Towards a standardization of biomethane potential tests

Water Science and Technology - Tập 74 Số 11 - Trang 2515-2522 - 2016
Christof Holliger1, M. M. Alves2, Diana R. Andrade‐Linares3, Irini Angelidaki4, Sergi Astals5, Urs Baier6, Claire Bougrier7, Pierre Buffière8, Marta Carballa9, Vinnie de Wilde10, Florian Ebertseder3, Belén Fernández11, E. Ficara12, Ioannis A. Fotidis4, Jean‐Claude Frigon13, Hélène Fruteau de Laclos14, Dara S.M. Ghasimi15, Gabrielle Hack1, Mathias Hartel3, J. Heerenklage16, Ilona Sárvári Horváth17, Pavel Jeníček18, Konrad Koch19, Judith Krautwald6, Javier Lizasoain20, Jing Liu21, Lona Mosberger6, Mihaela Nistor21, Hans Oechsner22, João Vítor Oliveira23, M.A.J. Paterson24, André Pauss25, Sébastien Pommier26, I. Porqueddu12, F. Raposo27, Thierry Ribeiro28, Florian Rüsch Pfund6, Sten Strömberg21, Michel Torrijos29, M.H.A. van Eekert30, Jules B. van Lier15, Harald Wedwitschka31, Isabella Wierinck32
1ENAC IIE Laboratory for Environmental Biotechnology, Ecole Polytechnique Fédérale de Lausanne (EPFL), Lausanne, Switzerland
2IBB-CBE - Centre of Biological Engineering [Univ. Minho] (Institute for Biotechnology and Bioengineering, University of Minho, Campus de Gualtar, 4710-057 Braga - Portugal)
3Bavarian State Research Center for Agriculture, Freising, Germany
4DTU - Danmarks Tekniske Universitet = Technical University of Denmark (Anker Engelunds Vej 1 , Bygning 101A , 2800 Kgs. Lyngby - Denmark)
5Advanced Water Management Center, The University of Queensland, Brisbane, Australia
6Institute for Chemistry and Biotechnology, ZHAW School of Life Sciences and Facility Management, Wädenswil, Switzerland
7Veolia Environnement Research and Innovation (France)
8Université de Lyon, INSA-Lyon, Lyon, France
9Department of Chemical Engineering, Institute of Technology, Universidade de Santiago de Compostela, Santiago de Compostela, Spain
10Sub-Department of Environmental Technology (Biotechnion Bomenweg 2 6700 EV Wageningen - Netherlands)
11IRTA, Barcelona, Spain
12DICA - Dipartimento di Ingegneria Civile e Ambientale (P.zza Leonardo da Vinci 32, 20133 Milano (Italie) - Italy)
13NRC - National Research Council of Canada (1200 Montreal Road, Building M-58, Ottawa, Ontario K1A 0R6 - Canada)
14Methaconsult, Préverenges, Switzerland
15TU Delft - Delft University of Technology (Postbus 5, 2600 AA Delft - Netherlands)
16Hamburg University of Technology, Hamburg, Germany
17The Swedish Centre for Resource Recovery, University of Borås, Borås, Sweden
18University of Chemistry and Technology Prague, Prague, Czech Republic
19Chair of Urban Water Systems Engineering, Technical University of Munich, Garching, Germany
20University of Natural Resources and Life Sciences Vienna, Austria
21Bioprocess Control AB, Lund, Sweden
22State Institute of Agricultural Engineering and Bioenergy, University of Hohenheim, Stuttgart, Germany
23Centre of Biological Engineering, University of Minho, Braga, Portugal
24Association for Technology and Structures in Agriculture (KTBL), Darmstadt, Germany
25Sorbonne Universités, EA 4297 TIMR UTC/ESCOM, Compiègne, France
26LISBP, Université de Toulouse, CNRS, INRA, INSA, Toulouse, France
27Instituto de la Grasa (Campus de la Universidad Pablo de Olavide - Edificio 46 Ctra. de Utrera, km. 1 - 41013 - Sevilla - Spain)
28Département des Sciences et Techniques Agro-Industrielles, Institut Polytechnique LaSalle Beauvais, Beauvais, France
29LBE - Laboratoire de Biotechnologie de l'Environnement [Narbonne] (Avenue des Etangs - 11100 Narbonne - France)
30LeAF, Wageningen, the Netherlands
31DBFZ Deutsches Biomasseforschungszentrum, Leipzig, Germany
32OWS - Organic Waste Systems (Dok Noord 5, 9000 Gent - Belgium)

Tóm tắt

Production of biogas from different organic materials is a most interesting source of renewable energy. The biomethane potential (BMP) of these materials has to be determined to get insight in design parameters for anaerobic digesters. Although several norms and guidelines for BMP tests exist, inter-laboratory tests regularly show high variability of BMPs for the same substrate. A workshop was held in June 2015, in Leysin, Switzerland, with over 40 attendees from 30 laboratories around the world, to agree on common solutions to the conundrum of inconsistent BMP test results. This paper presents the consensus of the intense roundtable discussions and cross-comparison of methodologies used in respective laboratories. Compulsory elements for the validation of BMP results were defined. They include the minimal number of replicates, the request to carry out blank and positive control assays, a criterion for the test duration, details on BMP calculation, and last but not least criteria for rejection of the BMP tests. Finally, recommendations on items that strongly influence the outcome of BMP tests such as inoculum characteristics, substrate preparation, test setup, and data analysis are presented to increase the probability of obtaining validated and reproducible results.

Từ khóa


Tài liệu tham khảo

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VDI 4630, 2016