New insights into the structure and reduction of graphite oxide

Nature Chemistry - Tập 1 Số 5 - Trang 403-408 - 2009
Wei Gao1, Lawrence B. Alemany, Lijie Ci2, Pulickel M. Ajayan2
1Department of Chemistry, Rice University, Houston, Texas 77005 USA
2Department of Mechanical Engineering and Materials Science, Rice University, Houston, USA

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Si, Y. & Samulski, E. T. Synthesis of water soluble graphene. Nano Lett. 8, 1679–1682 (2008).

Li, D., Müller, M. B., Gilje, S., Kaner, R. B. & Wallace, G. G. Processable aqueous dispersions of graphene nanosheets. Nature Nanotech. 3, 101–105 (2008).

Li, X. et al. Highly conducting graphene sheets and Langmuir-Blodgett films. Nature Nanotech. 3, 538–542 (2008).

Hernandez, Y. et al. High-yield production of graphene by liquid-phase exfoliation of graphite. Nature Nanotech. 3, 563–568 (2008).

Lerf, A., He, H., Forster, M. & Klinowski, J. Structure of graphite oxide revisited. J. Phys. Chem. B 102, 4477–4482 (1998).

Szabó, T. et al. Evolution of surface functional groups in a series of progressively oxidized graphite oxides. Chem. Mater. 18, 2740–2749 (2006).

Cai, W. et al. Synthesis and solid-state NMR structural characterization of 13C-labeled graphite oxide. Science 321, 1815–1817 (2008).

Blumenfeld, A. L., Muradyan, V. E., Shumilova, I. B., Parnes, Z. N. & Novikov, Y. N. Investigation of graphite oxide by means of 13C NMR and 1H spin-lattice relaxation. Mater. Sci. Forum 91–93, 613–617 (1992).

Boehm, H. P., Diehl, E., Heck, W. & Sappok, R. Surface oxides of carbon. Angew. Chem. Int. Ed. 3, 669–677 (1964).

Boehm, H. P. Some aspects of the surface chemistry of carbon blacks and other carbons. Carbon 32, 759–769 (1994).

Fuente, E., Menéndez, J. A., Díez, M. A., Suárez, D. & Montes-Morán, M. A. Infrared spectroscopy of carbon materials: a quantum chemical study of model compounds. J. Phys. Chem. B 107, 6350–6359 (2003).

Wang, Z. M., Hoshinoo, K., Shishibori, K., Kanoh, H. & Ooi, K. Surfactant-mediated synthesis of a novel nanoporous carbon-silica composite. Chem. Mater. 15, 2926–2935 (2003).

Gillis, R. G. & Porter, Q. N. 5-Methoxyphenanthrene-4-carboxylic acid. Aust. J. Chem. 42, 1007–1010 (1989).

Pelletier, S. W., Djarmati, Z. & Pape, C. Substituent effects in 13C NMR Spectroscopy: methyl, ethyl, 2-propyl and 2-methyl-2-propyl carboxylates. Tetrahedron 32, 995–996 (1976).

Mukaiyama, T., Shintou, T. & Fukumoto, K. A convenient method for the preparation of inverted tert-alkyl carboxylates from chiral tert-alcohols by a new type of oxidation-reduction condensation using 2,6-dimethyl-1,4-benzoquinone. J. Am. Chem. Soc. 125, 10538–10539 (2003).

Sweeting, L. M. et al. Crystal structure and triboluminescence 2. 9-anthracenecarboxylic acid and its esters. Chem. Mater. 9, 1103–1105 (1997).

Rubin, I. B. & Buchanan, M. V. Carbon-13 NMR spectra of anthraquinone-derived dyes. Magn. Reson. Chem. 23, 161–165 (1985).

Sakamoto, Y. et al. Structure-reactivity studies by NMR spectroscopy and molecular orbital calculation: nitration of polycyclic aromatic ketones. Polycycl. Aromat. Comp. 14–15, 77–86 (1999).

Exner, O., Fiedler, P., Buděšínský, M. & Kulhánek, J. Conformation and steric effects in mono- and dimethoxybenzoic acids. J. Org. Chem. 64, 3513–3518 (1999).

Hansen, P. E., Poulsen, O. K. & Berg, A. 13C, 13C coupling constants and 13C chemical shifts of aromatic carbonyl compounds. Effects of ortho- and peri-interactions involving the carbonyl substituent. Org. Magn. Resonance 9, 649–658 (1977).

Chaikin, S. W. & Brown, W. G. Reduction of aldehydes, ketones and acid chlorides by sodium borohydride. J. Am. Chem. Soc. 71, 122–125 (1949).

Stankovich, S. et al. Synthesis of graphene-based nanosheets via chemical reduction of exfoliated graphite oxide. Carbon 45, 1558–1565 (2007).

Schniepp, H. C. et al. Functionalized single graphene sheets derived from splitting graphite oxide. J. Phys. Chem. B 110, 8535–8539 (2006).

Witter, R. et al. 13C chemical shift constrained crystal structure refinement of cellulose Iα and its verification by NMR anisotropy experiments. Macromolecules 39, 6125–6132 (2006).

Miyoshi, T., Hu, W. & Hagihara, H. Local packing disorders in a polymer crystal by two dimensional solid-state NMR. Macromolecules 40, 6789–6792 (2007).

Verel, R., Manolikas, T., Siemer, A. B. & Meier, B. H. Improved resolution in 13C solid-state spectra through spin-state-selection. J. Magn. Reson. 184, 322–329 (2007).

Cadars, S. et al. The refocused INADEQUATE MAS NMR experiment in multiple spin-systems: interpreting observed correlation peaks and optimising lineshapes. J. Magn. Reson. 188, 24–34 (2007).

Holland, G. P., Jenkins, J. E., Creager, M. S., Lewis, R. V. & Yarger, J. L. Quantifying the fraction of glycine and alanine in β-sheet and helical conformations in spider dragline silk using solid-state NMR. Chem. Commun. 5568–5570 (2008).

Kovtyukhova, N. I. et al. Layer-by-layer assembly of ultrathin composite films from micron-sized graphite oxide sheets and polycations. Chem. Mater. 11, 771–778 (1999).

Hummers, W. S. & Offeman, R. E. Preparation of graphite oxide. J. Am. Chem. Soc. 80, 1339–1339 (1958).

Mukherjee, A. et al. Dodecylated large fullerenes: an unusual class of solids. Chem. Mater. 20, 5513–5521 (2008)