Elucidation of Structure of Lipid A from the Marine Gram-Negative Bacterium Pseudoalteromonas haloplanktis ATCC 14393T

Russian Journal of Bioorganic Chemistry - Tập 30 - Trang 367-373 - 2004
I. N. Krasikova, N. V. Kapustina1, V. V. Isakov1, N. M. Gorshkova1, T. F. Solov'eva1
1Pacific Institute of Bioorganic Chemistry, Far Eastern Division, Russian Academy of Sciences, pr, Stoletiya Vladivostoka, Russia

Tóm tắt

The chemical structure of lipid A, from the marine γ-proteobacterium Pseudoalteromonas haloplanktis АТСС 14393Т, a main product of lipopolysaccharide hydrolysis (1% AcOH), was determined using chemical methods and NMR spectroscopy. The lipid A was shown to be β-1,6-glucosaminobiose 1,4′-diphosphate acylated with two (R)-3-hydroxyalkanoic acid residues at C3 and C3′ and amidated with one (R)-3-hydroxydodecanoyl and one (R)-3-dodecanoyloxydodecanoyl residue at N2 and N2′, respectively.

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