Development of an Integrated Thermocouple for the Accurate Sample Temperature Measurement During High Temperature Environmental Scanning Electron Microscopy (HT-ESEM) Experiments

Microscopy and Microanalysis - Tập 21 Số 2 - Trang 307-312 - 2015
Renaud Podor1, Damien Pailhon1, Johann Ravaux1, Henri‐Pierre Brau1
1Institut de Chimie Séparative de Marcoule, UMR 5257 CEA-CNRS-UM2-ENSCM, Site de Marcoule, Bat 426, BP 17171, F-30207 Bagnols sur Cèze Cedex, France

Tóm tắt

AbstractWe have developed two integrated thermocouple (TC) crucible systems that allow precise measurement of sample temperature when using a furnace associated with an environmental scanning electron microscope (ESEM). Sample temperatures measured with these systems are precise (±5°C) and reliable. The TC crucible systems allow working with solids and liquids (silicate melts or ionic liquids), independent of the gas composition and pressure. These sample holder designs will allow end users to perform experiments at high temperature in the ESEM chamber with high precision control of the sample temperature.

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Thông tin xuất bản

Microscopy and Microanalysis

Tập 21 Số 2

307-312

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