Synthesis and Crystal Structures of N-Aryl-N-methylaminocyclohexanols

Springer Science and Business Media LLC - Tập 43 - Trang 646-654 - 2013
Alexander J. Cresswell1, Stephen G. Davies1, David S. Hewings1, Wataru Kurosawa1, James A. Lee1, Melloney J. Morris2, Paul M. Roberts1, Amber L. Thompson1, James E. Thomson1
1Chemistry Research Laboratory, Department of Chemistry, University of Oxford, Oxford, UK
2Syngenta Jealott′s Hill International Research Centre, Berkshire, UK

Tóm tắt

N-Aryl-N-methylaminocyclohexanols 10–12 were synthesised and their crystal structures were studied by X-ray diffraction. Compound 10 crystallizes in the monoclinic space group Cc with cell parameters of a = 13.7366(2) Å, b = 13.7234(2) Å, c = 26.9057(5) Å, β = 93.0900(5)°, V = 5064.70(14) Å3 and Z = 16. Compound 11 crystallizes in the trigonal space group $$P\bar{3}$$ with cell parameters of a = b = 25.4429(4) Å, c = 9.6417(2) Å, V = 5405.27(16) Å3 and Z = 18. Compound 12 crystallizes in the monoclinic space group P21/n with cell parameters of a = 9.9511(2) Å, b = 11.5777(2) Å, c = 20.5968(4) Å, β = 95.5037(9)°, V = 2362.04(8) Å3 and Z = 8. All three structures were characterised by arrays of hydrogen bonding interactions and these crystallographic studies revealed conformations of 10–12 which gave valuable information into the mechanism of the reaction during their formation. Crystals of (RS,RS,RS)-3-[N-methyl-N-(4'-methoxyphenyl)amino]cyclohexane-1,2-diol, (RS,RS,RS)-3-(N-methyl-N-phenylamino)cyclohexane-1,2-diol and (RS,RS,RS)-2-fluoro-6-(N-methyl-N-phenylamino)cyclohexan-1-ol were synthesised and their structures were studied by X-ray diffraction. .

Tài liệu tham khảo

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