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Of interest in this connection is a recent work by Buhro et al. describing the synthesis of titanium and nickel aluminides from the metal chlorides and lithium aluminium hydride in refluxing mesitylene and subsequent heating of the precipitates in the solid state at 550°C: J.A. Haber, J.L. Crane, W.E. Buhro, C.A. Frey, S.M.L. Sastry, J.J. Balbach and M.S. Conradi, Adv. Mater., 8 (1996) 163.