[Mo₄(μ₃‐S)₄(μ‐S₂CNEt₂)₂(S₂CNEt₂)₄], a Compound Containing a Cubane‐Like Mo₄S₄ Cluster

10.1073/pnas.69.9.2437

10.1007/BFb0111303

10.1021/ja00398a009

10.1021/ic00159a006

Bandy J. A., J. Chem. Soc. Chem. Commun, 1983, 1395

10.1002/ange.19830950720

10.1002/anie.198305491

10.1016/S0020-1693(00)80108-5

Procedurefor4: A solution of 2 g Mo2(S2CNEt2)6in 100 mL toluene is refluxed for 20 h. The reaction mixture is then cooled to 333–343 K and after about 50% of the solvent was evaporated under reduced pressure black crystals were obtained by filtration. Yield 25–35%.

Further details of the crystal structure investigation can be obtained from the Fachinformationszentrum Energie Physik Mathematik D‐7514 Eggenstein‐Leopoldshafen 2 by quoting the depository number CSD 50819 the names of the authors and the journal citation.