Synthesis, crystal structures and properties of the bis-(trimetaphosphimato)-metallates Na4{Co[(PO2NH)3]2}·12H2O and Na4{Ni[(PO2NH)3]2}·12H2O

Solid State Sciences - Tập 6 - Trang 953-965 - 2004
Sascha Correll1, Norbert Stock1, Wolfgang Schnick1
1Department Chemie und Biochemie, Lehrstuhl für Anorganische Festkörperchemie, Ludwig-Maximilians-Universität München, Butenandtstraße 5-13 (D), 81377 München, Germany

Tài liệu tham khảo

Durif, 1995 Stokes, 1895, Ber. Dtsch. Chem. Ges., 28, 437, 10.1002/cber.189502801106 Marchand, 2000, Adv. Inorg. Chem., 50, 193, 10.1016/S0898-8838(00)50005-1 Correll, 2000, Z. Anorg. Allg. Chem., 626, 2347, 10.1002/1521-3749(200011)626:11<2347::AID-ZAAC2347>3.0.CO;2-W Stock, 1999, Z. Anorg. Allg. Chem., 625, 555, 10.1002/(SICI)1521-3749(199904)625:4<555::AID-ZAAC555>3.0.CO;2-R Rozanov, 1981, Zh. Neorg. Khim., 26, 668 Olthof, 1965, Acta Crystallogr., 19, 596, 10.1107/S0365110X65003948 Herrendorf, 1993 Sheldrick, 1997 Determined positions of atoms only represent local maxima of the electron density function. In case of light elements (e.g., hydrogen) these maxima of electron density do not have to agree exactly with the real positions of the atoms. Distances between hydrogen atoms and atoms which they are linked to were found to be too short. For this reason values of observed hydrogen bonds have been corrected by the program PARST97 from M. Nardelli, University of Parma, Italy, 1997 Stock, 1997, Z. Naturforsch., 52b, 251, 10.1515/znb-1997-0219 Stock, 1998, Eur. J. Inorg. Chem., 4, 469, 10.1002/(SICI)1099-0682(199804)1998:4<469::AID-EJIC469>3.0.CO;2-Q Sokol, 1974, Izv. Akad. Nauk SSSR, Ser. Khim., 2, 485 S. Correll, W. Schnick, unpublished Olbertz, 1993, Z. Kristallogr., 208, 374, 10.1524/zkri.1993.208.Part-2.374 Olbertz, 1998, Z. Kristallogr., 213, 241 Olbertz, 1995, Acta Crystallogr. C, 51, 1047, 10.1107/S0108270194012680 Shannon, 1969, Acta Crystallogr. B, 25, 925, 10.1107/S0567740869003220 Shannon, 1976, Acta Crystallogr. A, 32, 751, 10.1107/S0567739476001551