Shaped optimal control pulses for increased excitation bandwidth in EPR

Journal of Magnetic Resonance - Tập 218 - Trang 49-58 - 2012
Philipp E. Spindler1, Yun Zhang2, Burkhard Endeward1, Naum Gershernzon3, Thomas E. Skinner3, Steffen J. Glaser2, Thomas F. Prisner1
1Institut für Physikalische und Theoretische Chemie , Goethe-Universität Frankfurt , Max-von-Laue-Straße 7 , 60438 Frankfurt am Main , Germany.
2Department of Chemistry, Technische Universität München, Lichtenbergstr. 4, 85747 Garching, Germany
3Physics Department, Wright State University, Dayton, OH 45735, USA

Tóm tắt

Từ khóa


Tài liệu tham khảo

Ernst, 1966, Application of Fourier transform spectroscopy to magnetic resonance, Rev. Sci. Instrum., 37, 93, 10.1063/1.1719961

Hu, 1974, Theory of spectral diffusion using an uncorrelated-sudden-jump model, Phys. Rev. B, 9, 1, 10.1103/PhysRevB.9.1

Klauder, 1962, Spectral diffusion decay in spin resonance experiments, Phys. Rev., 125, 912, 10.1103/PhysRev.125.912

Salikov, 1996, A theoretical approach to the analysis of arbitrary pulses in magnetic resonance, Chem. Phys. Lett., 262, 17, 10.1016/0009-2614(96)01044-5

Baum, 1985, Broadband and adiabatic inversion of a two-level system by phase modulated pulses, Phys. Rev. A, 32, 3435, 10.1103/PhysRevA.32.3435

Levitt, 1986, Composite pulses, Prog. Nucl. Magn. Reson. Spectrosc., 18, 61, 10.1016/0079-6565(86)80005-X

Ernst, 1966, Nuclear magnetic double resonance with an incoherent radio-frequency field, J. Chem. Phys., 45, 3845, 10.1063/1.1727409

Ernst, 1970, Magnetic resonance with stochastic excitation, J. Magn. Reson., 3, 10

Kaiser, 1970, Coherent spectroscopy with noise signals, J. Magn. Reson., 28, 28

Blümich, 1983, Nonlinear noise analysis in nuclear magnetic resonance spectroscopy. 1D, 2D, and 3D spectra, J. Chem. Phys., 78, 1059, 10.1063/1.444889

Gezelter, 1990, Use of neural networks to design shaped radiofrequency pulses, J. Magn. Reson., 90, 397

Böhlen, 1969, Frequency-modulated “Chirp” pulses for broadband inversion recovery in magnetic resonance, J. Magn. Reson., 90, 183

Kupče, 1995, Adiabatic pulse for wideband inversion and broadband decoupling, J. Magn. Reson., 115, 273, 10.1006/jmra.1995.1179

O’Dell, 2008, QCPMG using adiabatic pulses for faster acquisition of ultra-wideline NMR spectra, Chem. Phys. Lett., 464, 97, 10.1016/j.cplett.2008.08.095

Bhattacharyya, 2007, Quadrupolar nuclear magnetic resonance spectroscopy in solids using frequency-swept echoing pulses, J. Chem. Phys., 127, 194503, 10.1063/1.2793783

Crepeau, 1989, Composite pulses in time domain ESR, J. Magn. Reson., 84, 184

Prisner, 1989, ESR with stochastic excitation, J. Magn. Reson., 84, 296

Fuhs, 2001, Fourier transform EPR at high-field/high-frequency (3.4T/95GHz) using broadband stochastic microwave excitation, J. Magn. Reson., 67, 10.1006/jmre.2000.2272

Cruickshank, 2009, A kilowatt pulsed 94GHz electron paramagnetic resonance spectrometer with high concentration, high sensitivity, high instantaneous bandwidth, and low deadtime, Rev. Sci. Instrum., 80, 10.1063/1.3239402

Pursley, 2003, Stochastic excitation and Hadamard correlation spectroscopy with bandwidth extension in RF FT-EPR, J. Magn. Reson., 162, 35, 10.1016/S1090-7807(03)00050-8

Devasahayam, 2004, Tailored sinc pulses for uniform excitation and artifact-free radio frequency time-domain EPR imaging, J. Magn. Reson., 168, 110, 10.1016/j.jmr.2004.01.016

Khaneja, 2005, Optimal control of coupled spin dynamics: design of NMR pulse sequences by gradient ascent algorithms, J. Magn. Reson., 172, 296, 10.1016/j.jmr.2004.11.004

Skinner, 2003, Application of optimal control theory to the design of broadband excitation pulses for high resolution NMR, J. Magn. Reson., 163, 8, 10.1016/S1090-7807(03)00153-8

N.C. Nielsen, C. Kehlet, S.J. Glaser, N. Khaneja, Optimal control methods in NMR spectroscopy, in: Encyclopedia of Magnetic Resonance, John Wiley & Sons, Ltd., 2007.

O’Dell, 2010, Optimized excitation pulses for the acquisition of static NMR powder patterns from half-integer quadrupolar nuclei, J. Magn. Reson., 203, 156, 10.1016/j.jmr.2009.12.016

Assèmat, 2010, Simultaneous time-optimal control of the inversion of two spin 1/2 particles, Phys. Rev. A, 82, 013415, 10.1103/PhysRevA.82.013415

Khaneja, 2003, Boundary of quantum evolution under decoherence, Proc. Natl. Acad. Sci. USA, 100, 13162, 10.1073/pnas.2134111100

Lapert, 2010, Singular extremals for the time-optimal control of dissipative spin 1/2 particles, Phys. Rev. Lett., 104, 083001, 10.1103/PhysRevLett.104.083001

Tosner, 2009, Optimal control in NMR spectroscopy: numerical implementation in SIMPSON, J. Magn. Reson., 197, 120, 10.1016/j.jmr.2008.11.020

P.d. Fouquières, S.G. Schirmer, S.J. Glaser, I. Kuprov, Second order gradient ascent pulse engineering, J. Magn. Reson., in press.

Kobzar, 2004, Exploring the limits of broadband excitation and inversion pulses, J. Magn. Reson., 170, 236, 10.1016/j.jmr.2004.06.017

Neves, 2006, Exploring the limits of polarization transfer efficiency in homonuclear three spin systems, J. Magn. Reson., 181, 126, 10.1016/j.jmr.2006.03.021

Braun, 2010, Cooperative pulses, J. Magn. Reson., 207, 114, 10.1016/j.jmr.2010.08.013

Gershenzon, 2007, Optimal control design of excitation pulses that accomodate relaxation, J. Magn. Reson., 188, 330, 10.1016/j.jmr.2007.08.007

Zhang, 2011, Time-optimal control of spin 1/2 particles in the presence of radiation damping and relaxation, J. Chem. Phys., 134, 054103, 10.1063/1.3543796

Skinner, 2004, Reducing the duration of broadband excitation pulses using optimal control with limited RF amplitude, J. Magn. Reson., 167, 68, 10.1016/j.jmr.2003.12.001

Skinner, 2011, Design and application of robust RF pulses for toroid cavity NMR spectroscopy, J. Magn. Reson., 209, 282, 10.1016/j.jmr.2011.01.026

Schweiger, 2001

Davis, 1981, Use of a microwave delay line to reduce dead time in electron spin echo envelope spectroscopy, Rev. Sci. Instrum., 52, 131, 10.1063/1.1136423

Rinard, 2002, 250MHz crossed-loop resonator for pulsed electron paramagnetic resonance, Concepts Magn. Reson., 15, 37, 10.1002/cmr.10016

Prisner, 1988, FT ESR study of photoinduced electron transfer, J. Am. Chem. Soc., 110, 1622, 10.1021/ja00213a045

Dinse, 1989, Photo-induced electron transfer reactions studied by Fourier-transform ESR, Bull. Magn. Reson., 11, 174

Prisner, 1992, FT-EPR at 140GHz, Isr. J. Chem., 32, 357, 10.1002/ijch.199200042

Prisner, 1994, Pulsed 95GHz high-field EPR heterodyne spectrometer with high spectral and time resolution, Appl. Magn. Reson., 7, 167, 10.1007/BF03162610

Hornak, 1986, Spectral rotation in pulsed ESR spectroscopy, J. Magn. Reson., 67, 501

Gorcester, 1986, Two-dimensional Fourier transform ESR spectroscopy, J. Chem. Phys., 85, 5375, 10.1063/1.451158

Gorcester, 1988, Two dimensional Fourier transform correlation spectroscopy, J. Chem. Phys., 88, 4678, 10.1063/1.453782

Saxena, 1996, Double quantum two dimensional Fourier transform electron spin resonance: distance measurements, Chem. Phys. Lett., 251, 102, 10.1016/0009-2614(96)00075-9

Borbat, 1999, Multiple-quantum ESR and distance measurements, Chem. Phys. Lett., 313, 145, 10.1016/S0009-2614(99)00972-0

Höfer, 1986, Hyperfine sublevel correlation (hyscore) spectroscopy: a 2D ESR investigation of the squaric acid radical, Chem. Phys. Lett., 132, 279, 10.1016/0009-2614(86)80124-5

Gemperle, 1991, Electron-spin-echo envelope modulation with improved modulation depth, Chem. Phys. Lett., 178, 565, 10.1016/0009-2614(91)87021-3

Schosseler, 1994, Pulsed ELDOR detected NMR, Chem. Phys. Lett., 224, 319, 10.1016/0009-2614(94)00548-6

Wacker, 1991, Fourier-transform EPR-detected NMR, Chem. Phys. Lett., 186, 27, 10.1016/0009-2614(91)80187-3

Maly, 2004, Relaxation filtered hyperfine (REFINE) spectroscopy: a novel tool for studying overlapping biological electron paramagnetic resonance signals applied to mitochondrial complex I, Biochemistry, 43, 3969, 10.1021/bi035865e

Kröhnke, 1980, Radikalkationensalze einfacher Arene – eine neue Familie “organischer Metalle”, Angew. Chem., 92, 941, 10.1002/ange.19800921119

Sachs, 1982, Electron spin relaxation of new organic conductors: fluroranthenyl radical cation salts, Chem. Phys. Lett., 89, 179, 10.1016/0009-2614(82)80037-7

Sogo, 1957, Free radical from perinaphthene, J. Chem. Phys., 26, 1343, 10.1063/1.1743526

Skinner, 2005, Tailoring the optimal control cost function to a desired output: application to minimizing phase errors in short broadband excitation pulses, J. Magn. Reson., 172, 17, 10.1016/j.jmr.2004.09.011

Rife, 1989, Transfer-function measurement with maximum-length sequences, J. Audio Eng. Soc., 37, 419

Gershenzon, 2008, Linear phase slope in pulse design: application to coherence transfer, J. Magn. Reson., 192, 235, 10.1016/j.jmr.2008.02.021

Luy, 2005, Construction of universal rotations from point to point transformations, J. Magn. Reson., 176, 179, 10.1016/j.jmr.2005.06.002

Skinner, 2010, Optimal control design of pulse shapes as analytic functions, J. Magn. Reson., 204, 248, 10.1016/j.jmr.2010.03.002

Tabuchi, 2010, Total compensation of pulse transients inside a resonator, J. Magn. Reson., 204, 327, 10.1016/j.jmr.2010.03.014

Motzoi, 2011, Coarse-grained optimal control methods for fast time-varying Hamiltonians, Phys. Rev. A, 84, 022307, 10.1103/PhysRevA.84.022307

Pannier, 2000, Dead-time free measurement of dipole–dipole interactions between electron spins, J. Magn. Reson., 142, 331, 10.1006/jmre.1999.1944