Solid-phase microextraction coatings based on anodic and cathodic plasma electrolytic deposition on titanium wire for determination of nerolidol in aqueous samples
Tóm tắt
Novel solid-phase microextraction coatings were prepared using cathodic and anodic plasma electrolytic deposition and used to measure the content of nerolidol in water and water distillate of bitter orange blossoms with GC-FID. The morphology of the prepared coatings was examined by field emission scanning electron microscopy. Effective parameters in the extraction and desorption were investigated. The optimal conditions include microextraction of 50 mL of an aqueous solution containing 35% (w/v) NaCl at 45 °C for 45 min using anodic coating, followed by desorption using 50 μL hexane in an ultrasonic bath for 5 min. The developed method has a linear dynamic range of 1–1000 ng mL−1 (R2 = 0.9980). The limit of detection (S/N = 3) and the limit of quantification (S/N = 10) of the developed method were 0.3 and 1 ng mL−1, respectively. The intra-, inter-day, and fiber-to-fiber relative standard deviations were 8–16, 9.2–16.7 and 10.1–13.0%, respectively. The concentration of the water distillate of bitter orange blossom was measured as 250 ng mL−1. The prepared adsorbent can be used many times due to its good mechanical stability. The developed method was used for the determination of nerolidol, as a product quality indicator, in the water distillate of bitter orange blossom. The developed method is simple, convenient, sensitive and with acceptable reproducibility that can be used for the microextraction of volatile organic compounds in various aqueous and food matrices.
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