Use of monolithic supports for fast analysis of drugs and metabolites in plasma by direct injection

Springer Science and Business Media LLC - Tập 57 - Trang 569-575 - 2003
S. Souverain1, S. Rudaz1, J. -L. Veuthey1
1Laboratory of Analytical Pharmaceutical Chemistry, School of Pharmacy, University of Geneva, Geneva 4, Switzerland

Tóm tắt

Commercial monolithic columns were evcluated as extraction supports for the analysis of various drugs and their metabolites from plasma. For this purpose, a precolumn packed with a monolithic phase was used as extraction and enrichment support and integrated in a column-switching system for the direct and simultaneous analysis of fluoxetine and norfluoxetine, methadone and EDDP, flunitrazepam and norflunitrazepom in humon plasma. In this configuration, plasma samples were directly injected onto a Chromolith Flash precolumn (25×4.6 mm I.D.) coupled to a microbore analytical column packed with a conventional reversed-phase malerial. Detection was by an electrospray-ionization mass spectrometer (ESl-MS). Total analysis time, including extraction and separation of the six analytes, was <10 min. For all the investigated compounds, the limits of quantitation (LOQ) were estimated in the ng.mL1 range for an injection volume of 50 μL. The method was also applied to a real clinical case to demonstrate its applicability.

Tài liệu tham khảo

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