Nucleation and crystallization of solids from solution

Ferdi Schüth1
1MPI für Kohlenforschung, Kaiser-Wilhelm-Platz 1, 45470 Mülheim, Germany

Tài liệu tham khảo

Maksimov, 2000, Energy barrier effect on transient nucleation kinetics: nucleation flux and lag-time calculation, J Chem Phys, 113, 3323, 10.1063/1.1286095 Gránásy, 2000, Cahn–Hilliard theory with triple-parabolic free energy. I. Nucleation and growth of a stable crystalline phase, J Chem Phys, 112, 2399, 10.1063/1.480806 Gránásy, 2000, Cahn–Hilliard theory with triple-parabolic free energy. I. Nucleation and growth in the presence of a metastable crystalline phase, J Chem Phys, 112, 2410, 10.1063/1.480807 ten Wolde, 1997, Enhancement of protein crystal nucleation by critical density fluctuation, Science, 277, 1975, 10.1126/science.277.5334.1975 Talanquer, 1998, Crystal nucleation in the presence of a metastable critical point, J Chem Phys, 109, 223, 10.1063/1.476554 Galkin, 2000, Control of protein crystal nucleation around the metastable liquid–liquid phase boundary, PNAS, 97, 6277, 10.1073/pnas.110000497 Kierzek, 1999, Lattice simulations of protein crystal formation, Biophys Chem, 77, 123, 10.1016/S0301-4622(99)00019-8 Auer, 2001, Prediction of absolute crystal nucleation rate in hard-sphere colloids, Nature, 409, 1020, 10.1038/35059035 Gavezotti, 1999, Molecular aggregation of acetic acid in a carbon tetrachloride solution: a molecular dynamics study with a view to crystal nucleation, Chem Eur J, 5, 567, 10.1002/(SICI)1521-3765(19990201)5:2<567::AID-CHEM567>3.0.CO;2-6 Shore, 2000, Simulations of the nucleation of AgBr from solution, J Chem Phys, 113, 6276, 10.1063/1.1308517 Anwar, 1998, Computer simulation of crystallization from solution, J Am Chem Soc, 120, 9600, 10.1021/ja972750n Schüth F, Bussian P, Agren P, Schunk S, Linden M. Techniques for studying the early stages of crystallization reactions. Solid State Sci, in press. Taulelle, 1999, NMR of microporous compounds: from in situ reactions to solid paving, Colloids Surf A, 158, 299, 10.1016/S0927-7757(99)00200-9 Allouche, 2001, 3QMAS of three aluminum polycations: space group consistency between NMR and XRD, J Phys Chem Solids, 62, 1525, 10.1016/S0022-3697(01)00069-5 Sobott, 1998, Condensation products of group IV A alkoxides examined with LILBID mass spectrometry, Chem Eur J, 4, 2353, 10.1002/(SICI)1521-3765(19981102)4:11<2353::AID-CHEM2353>3.0.CO;2-I Bussian, 2000, Speciation in solution: analysis of silicate oligomers using ESI-MS, Angew Chem Int Ed Engl, 39, 3901, 10.1002/1521-3773(20001103)39:21<3901::AID-ANIE3901>3.0.CO;2-D de Moor, 2000, Si-MFI crystallization using a ‘dimer’ and ‘trimer’ of TPA studied with small angle X-ray scattering, J Phys Chem B, 104, 7600, 10.1021/jp0006476 de Moor, 1999, In situ observation of nucleation and crystal growth in zeolite synthesis. A small angle X-ray scattering investigation on Si-TPA-MFI, J Phys Chem B, 103, 1639, 10.1021/jp982553q Ravishankar, 1999, Characterization of nanosized material extracted from clear suspensions for MFI zeolite synthesis, J Phys Chem B, 103, 4960, 10.1021/jp990296z Kirschhock, 1999, Identification of precursor species in the formation of MFI zeolite in the TPAOH–TEOS–H2O system, J Phys Chem B, 103, 4965, 10.1021/jp990297r Kirschhock, 1999, Mechanism of transformation of precursors into nanoslabs in the early stages of MFI and MEL zeolite formation from TPAOH–TEOS–H2O and TBAOH–TEOS–H2O mixtures, J Phys Chem B, 103, 4972, 10.1021/jp990298j Tebbutt, 1999, Monitoring crystallisation phenomena by ultrasound, Electron Lett, 35, 90, 10.1049/el:19990038 Moreno, 2000, Turbidity as a useful optical parameter to predict protein crystallization by dynamic light scattering, J Mol Struct, 519, 243, 10.1016/S0022-2860(99)00318-X Darcy, 1999, Identifying nucleation temperatures for lysozyme via differential scanning calorimetry, J Cryst Growth, 196, 243, 10.1016/S0022-0248(98)00845-8 Walton, 2000, Watching solids crystallise using in situ powder diffraction, PCCP, 2, 2283 Engelke, 2001, In situ X-ray diffraction studies of the crystallization of layered manganese thioantimonates(III) under hydrothermal conditions, Chem Mater, 13, 1383, 10.1021/cm001234k Agren, 2000, Kinetics of co-surfactant-surfactant-silicate phase behavior. 2. Short-chain amines, Langmuir, 16, 8809, 10.1021/la000402k Linden, 2000, Solubilization of oil in silicate–surfactant mesostructures, Langmuir, 16, 5831, 10.1021/la991671h Lindén, 1998, In situ XRD study of the initial stages of formation of MCM-41 in a tubular reactor, Angew Chem Int Ed Engl, 37, 821, 10.1002/(SICI)1521-3773(19980403)37:6<821::AID-ANIE821>3.0.CO;2-I Muncaster, 2000, On the advantages of the use of the three-element detector system for measuring EDXRD patterns to follow the crystallisation of open-framework structures, PCCP, 2, 3523, 10.1039/b004171h Anderson MW, Agger JR, Hanif N, Terasaki O. Crystal growth in framework materials. Solid State Sci, in press. Anderson, 1996, Angew Chem Int Ed Engl, 35, 1210, 10.1002/anie.199612101 Yau, 2000, Quasi-planar nucleus structure in apoferritin crystallization, Nature, 406, 494, 10.1038/35020035 Yau, 2001, Direct observation of nucleus structure and nucleation pathways in apoferritin crystallization, J Am Chem Soc, 123, 1080, 10.1021/ja003039c Yau, 2000, Molecular mechanisms of crystallization and defect formation, Phys Rev Lett, 85, 353, 10.1103/PhysRevLett.85.353 Gasser, 2001, Real-space imaging of nucleation and growth in colloidal crystallization, Science, 292, 258, 10.1126/science.1058457 Sugimoto, 2000, Spontaneous nucleation of monodisperse silver halide particles from homogeneous gelatin solution I: silver chloride, Colloids Surf A, 164, 183, 10.1016/S0927-7757(99)00366-0 Sugimoto, 2000, Spontaneous nucleation of monodisperse silver halide particles from homogeneous gelatin solution I: silver bromide, Colloids Surf A, 164, 205, 10.1016/S0927-7757(99)00365-9 Soler-Illia, 1999, Synthesis of nickel hydroxide by homogeneous alkalinization. Precipitation mechanism, Chem Mater, 11, 3140, 10.1021/cm9902220 Taulelle F. Clipping a network into a crystal. Solid State Sci, in press. The author describes the analysis of all steps in the evolution of a molecular sieve from the solution state to the final crystal, with NMR spectroscopy being the main technique used for the analysis. Schoeman, 1993, Synthesis and size tailoring of colloidal zeolite particles, J Chem Soc Chem Commun, 994, 10.1039/c39930000994 Nikolakis, 2000, Zeolite growth by addition of subcolloidal particles: modeling and experimental validation, Chem Mater, 12, 845, 10.1021/cm990653i van Grieken, 2000, Anomalous crystallization mechanism in the synthesis of nanocrystalline ZSM-5, Micropor Mesopor Mater, 39, 135, 10.1016/S1387-1811(00)00190-6 Mintova, 1999, Mechanism of zeolite A nanocrystal growth from colloids at room temperature, Science, 283, 958, 10.1126/science.283.5404.958 Kirschhock, 1999, Aggregation mechanism of nanoslabs with zeolite MFI-type structure, J Phys Chem B, 103, 11021, 10.1021/jp992272y Hanif, 2000, The effect of stirring on the synthesis of intergrowths of zeolite Y polymorphs, PCCP, 2, 3349, 10.1039/b002314k Alfredsson, 1993, Investigation of the surface structure of the zeolites FAU and EMT by high-resolution electron microscopy, Angew Chem Int Ed Engl, 32, 1210, 10.1002/anie.199312101