Sensitivity Improvement of Transverse Relaxation-Optimized Spectroscopy
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Tài liệu tham khảo
Goldman, 1984, Interference effects in the relaxation of a pair of unlike spin-1/2 nuclei, J. Magn. Reson., 60, 437
Shimizu, 1964, Theory of the dependence of nuclear magnetic relaxation on the absolute sign of spin–spin coupling constant, J. Chem. Phys., 40, 3357, 10.1063/1.1725007
Guéron, 1983, Proton nuclear magnetic relaxation of15, J. Am. Chem. Soc., 105, 7262
Griffey, 1987, Proton-detected heteronuclear edited and correlated nuclear magnetic resonance and nuclear Overhauser effect in solution, Q. Rev. Biophys., 19, 51, 10.1017/S0033583500004029
Cavanagh, 1990, Sensitivity improvement in isotropic mixing (TOCSY) experiments, J. Magn. Reson., 88, 72
Rance, 1994, Sensitivity improvement in multi-dimensional NMR spectroscopy, Bull. Magn. Reson., 16, 54
Palmer, 1991, Sensitivity improvement in proton-detected two-dimensional heteronuclear correlation NMR spectroscopy, J. Magn. Reson., 93, 151
Palmer, 1992, Sensitivity improvement in three-dimensional heteronuclear correlation NMR spectroscopy, J. Magn. Reson., 96, 416
Skelton, 1993, Practical aspects of two-dimensional proton-detected15, J. Magn. Reson. B, 102, 253, 10.1006/jmrb.1993.1095
Kay, 1992, Pure absorption gradient enhanced heteronuclear single quantum correlation spectroscopy with improved sensitivity, J. Am. Chem. Soc., 114, 10663, 10.1021/ja00052a088
Akke, 1994, Three-dimensional heteronuclear NMR spectroscopy with simultaneous isotope filtration, quadrature detection and sensitivity enhancement usingz, J. Magn. Reson. B, 104, 298, 10.1006/jmrb.1994.1090
Schleucher, 1994, A general enhancement scheme in heteronuclear multidimensional NMR employing pulsed field gradients, J. Biomol. NMR, 4, 301, 10.1007/BF00175254
Sørensen, 1983, Product operator formalism for the description of NMR pulse experiments, Prog. NMR Spectrosc., 16, 163, 10.1016/0079-6565(84)80005-9
van de Ven, 1983, A simple formalism for the description of multiple-pulse experiments. Application to a weakly coupled two-spin (I12, J. Magn. Reson., 54, 512
Packer, 1983, The use of single-spin operator basis sets in the NMR spectroscopy of scalar-coupled spin systems, Mol. Phys., 50, 797, 10.1080/00268978300102691
Cavanagh, 1996
Abragam, 1961
Palmer, 1992, Suppression of the effects of cross-correlation between dipolar and anisotropic chemical shift relaxation mechanisms in the measurement of spin–spin relaxation rates, Mol. Phys., 75, 699, 10.1080/00268979200100511
Müller, 1979, Coherence transfer in the rotating frame. Application to heteronuclear cross-correlation spectroscopy, Mol. Phys., 38, 963, 10.1080/00268977900102161
Grzesiek, 1993, The importance of not saturating H2, J. Am. Chem. Soc., 115, 12593, 10.1021/ja00079a052
Stonehouse, 1994, Minimizing sensitivity losses in gradient-selected151, J. Magn. Reson. A, 107, 178, 10.1006/jmra.1994.1066
Kay, 1994, Enhanced-sensitivity triple-resonance spectroscopy with minimal H2, J. Magn. Reson. A, 109, 129, 10.1006/jmra.1994.1145
Mori, 1995, Improved sensitivity of HSQC spectra of exchanging protons at short interscan delays using a new fast HSQC (FHSQC) detection scheme that avoids water saturation, J. Magn. Reson. B, 108, 94, 10.1006/jmrb.1995.1109
Sklenář, 1993, Gradient-tailored water suppression for115, J. Magn. Reson. A, 102, 241
Liu, 1998, Improved WATERGATE pulse sequences for solvent suppression in NMR spectroscopy, J. Magn. Reson., 132, 125, 10.1006/jmre.1998.1405
Piotto, 1992, Gradient-tailored excitation for single-quantum NMR spectroscopy of aqueous solutions, J. Biomol. NMR, 2, 661, 10.1007/BF02192855
Bax, 1991, Removal ofF1, J. Magn. Reson., 91, 174
Sambrook, 1989
Komives, 1991, Electrophilic catalysis in triosephosphate isomerase: The role of histidine-95, Biochemistry, 30, 3011, 10.1021/bi00226a005
Putman, 1972, Specificity and kinetics of triose phosphate isomerase from chicken muscle, Biochem. J., 129, 301, 10.1042/bj1290301
Williams, 1995, Dynamics of the flexible loop of triosephosphate isomerase: The loop motion is not ligand gated, Biochemistry, 34, 8309, 10.1021/bi00026a012