Reactive Dye Adsorption from Aqueous Solution on HPEI-Modified Fe3O4 Nanoparticle as a Superadsorbent: Characterization, Modeling, and Optimization

Journal of Polymers and the Environment - Tập 26 - Trang 3470-3483 - 2018
Arash Dalvand1,2, Mehdi Khoobi3,4, Ramin Nabizadeh2, Mohammad Reza Ganjali5,6, Elham Gholibegloo7, Amir Hossein Mahvi8,9,10
1Environmental Science and Technology Research Center, Department of Environmental Health Engineering, School of Public Health, Shahid Sadoughi University of Medical Sciences, Yazd, Iran
2Department of Environmental Health Engineering, School of Public Health, Tehran University of Medical Sciences, Tehran, Iran
3Medical Biomaterials Research Center, Tehran University of Medical Sciences, Tehran, Iran
4Department of Medicinal Chemistry, Faculty of Pharmacy and Pharmaceutical Sciences Research Center, Tehran University of Medical Sciences, Tehran, Iran
5Center of Excellence in Electrochemistry, Faculty of Chemistry, University of Tehran, Tehran, Iran
6Biosensor Research Center, Endocrinology and Metabolism Molecular-Cellular Sciences Institute, Tehran University of Medical Sciences, Tehran, Iran
7Depatment of Organic Chemistry, University of Zanjan, Zanjan, Iran
8Center for Water Quality Research, Institute for Environmental Research, Tehran University of Medical Sciences, Tehran, Iran
9Center for Solid Waste Research, Institute for Environmental Research, Tehran University of Medical Sciences, Tehran, Iran
10National Institute of Health Research, Tehran University of Medical Sciences, Tehran, Iran

Tóm tắt

In this work, the optimum condition for the adsorption of Reactive Blue 19 dye onto Fe3O4 functionalized with hyperbranched polyethylenimine (Fe@HPEI) was determined using response surface methodology. The properties of synthesized magnetic Fe@HPEI nanoparticles were ascertained using FTIR, SEM, TEM, VSM and zeta potential measurement. The experimental adsorption data indicating the positive effect of adsorbent dose and contact time, and the negative effect of pH, initial dye concentration and ionic strength on dye adsorption. At optimal condition; pH 3.4, contact time 25 min, adsorbent dose 0.4 g/L and initial dye concentration 113 mg/L, Fe@HPEI nanoparticles removed dye up to 99.27%. The maximum experimental dye adsorption was near to the predicted value of 100%, which confirmed the reliability of the selected statistical model. The dye adsorption data were fitted well to Langmuir isotherm and pseudo-second-order kinetic, and the maximum adsorption capacity was 500 mg/g. Totally, Fe@HPEI as an effective superadsorbent can be repeatedly utilized for the adsorption of dye from the aqueous environment.

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