Alder, N. J. Greenfield and G. D. Fasman, “Methods in Enzymology vol. XXVII.”, edited by C. H. W. Hirs and S. N. Timasheff, p. 675, Academi Press, New York and London (1973).
T. Takakuwa, T. Konno and H. Meguro, unpublished data.
The two recrystallizations were sufficient for CSA as starting reagents from Tokyo Kasei Co., Aldrich Chemical Co. and Baker Chemical Co.
“THE Merck index”, 9th Edition, p. 220, Merck&Co., Rahway, N. J. (1976).
This reagent was prepared by a method similar to ours and was purified from ethanol. However, the [θ], [M] and [α]D agreed with ours (less than 0.1 % of error).