Pd-based nanocatalysts for oxygen reduction reaction: Preparation, performance, and in-situ characterization

Cano, 2018, Batteries and fuel cells for emerging electric vehicle markets, Nat. Energy, 3, 279, 10.1038/s41560-018-0108-1 Debe, 2012, Electrocatalyst approaches and challenges for automotive fuel cells, Nature, 486, 43, 10.1038/nature11115 Walter, 2010, Solar water splitting cells, Chem. Rev., 110, 6446, 10.1021/cr1002326 Youngblood, 2009, Visible light water splitting using dye-sensitized oxide semiconductors, Acc. Chem. Res., 42, 1966, 10.1021/ar9002398 Cheng, 2012, Metal-air batteries: from oxygen reduction electrochemistry to cathode catalysts, Chem. Soc. Rev., 41, 2172, 10.1039/c1cs15228a Lee, 2011, Metal-air batteries with high energy density: Li-air versus Zn-air, Adv. Energy Mater., 1, 34, 10.1002/aenm.201000010 Chen, 2020, Recent advances in carbon-based electrocatalysts for oxygen reduction reaction, Chin. Chem. Lett., 31, 626, 10.1016/j.cclet.2019.08.008 Xiao, 2021, Recent advances in electrocatalysts for proton exchange membrane fuel cells and alkaline membrane fuel cells, Adv. Mater., 33, 2006292, 10.1002/adma.202006292 Jiao, 2015, Design of electrocatalysts for oxygen- and hydrogen-involving energy conversion reactions, Chem. Soc. Rev., 44, 2060, 10.1039/C4CS00470A Ma, 2020, Enhancing oxygen reduction activity of Pt-based electrocatalysts: from theoretical mechanisms to practical methods, Angew. Chem. Int. Ed., 59, 18334, 10.1002/anie.202003654 Yu, 2011, Oxygen reduction reaction mechanism on nitrogen-doped graphene: a density functional theory study, J. Catal., 282, 183, 10.1016/j.jcat.2011.06.015 Norskov, 2004, Origin of the overpotential for oxygen reduction at a fuel-cell cathode, J. Phys. Chem. B, 108, 17886, 10.1021/jp047349j Antolini, 2009, Palladium in fuel cell catalysis, Energy Environ. Sci., 2, 915, 10.1039/b820837a Xue, 2017, Polyethyleneimine modified AuPd@PdAu alloy nanocrystals as advanced electrocatalysts towards the oxygen reduction reaction, J. Energy Chem., 26, 1153, 10.1016/j.jechem.2017.06.007 Wang, 2016, Size-dependent disorder-order transformation in the synthesis of monodisperse intermetallic PdCu nanocatalysts, ACS Nano, 10, 6345, 10.1021/acsnano.6b02669 Sahoo, 2020, Boosting bifunctional oxygen reduction and methanol oxidation electrocatalytic activity with 2D superlattice-forming Pd nanocubes generated by precise acid etching, ACS Appl. Nano Mater., 3, 8117, 10.1021/acsanm.0c01543 Sahoo, 2022, Ultrathin twisty PdNi alloy nanowires as highly active ORR electrocatalysts exhibiting morphology-induced durability over 200 K cycles, Nano Lett., 22, 246, 10.1021/acs.nanolett.1c03704 Liu, 2020, Interlaced Pd–Ag nanowires rich in grain boundary defects for boosting oxygen reduction electrocatalysis, Nanoscale, 12, 5368, 10.1039/D0NR00046A Yu, 2021, Defect-rich porous palladium metallene for enhanced alkaline oxygen reduction electrocatalysis, Angew. Chem. Int. Ed., 60, 12027, 10.1002/anie.202101019 Luo, 2019, PdMo bimetallene for oxygen reduction catalysis, Nature, 574, 81, 10.1038/s41586-019-1603-7 Zhang, 2020, Atomically deviated Pd–Te nanoplates boost methanol-tolerant fuel cells, Sci. Adv., 6, eaba9731, 10.1126/sciadv.aba9731 Guo, 2021, Template-directed rapid synthesis of Pd-based ultrathin porous intermetallic nanosheets for efficient oxygen reduction, Angew. Chem. Int. Ed., 60, 10942, 10.1002/anie.202100307 Tang, 2019, Fully tensile strained Pd3Pb/Pd tetragonal nanosheets enhance oxygen reduction catalysis, Nano Lett., 19, 1336, 10.1021/acs.nanolett.8b04921 Jiang, 2020, Freestanding single-atom-layer Pd-based catalysts: oriented splitting of energy bands for unique stability and activity, Chem, 6, 431, 10.1016/j.chempr.2019.11.003 Tan, 2015, Wet-chemical synthesis and applications of non-layer structured two-dimensional nanomaterials, Nat. Commun., 6, 7873, 10.1038/ncomms8873 Zhou, 2014, Pd particle size effects on oxygen electrochemical reduction, Int. J. Hydrogen Energy, 39, 6433, 10.1016/j.ijhydene.2014.01.197 Shi, 2014, Oleylamine-functionalized palladium nanoparticles with enhanced electrocatalytic activity for the oxygen reduction reaction, J. Power Sources, 246, 356, 10.1016/j.jpowsour.2013.07.099 Fu, 2013, Polyallylamine functionalized palladium icosahedra: one-pot water-based synthesis and their superior electrocatalytic activity and ethanol tolerant ability in alkaline media, Langmuir, 29, 4413, 10.1021/la304881m Xiong, 2007, Shape-controlled synthesis of metal nanostructures: the case of palladium, Adv. Mater., 19, 3385, 10.1002/adma.200701301 Kabiraz, 2021, Shape and hydriding effects of palladium nanocatalyst toward oxygen electroreduction reaction, B. Korean Chem. Soc., 42, 802, 10.1002/bkcs.12183 Shao, 2011, Structural dependence of oxygen reduction reaction on palladium nanocrystals, Chem. Commun., 47, 6566, 10.1039/c1cc11004g Erikson, 2011, Enhanced electrocatalytic activity of cubic Pd nanoparticles towards the oxygen reduction reaction in acid media, Electrochem. Commun., 13, 734, 10.1016/j.elecom.2011.04.024 Huang, 2015, Truncated palladium nanocubes: synthesis and the effect of OH− concentration on their catalysis of the alkaline oxygen reduction reaction, Electrochim. Acta, 157, 78, 10.1016/j.electacta.2015.01.059 Erikson, 2016, Oxygen electroreduction on carbon-supported Pd nanocubes in acid solutions, Electrochim. Acta, 188, 301, 10.1016/j.electacta.2015.11.125 Luesi, 2016, Oxygen reduction reaction on carbon-supported palladium nanocubes in alkaline media, Electrochem. Commun., 64, 9, 10.1016/j.elecom.2015.12.016 Xiao, 2009, Activating Pd by morphology tailoring for oxygen reduction, J. Am. Chem. Soc., 131, 602, 10.1021/ja8063765 Zhang, 2012, Enhancing the catalytic and electrocatalytic properties of Pt-based catalysts by forming bimetallic nanocrystals with Pd, Chem. Soc. Rev., 41, 8035, 10.1039/c2cs35173k Yang, 2011, Platinum-based electrocatalysts with core-shell nanostructures, Angew. Chem. Int. Ed., 50, 2674, 10.1002/anie.201005868 Xie, 2014, Atomic layer-by-layer deposition of Pt on Pd nanocubes for catalysts with enhanced activity and durability toward oxygen reduction, Nano Lett., 14, 3570, 10.1021/nl501205j Cui, 2013, Compositional segregation in shaped Pt alloy nanoparticles and their structural behaviour during electrocatalysis, Nat. Mater., 12, 765, 10.1038/nmat3668 Bampos, 2017, Comparison of the activity of Pd–M (M: Ag, Co, Cu, Fe, Ni, Zn) bimetallic electrocatalysts for oxygen reduction reaction, Top. Catal., 60, 1260, 10.1007/s11244-017-0795-z Bampos, 2020, Oxygen reduction reaction activity of Pd-based bimetallic electrocatalysts in alkaline medium, Catal. Today, 355, 685, 10.1016/j.cattod.2019.06.010 Chen, 2016, Gold-catalyzed formation of core-shell gold-palladium nanoparticles with palladium shells up to three atomic layers, J. Mater. Chem., 4, 3813, 10.1039/C5TA10303G Shi, 2021, Ag–Pd core-shell electrocatalysts for ethanol oxidation and oxygen reduction reactions in alkaline medium, J. Phys. Mater., 4, 014002, 10.1088/2515-7639/abc733 Shao, 2013, Manipulating the oxygen reduction activity of platinum shells with shape-controlled palladium nanocrystal cores, Chem. Commun., 49, 9030, 10.1039/c3cc43276a Lv, 2014, A simple one-pot strategy to platinum-palladium@palladium core-shell nanostructures with high electrocatalytic activity, J. Power Sources, 265, 231, 10.1016/j.jpowsour.2014.04.108 Huang, 2020, A stable PdCu@Pd core-shell nanobranches with enhanced activity and methanol-tolerant for oxygen reduction reaction, Electrochim. Acta, 354, 136680, 10.1016/j.electacta.2020.136680 Wang, 2010, Pt-decorated PdCo@Pd/C core-shell nanoparticles with enhanced stability and electrocatalytic activity for the oxygen reduction reaction, J. Am. Chem. Soc., 132, 17664, 10.1021/ja107874u Jiang, 2016, Core/shell FePd/Pd catalyst with a superior activity to Pt in oxygen reduction reaction, Sci. Bull., 61, 1248, 10.1007/s11434-016-1125-8 Sun, 2015, Synthesis of Pd9Ru@Pt nanoparticles for oxygen reduction reaction in acidic electrolytes, J. Power Sources, 277, 116, 10.1016/j.jpowsour.2014.11.102 Wang, 2016, Tuning nanowires and nanotubes for efficient fuel-cell electrocatalysis, Adv. Mater., 28, 10117, 10.1002/adma.201601909 Li, 2018, Ultrathin metallic nanowire-based architectures as high-performing electrocatalysts, ACS Omega, 3, 3294, 10.1021/acsomega.8b00169 Chang, 2020, Strain-modulated platinum-palladium nanowires for oxygen reduction reaction, Nano Lett., 20, 2416, 10.1021/acs.nanolett.9b05123 Koenigsmann, 2012, Highly enhanced electrocatalytic oxygen reduction performance observed in bimetallic palladium-based nanowires prepared under ambient, surfactantless conditions, Nano Lett., 12, 2013, 10.1021/nl300033e Zhu, 2012, PdM (M = Pt, Au) bimetallic alloy nanowires with enhanced electrocatalytic activity for electro-oxidation of small molecules, Adv. Mater., 24, 2326, 10.1002/adma.201104951 Zhang, 2019, Defect engineering of palladium-tin nanowires enables efficient electrocatalysts for fuel cell reactions, Nano Lett., 19, 6894, 10.1021/acs.nanolett.9b02137 Duan, 2019, Facile one-pot aqueous fabrication of interconnected ultrathin PtPbPd nanowires as advanced electrocatalysts for ethanol oxidation and oxygen reduction reactions, Int. J. Hydrogen Energy, 44, 27455, 10.1016/j.ijhydene.2019.08.225 Jiang, 2020, Trimetallic Au@PdPb nanowires for oxygen reduction reaction, Nano Res., 13, 2691, 10.1007/s12274-020-2911-9 Liu, 2022, Trimetallic Au@PdPt porous core-shell structured nanowires for oxygen reduction electrocatalysis, Chem. Eng. J., 428, 131070, 10.1016/j.cej.2021.131070 Guo, 2020, Structure design reveals the role of Au for ORR catalytic performance optimization in PtCo-based catalysts, Adv. Funct. Mater., 30, 2001575, 10.1002/adfm.202001575 Lin, 2016, The structure-dependent enhancement of the oxygen reduction reaction performance of Co-based low Pt catalysts through Au addition, J. Mater. Chem., 4, 11023, 10.1039/C6TA04154J Zhang, 2020, Core-shell nanostructure-enhanced Raman spectroscopy for surface catalysis, Acc. Chem. Res., 53, 729, 10.1021/acs.accounts.9b00545 Chia, 2018, Characteristics and performance of two-dimensional materials for electrocatalysis, Nat. Catal., 1, 909, 10.1038/s41929-018-0181-7 Chen, 2018, Two-dimensional metal nanomaterials: synthesis, properties, and applications, Chem. Rev., 118, 6409, 10.1021/acs.chemrev.7b00727 Ma, 2018, Ultrathin two-dimensional metallic nanomaterials, Mater. Chem. Front., 2, 456, 10.1039/C7QM00548B Yang, 2016, Advances and challenges in chemistry of two-dimensional nanosheets, Nano Today, 11, 793, 10.1016/j.nantod.2016.10.004 Zhang, 2022, Highly wrinkled palladium nanosheets as advanced electrocatalysts for the oxygen reduction reaction in acidic medium, Chem. Eng. J., 431, 133237, 10.1016/j.cej.2021.133237 Wang, 2021, Palladium nanobelts with expanded lattice spacing for electrochemical oxygen reduction in alkaline media, ACS Appl. Nano Mater., 4, 2118, 10.1021/acsanm.0c03398 Yang, 2019, Facile synthesis of ultrathin Pt–Pd nanosheets for enhanced formic acid oxidation and oxygen reduction reaction, J. Mater. Chem., 7, 18846, 10.1039/C9TA03945G Xu, 2021, Recent progress of ultrathin 2D Pd-based nanomaterials for fuel cell electrocatalysis, Small, 17, 2005092, 10.1002/smll.202005092 Wang, 2015, 2D ultrathin core-shell Pd@Pt-monolayer nanosheets: defect-mediated thin film growth and enhanced oxygen reduction performance, Nanoscale, 7, 11934, 10.1039/C5NR02748A Tyo, 2015, Catalysis by clusters with precise numbers of atoms, Nat. Nanotechnol., 10, 577, 10.1038/nnano.2015.140 Liang, 2015, The power of single-atom catalysis, ChemCatChem, 7, 2559, 10.1002/cctc.201500363 Yang, 2013, Single-atom catalysts: a new frontier in heterogeneous catalysis, Acc. Chem. Res., 46, 1740, 10.1021/ar300361m Su, 2021, Single atom catalyst for electrocatalysis, Chin. Chem. Lett., 32, 2947, 10.1016/j.cclet.2021.03.082 Xiang, 2018, Palladium single atoms supported by interwoven carbon nanotube and manganese oxide nanowire networks for enhanced electrocatalysis, J. Mater. Chem., 6, 23366, 10.1039/C8TA09034C Kim, 2019, Palladium single-atom catalysts supported on C@C3N4 for electrochemical reactions, ChemElectroChem, 6, 4757, 10.1002/celc.201900772 Liu, 2020, Atomic dispersion and surface enrichment of palladium in nitrogen-doped porous carbon cages lead to high-performance electrocatalytic reduction of oxygen, ACS Appl. Mater. Interfaces, 12, 17641, 10.1021/acsami.0c03415 Xi, 2021, Highly active, selective, and stable Pd single-atom catalyst anchored on N-doped hollow carbon sphere for electrochemical H2O2 synthesis under acidic conditions, J. Catal., 393, 313, 10.1016/j.jcat.2020.11.020 Fu, 2020, A Ti3C2O2 supported single atom, trifunctional catalyst for electrochemical reactions, J. Mater. Chem., 8, 7801, 10.1039/D0TA01047B Guo, 2013, Tuning nanoparticle catalysis for the oxygen reduction reaction, Angew Chem. Int. Ed., 52, 8526, 10.1002/anie.201207186 Seh, 2017, Combining theory and experiment in electrocatalysis: insights into materials design, Science, 355, eaad4998, 10.1126/science.aad4998 Handoko, 2018, Understanding heterogeneous electrocatalytic carbon dioxide reduction through operando techniques, Nat. Catal., 1, 922, 10.1038/s41929-018-0182-6 Ze, 2021, Molecular insight of the critical role of Ni in Pt-based nanocatalysts for improving the oxygen reduction reaction probed using an in situ SERS borrowing strategy, J. Am. Chem. Soc., 143, 1318, 10.1021/jacs.0c12755 Wang, 2019, In situ spectroscopic insight into the origin of the enhanced performance of bimetallic nanocatalysts towards the oxygen reduction reaction (ORR), Angew Chem. Int. Ed., 58, 16062, 10.1002/anie.201908907 Chen, 2022, In situ studies of energy-related electrochemical reactions using Raman and X-ray absorption spectroscopy, Chin. J. Catal., 43, 33, 10.1016/S1872-2067(21)63874-3 Wu, 2015, Composition-structure-activity relationships for palladium-alloyed nanocatalysts in oxygen reduction reaction: an ex-situ/in-situ high energy X-ray diffraction study, ACS Catal., 5, 5317, 10.1021/acscatal.5b01608 Mondal, 2022, In situ mechanistic insights for the oxygen reduction reaction in chemically modulated ordered intermetallic catalyst promoting complete electron transfer, J. Am. Chem. Soc., 144, 11859, 10.1021/jacs.2c04541 Tian, 2007, Expanding generality of surface-enhanced Raman spectroscopy with borrowing SERS activity strategy, Chem. Commun., 3514, 10.1039/b616986d Nie, 1997, Probing single molecules and single nanoparticles by surface-enhanced Raman scattering, Science, 275, 1102, 10.1126/science.275.5303.1102 Zhang, 2020, Core-shell nanostructure-enhanced Raman spectroscopy for surface catalysis, Acc. Chem. Res., 53, 729, 10.1021/acs.accounts.9b00545 Sun, 2022, Exploring the effect of Pd on the oxygen reduction performance of Pt by in situ Raman spectroscopy, Anal. Chem., 94, 4779, 10.1021/acs.analchem.1c05566 Li, 2010, Shell-isolated nanoparticle-enhanced Raman spectroscopy, Nature, 464, 392, 10.1038/nature08907 Dong, 2019, In situ Raman spectroscopic evidence for oxygen reduction reaction intermediates at platinum single-crystal surfaces, Nat. Energy, 4, 60, 10.1038/s41560-018-0292-z Zhang, 2017, In situ dynamic tracking of heterogeneous nanocatalytic processes by shell-isolated nanoparticle-enhanced Raman spectroscopy, Nat. Commun., 8, 15447, 10.1038/ncomms15447 Chung, 2014, Electrocatalyst for the oxygen reduction reaction: from the nanoscale to the macroscale, J. Electrochem. Sci. Technol., 5, 65, 10.33961/JECST.2014.5.3.65 Guo, 2013, Tuning nanoparticle catalysis for the oxygen reduction reaction, Angew. Chem. Int. Ed., 52, 8526, 10.1002/anie.201207186 Li, 2022, Oxidative stability matters: a case study of palladium hydride nanosheets for alkaline fuel cells, J. Am. Chem. Soc., 144, 8106, 10.1021/jacs.2c00518 Shao, 2011, Palladium-based electrocatalysts for hydrogen oxidation and oxygen reduction reactions, J. Power Sources, 196, 2433, 10.1016/j.jpowsour.2010.10.093 Wells, 2009, Preparation, structure, and stability of Pt and Pd monolayer modified Pd and Pt electrocatalysts, Phys. Chem. Chem. Phys., 11, 5773, 10.1039/b823504j Tian, 2020, Advanced electrocatalysts for the oxygen reduction reaction in energy conversion technologies, Joule, 4, 45, 10.1016/j.joule.2019.12.014 Fan, 2021, Bridging the gap between highly active oxygen reduction reaction catalysts and effective catalyst layers for proton exchange membrane fuel cells, Nat. Energy, 6, 475, 10.1038/s41560-021-00824-7