Initial step of B12-dependent enzymatic catalysis: energetic implications regarding involvement of the one-electron-reduced form of adenosylcobalamin cofactor

JBIC Journal of Biological Inorganic Chemistry - Tập 17 - Trang 293-300 - 2011
Pawel M. Kozlowski1, Takashi Kamachi2, Manoj Kumar1, Kazunari Yoshizawa2
1Department of Chemistry, University of Louisville, Louisville, USA
2Institute for Materials Chemistry and Engineering, Kyushu University, Fukuoka, Japan

Tóm tắt

Density functional theory analysis was performed to elucidate the impact of one-electron reduction upon the initial step of adenosylcobalamin-dependent enzymatic catalysis. The transition state (TS) corresponding to the Co–C bond cleavage and subsequent hydrogen abstraction from the substrate was located. The intrinsic reaction coordinate calculations predicted that the reaction consisting of Co–C5′ bond cleavage in [CoIII(corrin•)]–Rib (where Rib is ribosyl) and hydrogen-atom abstraction from the CH3–CH2–CHO substrate occurs in a concerted fashion. The computed activation energy barrier of the reaction (15.0 kcal/mol) was lowered by approximately 54.5% in comparison with the reaction involving the positively charged cofactor model (Im–[CoIII(corrin)]–Rib+, where Im is imidazole; energy barrier = 33.0 kcal/mol). The Im base was detached during the TS search in the reaction involving the one-electron-reduced analogue. Thus, to compare the energetics of the two reactions, the axial Im ligand detachment energy for the Im–[CoIII(corrin•)]–Rib model was computed [7.6 kcal/mol (gas phase); 4.6 kcal/mol (water)]. Consequently, the effective activation energy barrier for the reaction mediated by the Im-off [CoIII(corrin•)]–Rib was estimated to be 22.6 kcal/mol, which implied an overall 31.5% reduction in the energetic demands of the reaction. Considering that the lengthened Co–Naxial bond has been observed in X-ray crystal structure studies of B12-dependent mutases, the catalytic impact induced by one-electron reduction of the cofactor is expected to be higher in the presence of the enzymatic environment.

Tài liệu tham khảo

Marzilli LG (1993) In: Reedijk J (ed) Bioinorganic catalysis. Marcel Dekker, New York, p 227 Kräutler B, Arigoni D, Golding BT (eds) (1998) Vitamin B12 and B12 proteins. Lectures presented at the 4th European symposium on vitamin B12 and B12 proteins. Wiley-VCH, New York Banerjee R (1999) Chemistry and biochemistry of B12. Wiley, New York Toraya T (2003) Chem Rev 103:2095–2127 Toraya T (2000) Cell Mol Life Sci 57:106–127 Banerjee R (2003) Chem Rev 103:2083–2094 Brown KL (2005) Chem Rev 105:2075–2149 Randaccio L, Geremia S, Nardin G, Wuerges J (2006) J Coord Chem Rev 250:1332–1350 Randaccio L, Geremia S, Wuerges J (2007) J Organomet Chem 692:1198 Halpern J (1985) Science 227:869–875 Finke RG (1998) In: Kräutler B, Arigoni D, Golding BT (eds) Vitamin B12 and B12 proteins, chap 25. Wiley-VCH, Weinheim Chowdhury S, Banerjee R (2000) Biochemistry 39:7998–8006 Kumar M, Kozlowski PM (2009) J Phys Chem B 113:9050–9054 Kozlowski PM, Kamachi T, Kumar M, Nakayama T, Yoshizawa K (2010) J Phys Chem B 114:5928–5937 Lexa D, Savéant J-M (1983) Acc Chem Res 16:235–243 Birke RL, Huang Q, Spataru T, Gosser DK Jr (2006) J Am Chem Soc 128:1922–1936 Vass I, Styring S (1991) Biochemistry 30:830–839 Miller A-F (2008) Acc Chem Res 41:501–510 Blomberg MRA, Siegbahn PEM, Babcock GT (1998) J Am Chem Soc 120:8812–8824 Becke AD (1986) J Chem Phys 84:4524–4529 Perdew JP (1986) Phys Rev B 33:8822–8824 Jensen KP, Ryde U (2003) J Phys Chem A 107:7539–7545 Kuta J, Patchkovskii S, Zgierski MZ, Kozlowski PM (2006) J Comput Chem 27:1429–1437 Kozlowski PM, Kamachi T, Toraya T, Yoshizawa K (2007) Angew Chem Int Ed 46:980–983 Finke RG, Hay BP (1984) Inorg Chem 23:3041–3043 Hay BP, Finke RG (1986) J Am Chem Soc 108:4820–4829 Finke RG, Hay BP (1988) Polyhedron 7:1469–1481 Luo LB, Li G, Chen HL, Fu SW, Zhang SY (1998) J Chem Soc Dalton Trans 2103–2107 Kozlowski PM, Kuta J, Galezowski W (2007) J Phys Chem B 111:7638–7645 Galezowski W, Kuta J, Kozlowski PM (2008) J Phys Chem B 112:3177–3183 Brown KL, Peck-Siler S (1988) Inorg Chem 27:3548–3555 Sirovatka-Dorweiler J, Matthews RG, Finke RG (2002) Inorg Chem 41:6217–6224 Mancia F, Evans PR (1998) Structure 6:711–720 Gruber K, Reitzer R, Kratky C (2001) Angew Chem 113:3481–3484 Alfonso-Prieto M, Biarnés X, Kumar M, Rovira C, Kozlowski PM (2010) J Phys Chem B 114:12965–12971 Lexa D, Savéant J-M (1978) J Am Chem Soc 100:3220–3222 Kim M-H, Birke RL (1983) J Electroanal Chem 144:331–350 Spataru T, Birke RL (2006) J Electroanal Chem 593:74–86 Schosser SG, Hannak RB, Konrat R, Gruber K, Mikl C, Kratky C, Kräutler B (2005) Chem Eur J 11:81–93 Fukuoka M, Nakanishi Y, Hannak RB, Kräutler B, Toraya T (2005) FEBS J 272:4787–4796 Friendorf M, Kozlowski PM (2004) J Am Chem Soc 126:1928–1929 Buckel W, Golding BT, Kratky C (2006) Chem Eur J 272:352–362