Optical and Chromaticity Characteristics of Rare-Earth Element Complexes of Sulfochlorophenol and Sulfochlorophenol S

Journal of Analytical Chemistry - Tập 57 - Trang 110-117 - 2002
V. M. Ivanov1, N. V. Ermakova1
1Department of Chemistry, Moscow State University, Moscow, Russia

Tóm tắt

Optimal conditions of the complexation of Sulfochlorophenol and Sulfochlorophenol S with lanthanum, terbium, and erbium were found, and molar absorptivities of the complexes were calculated. Chromaticity characteristics of the complexes and molar coefficients of chromaticity functions were determined. It was demonstrated that the use of the most sensitive chromaticity functions provides an increase in the sensitivity of the determination of rare-earth elements of 1–2 orders of magnitude in comparison with conventional spectrophotometry. Dissociation constants of the reagents were determined using optical and chromaticity methods.

Tài liệu tham khảo

Nazarenko, V.A. and Antonovich, V.P., Zh. Anal. Khim., 1969, vol. 24, no. 7, p. 1008. Savvin, S.B., Pisarenko, I.D., and Yurchenko, E.I., Zh. Anal. Khim., 1966, vol. 21, no. 6, p. 669. Savvin, S.B., Alimarin, I.P., and Belova, T.Ya., Zh. Anal. Khim., 1968, vol. 23, no. 8, p. 1117. Elinson, C.V., Savvin, S.B., and Nezhnova, T.I., Zh. Anal. Khim., 1967, vol. 22, no. 4, p. 531. Ivanov, V.M. and Ermakova, N.V., Zh. Anal. Khim., 2001, vol. 56, no. 6. Ermakova, N.V., Burmaa, D., Ivanov V.M., and Figurovskaya V.N., Vestn. Mosk. Univ., Ser. 2: Khim., 2000, vol. 41, no. 5, p. 305. Morozko, S.A. and Ivanov, V.M., Zh. Anal. Khim., 1997, vol. 52, no. 8, p. 858. Ivanov, V.M., Kuznetsova, O.V., and Grineva, O.V., Zh. Anal. Khim., 1999, vol. 54, no. 3, p. 263. Edcolar, D., Haro, R., Sausedo, A., Ayoso, J., Jimenez, A., and Alvarez, J.A., Appl. Spectrosc., 1996, vol. 50, no. 10, p. 1290. Morozko, S.A., Kuznetsova, O.V., and Ivanov, V.M., Zh. Anal. Khim., 1997, vol. 52, no. 11, p. 1146. Budesinsky, B. and Savvin, S.B., Z. Anal. Chem., 1965, vol. 214, no. 3, p. 189. Devyatova, T.M., Gen', L.I., and Yampol'skii, M.Z., Zh. Anal. Khim., 1974, vol. 29, no. 10, p. 1934. Savvin, S.B. and Propistsova, R.F., Zh. Anal. Khim., 1968, vol. 23, no. 11, p. 653.