Synthesis, crystal structure and magnetic properties of one-dimensional cyano-bridged bimetallic complex of [Mn(Me2-bipy)2]3[W(CN)8]2·9H2O

Inorganic Chemistry Communications - Tập 12 - Trang 1179-1181 - 2009
Zhao-Xi Wang1,2, Bao-Lin Liu2, Jun Wang2, You Song2
1Department of Chemistry, College of Science, Shanghai University, Shanghai 200444, PR China
2State Key Laboratory of Coordination Chemistry, Nanjing National Laboratory of Microstructures, School of Chemistry and Chemical Engineering, Nanjing University, Nanjing 210093, PR China

Tài liệu tham khảo

Gatteschi, 2003, Angew. Chem., Int. Ed., 42, 268, 10.1002/anie.200390099 Glauber, 1963, J. Math. Phys., 4, 294, 10.1063/1.1703954 Caneschi, 2001, Angew. Chem., Int. Ed., 40, 1760, 10.1002/1521-3773(20010504)40:9<1760::AID-ANIE17600>3.0.CO;2-U Wang, 2004, J. Am. Chem. Soc., 126, 8900, 10.1021/ja0483995 Kurmoo, 2009, Chem. Soc. Rev., 38, 1353, 10.1039/b804757j Sieklucka, 2005, Coord. Chem. Rev., 249, 2203, 10.1016/j.ccr.2005.02.024 Zhong, 2000, J. Am. Chem. Soc., 122, 2952, 10.1021/ja992622u Podgajny, 2002, Chem. Commun., 1138, 10.1039/b202810g Song, 2003, Inorg. Chem., 42, 1848, 10.1021/ic025959x Przychodzeń, 2004, Inorg. Chem., 43, 2967, 10.1021/ic035464n Ikeda, 2005, Dalton Trans., 2120, 10.1039/b503426d Withers, 2006, Inorg. Chem., 45, 4307, 10.1021/ic0515251 Wang, 2006, Angew. Chem., Int. Ed., 45, 3287, 10.1002/anie.200600455 Ohkoshi, 2007, J. Am. Chem. Soc., 129, 3084, 10.1021/ja069353+ Wang, 2008, Dalton Trans., 2103, 10.1039/b803273b Pinkowicz, 2008, Inorg. Chem., 47, 9745, 10.1021/ic801248f Kosaka, 2009, Inorg. Chem., 48, 4604, 10.1021/ic9001576 Chelebaeva, 2009, Inorg. Chem., 48, 5983, 10.1021/ic900378d Stawski, 2009, Polyhedron, 28, 473, 10.1016/j.poly.2008.11.036 Zhang, 2009, Cryst. Growth Des., 9, 2050, 10.1021/cg900062y Song, 2005, J. Am. Chem. Soc., 127, 3708, 10.1021/ja042334k Lim, 2006, Angew. Chem., Int. Ed., 45, 7424, 10.1002/anie.200601759 Li, 2002, J. Chem. Soc., Dalton Trans., 2805, 10.1039/b205197b Li, 2003, Inorg. Chem., 42, 6123, 10.1021/ic034539k Withers, 2007, Polyhedron, 26, 2353, 10.1016/j.poly.2007.01.049 Yoo, 2009, Inorg. Chem., 48, 5617, 10.1021/ic900879d Crystal data for 1: C88H90Mn3N28O9W2, M=2215.39, monoclinic, space group C2/c, a=22.372(4)Å, b=16.468(3)Å, c=26.648(4)Å, β=90.112(3)°, V=9818(3)Å3, Z=4, Dc=1.500gcm3, F(000)=4436, μ(Mo Kα)=2.777mm−1, R1=0.0532, wR2=0.1119 for 8884 unique reflections and 593 parameters, S=1.027. Crystallographic data were collected using a Bruker SMART CCD diffractometer operating at room temperature. Intensities were collected with graphite monochromatized Mo Kα radiation (λ=0.71073Å), using the phi and omega scan technique. Data reduction was made with the Bruker SAINT package. Absorption correction was performed using the SADABS program. The structure was solved by direct methods and refined on F2 by full-matrix least-squares using SHELXL-2000 with anisotropic displacement parameters for all non-hydrogen atoms. H atoms were introduced in calculations using the riding model. All computations were carried out using the SHELXTL-2000 program package [28]. Bruker, SMART, SAINT, SADABS and SHELXTL, Bruker AXS Inc., Madison, WI, USA, 2000. Podgajny, 2002, Inorg. Chem., 41, 1323, 10.1021/ic010679n Wang, 2007, Inorg. Chem., 46, 10990, 10.1021/ic070195c Zhao, 2007, Chem. Eur. J., 13, 6573, 10.1002/chem.200700298 Zhong, 2000, Inorg. Chem., 39, 5095, 10.1021/ic0005994 Ruiz, 2005, Angew. Chem., Int. Ed., 44, 2711, 10.1002/anie.200500129 Borrás-Almenar, 1999, Inorg. Chem., 38, 6081, 10.1021/ic990915i Borrás-Almenar, 2001, J. Comput. Chem., 22, 985, 10.1002/jcc.1059