Preparation and characterization of cellulose nanocrystal extracted from Calotropis procera biomass

Bioresources and Bioprocessing - Tập 6 - Trang 1-8 - 2019
Kaili Song1,2,3, Xiaoji Zhu1,3, Weiming Zhu1,3, Xiaoyan Li4
1Engineering Research Center for Eco-Dyeing and Finishing of Textiles, College of Materials and Textiles, Zhejiang Sci-Tech University, Hangzhou, China
2Key Laboratory of Clean Dyeing and Finishing Technology of Zhejiang Province, Shaoxing University, Shaoxing, China
3Key Laboratory of Advanced Textile Materials and Manufacturing Technology, Ministry of Education, Zhejiang Sci-Tech University, Hangzhou, China
4College of Textile and Garment, Hebei University of Science and Technology, Hebei, China

Tóm tắt

Calotropis procera fiber (CPF) is the fruit fiber of C. procera and belongs to a typical cellulosic fiber. In this study, Calotropis procera fiber (CPF) was first purified in the pretreatment process including delignification and bleaching before the isolation of cellulose nanocrystal. Chemical composition of Calotropis procera fiber was determined according to TAPPI standard method. It was composed of 64.0 wt% cellulose, 19.5 wt% hemicelluloses, and 9.7 wt% of lignin. The morphology of the Calotropis procera fiber and fiber after each pretreatment process was also investigated. Cellulose nanocrystal was extracted by classical sulfuric acid hydrolysis of the pretreated Calotropis procera fiber. TEM and SEM were used to analyze the morphologies of the obtained CNC. The crystallinity, thermal stability and suspension stability of the CNC were also investigated. The interesting results proved that this under-utilized biomass could be exploited as a new source of cellulose raw material for the production of cellulose nanocrystal.

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Bioresources and Bioprocessing

Tập 6

1-8

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