Changes in interfacial bonding energies in the chemical activation of GaAs surfaces

Journal of Electronic Materials - Tập 34 - Trang 1010-1015 - 2005
Ning Liu1, Thomas F. Kuech2
1Materials Science Program, University of Wisconsin-Madison, Madison
2Department of Chemical and Biological Engineering University of Wisconsin-Madison, USA

Tóm tắt

The bonding chemistry and the role of the additional HCl-based prebonding treatment when combined with ozone and oxygen plasma treatments on the GaAs/GaAs direct bonding were investigated using multiple internal transmission Fourier transform infrared spectroscopy (MIT-FTIR) and atomic force microscopy (AFM). The results showed that the additional HCl-based pretreatment led to an increased bonding strength and a qualitative reduction in the void density. The removal of the initial native oxide facilitates the diffusion of water to the GaAs wafer surface where it can react to form primarily Ga-based oxides, leading to a substantially increased bond strength compared to those without the removal of interfacial native oxide.

Tài liệu tham khảo

Q.-Y. Tong and U. Gösele, Semiconductor Wafer Bonding Science and Technology, (Pennington, NJ: The Electrical Society Series, 1999). Y. Okuno, and M. Tamura, Jpn. J. Appl. Phys. Part 2, 35, L1652 (1996). A. PloBl and G. Krauter, Mater. Sci. Eng. R25, 1–88 (1999). F. Shi, S. MacLaren, C. Su, K.Y. Cheng, and K.C. Hsieh, J. Appl. Phys. 93, 5750 (2003). T. Akatsu, A. PloBl, H. Stenzel, and U. Gösele, J. Appl. Phys. 86, 7146 (1999). G. Kräuter, T. Akatsu, S. Senz, A. Plossl, and U. Gösele, Appl. Phys. A 70, 13 (2000). T. Akatsu, A. PloBl, R. Scholz, H. Stenzel, and U. Gösele, J. Appl. Phys. 90, 3856 (2001). D.M. Hansen, C.E. Albaugh, P.D. Moran, and T.F. Kuech, J. Appl. Phys. 90, 5991 (2001). D. Feijoo, Y.J. Chabal, and S.B. Christman, Appl. Phys. Lett. 65, 2548 (1994). S.-I. Lai, H.-Y. Lin, and C.-T. Hu, Mater. Chem. Phys. 83, 265 (2004). A. Milekhin, M. Friedrich, K. Hiller, M. Wiemer, T. Gessner, and D.R.T. Zahn, J. Phys. Chem. B 18, 1392 (2000). K.T. Queeney, H. Fukidome, E.E. Chaban, and Y.J. Chabal, J. Phys. Chem. B 105, 3903 (2001). M.K. Weldon, V.E. Marsico, Y.J. Chabal, D.R. Hamann, S.B. Christman, and E.E. Chaban, Surface Sci. 368, 163 (1996). S.J. Yun, K.-Y. Ahn, K.-S. Yi, and A.-W. Kang, J. Electrochem. Soc. 139, 2326 (1992). A.V. Felde, K. Kern, G.S. Higashi, Y.J. Chabal, and S.B. Christman, Phys. Rev. B 42, 5240 (1990). C.C. Bahr, A.V. Felde, and M.J. Cardillo, J. Electron. Spectrosc. Related Phenomena 54/55, 1075 (1990). J. Schneider, B. Dischler, H. Seelewind, and P.M. Mooney, Appl. Phys. Lett. 54, 1989 (1989). Z. Song, S. Shogen, M. Kawasaki, and I. Suemune, J. Vac. Sci. Technol. B 13, 77 (1995). C.T. Lenczycki and V.A. Burrows, Thin Solid Films 193/194, 610 (1990).