Preliminary validation of high performance liquid chromatography method for detection of methyl-testosterone residue in carp muscle

Jie Jiang1, Hong Lin1, Xiaoting Fu1, Mingming Li
1College of Food Science and Engineering, Ocean University of China, Qingdao, P.R. China

Tóm tắt

Từ khóa


Tài liệu tham khảo

Daeseleire, E., R. Vandeputte, and V. C. Peteghem, 1998. Validation of multi-residue methods for the detection of anabolic steroids by GC-MS in muscle tissues and urine samples from cattle. Analyst, 123: 2 595–2 598.

Gao, J., Y. Li, W. Chang, and Y. Ci, 2000. Phase seperation immunoassay of methyl testosterone. Chinese Journal of Analytical Chemistry, 28(1): 1–5.

Grumbach, M.M., and J.R. Ducharme, 1960. The effects of androgens on fetal sexual development: androgen-induced female pseudohermaphroditism. Fertility and Sterility, 11: 157–180.

Hartleb, M., and A. Nowak, 1990. Severe jaundice with destructive cholangitis after administration of methyltestosterone. American Journal of Gastroenterology, 85: 766–767.

Hartmann, S., and H. Steinhart, 1997. Simultaneous determination of anabolic and catabolic steroid hormones in meat by gas chromatography-mass spectrometry. Journal of Chromatography B, 704: 105–117.

Lucey, M. R., 1987. Severe cholestasis associated with methyltestosterone: a case report. American Journal of Gastroenterology, 82: 461–462.

Marchand, P., B. le Bizec, C. Gade, F. Monteau, and F. Andre, 2000. Ultra trace detection of a wide range of anabolic steroids in meat by gas chromatography coupled to mass spectrometry. Journal of Chromatography A, 867: 219–233.

Poucke, V. C, and V. C. Peteghem, 2002. Development and validation of a multi-analyte method for the detection of anabolic steroids in bovine urine with liquid chromatography-tandem mass spectrometry. Journal of Chromatography B, 772: 211–217.

Schardein, J. L., 1980. Congenital abnormalities and hormones during pregnancy: a clinical review. Teratology, 22: 251–270.

Schmidt, G., and H. Steinhart, 2002. Impact of extraction solvents on steroid contents determined in beef. Food Chemistry, 76: 83–88.

Westaby, D., S.J. Ogle, F.J. Paradinas, J. B. Randell, and I.M. Murray-Lyon, 1977. Liver damage from long-term methyltestosterone. Lancet, 2: 261–263.