Multi-residue method for determination of 58 pesticides, pharmaceuticals and personal care products in water using solvent demulsification dispersive liquid–liquid microextraction combined with liquid chromatography-tandem mass spectrometry

Talanta - Tập 146 - Trang 676-688 - 2016
Sergiane Souza Caldas1, Caroline Rombaldi1, Jean Lucas de Oliveira Arias1, Liziane Cardoso Marube1, Ednei Gilberto Prímel1
1Escola de Química e Alimentos, Universidade Federal do Rio Grande-FURG, 96203-900 Rio Grande, RS, Brazil.

Tóm tắt

Từ khóa


Tài liệu tham khảo

Caldas, 2013, Determination of pharmaceuticals, personal care products, and pesticides in surface and treated waters: method development and survey, Environ. Sci. Pollut. Res., 20, 1, 10.1007/s11356-013-1650-9

Herrero-Hernández, 2013, Occurrence of pesticides and some of their degradation products in waters in a Spanish wine region, J. Hydrol., 486, 234, 10.1016/j.jhydrol.2013.01.025

Richardson, 2011, Water Analysis: Emerging Contaminants and Current Issues, Anal. Chem., 83, 4614, 10.1021/ac200915r

Fent, 2006, Ecotoxicology of human pharmaceuticals, Aquat. Toxicol., 76, 122, 10.1016/j.aquatox.2005.09.009

Primel, 2012, Multi-residue analytical methods for the determination of pesticides and PPCPs in water by LC–MS/MS: a review, Cent. Eur. J. Chem., 10, 876

Gros, 2006, Multi-residue analytical methods using LC-tandem MS for the determination of pharmaceuticals in environmental and wastewater samples: a review, Anal. Bioanal. Chem., 386, 941, 10.1007/s00216-006-0586-z

Rezaee, 2006, Determination of organic compounds in water using dispersive liquid–liquid microextraction, J. Chromatogr. A, 1116, 1, 10.1016/j.chroma.2006.03.007

Kocúrová, 2012, Recent advances in dispersive liquid–liquid microextraction using organic solvents lighter than water. A review, Microchem. J., 102, 11, 10.1016/j.microc.2011.12.002

Leong, 2014, Beyond dispersive liquid–liquid microextraction, J. Chromatogr. A, 1335, 2, 10.1016/j.chroma.2014.02.021

Chen, 2010, Low-density extraction solvent-based solvent terminated dispersive liquid–liquid microextraction combined with gas chromatography–tandem mass spectrometry for the determination of carbamate pesticides in water samples, J. Chromatogr. A, 1217, 1244, 10.1016/j.chroma.2009.12.062

Guo, 2011, Low-density solvent-based solvent demulsification dispersive liquid–liquid microextraction for the fast determination of trace levels of sixteen priority polycyclic aromatic hydrocarbons in environmental water samples, J. Chromatogr. A, 1218, 5040, 10.1016/j.chroma.2011.05.069

Zhu, 2012, Low-density solvent-based solvent demulsification dispersive liquid-liquid microextraction combined with gas chromatography for determination of polycyclic aromatic hydrocarbons in water samples, Chin. J. Chromatogr., 30, 201, 10.3724/SP.J.1123.2011.10011

Seebunrueng, 2014, Vortex-assisted low density solvent based demulsified dispersive liquid–liquid microextraction and high-performance liquid chromatography for the determination of organophosphorus pesticides in water samples, Chemosphere, 103, 51, 10.1016/j.chemosphere.2013.11.024

Zacharis, 2010, Solvent-based de-emulsification dispersive liquid–liquid microextraction combined with gas chromatography–mass spectrometry for determination of trace organochlorine pesticides in environmental water samples, J. Chromatogr. A, 1217, 5896, 10.1016/j.chroma.2010.07.065

Tolcha, 2013, Low-density extraction solvent based solvent-terminated dispersive liquid–liquid microextraction for quantitative determination of ionizable pesticides in environmental waters, J. Sep. Sci., 36, 1119, 10.1002/jssc.201200849

Li, 2013, Low-density solvent-based dispersive liquid–liquid microextraction combined with single-drop microextraction for the fast determination of chlorophenols in environmental water samples by high performance liquid chromatography-ultraviolet detection, J. Chromatogr. A, 1280, 9, 10.1016/j.chroma.2013.01.023

Guo, 2014, Automated dispersive liquid–liquid microextraction–gas chromatography–mass spectrometry, Anal. Chem., 86, 3743, 10.1021/ac404088c

Zhang, 2013, Low-density solvent-based vortex-assisted surfactant-enhanced-emulsification liquid–liquid microextraction combined with gas chromatography–mass spectrometry for the fast determination of phthalate esters in bottled water, J. Chromatogr. A, 1274, 28, 10.1016/j.chroma.2012.12.017

Behbahani, 2013, Coupling of solvent-based de-emulsification dispersive liquid–liquid microextraction with high performance liquid chromatography for simultaneous simple and rapid trace monitoring of 2, 4-dichlorophenoxyacetic acid and 2-methyl-4-chlorophenoxyacetic acid, Environ. Monit. Assess., 1

Majidi, 2012, Solvent-based de-emulsification dispersive liquid–liquid microextraction of palladium in environmental samples and determination by electrothermal atomic absorption spectrometry, Talanta, 93, 245, 10.1016/j.talanta.2012.02.026

Behbahani, 2014, Modified nanoporous carbon as a novel sorbent before solvent-based de-emulsification dispersive liquid-liquid microextraction for ultra-trace detection of cadmium by flame atomic absorption spectrophotometry, Measurement, 51, 174, 10.1016/j.measurement.2014.02.010

DrugBank, 〈http://www.drugbank.ca/〉, (accessed March 2013, 2013).

C.Tomlin, The pesticide manual: A world compendium, Farnham, itd: British Crop Protecton Council/BCPC (2003).

SANCO, Guidance document on analytical quality control and validation procedures for pesticide residues analysis in food and feed, 〈http://www.eurl-pesticides.eu/library/docs/allcrl/AqcGuidance_Sanco_2013_12571.pdf〉, (accessed 22.08.14).

INMETRO, Orientação sobre Validação de Métodos Analíticos, 〈http://www.inmetro.gov.br/Sidoq/Arquivos/CGCRE/DOQ/DOQ-CGCRE-8_04.pdf〉, (accessed june, 2014).

Economou, 2009, Determination of multi-class pesticides in wines by solid-phase extraction and liquid chromatography–tandem mass spectrometry, J. Chromatogr. A, 1216, 5856, 10.1016/j.chroma.2009.06.031

Su, 2010, Determination of organophosphorous pesticides in water using in-syringe ultrasound-assisted emulsification and gas chromatography with electron-capture detection, J. Chromatogr. A, 1217, 5043, 10.1016/j.chroma.2010.06.006

Moradi, 2011, Analysis of abuse drugs in urine using surfactant‐assisted dispersive liquid–liquid microextraction, J. Sep. Sci., 34, 1722, 10.1002/jssc.201100132

Jia, 2010, Extraction of pesticides in water samples using vortex-assisted liquid–liquid microextraction, J. Chromatogr. A, 1217, 5868, 10.1016/j.chroma.2010.07.055

Saraji, 2010, Use of hollow fibre-based liquid–liquid–liquid microextraction and high-performance liquid chromatography–diode array detection for the determination of phenolic acids in fruit juices, Food Chem., 123, 1310, 10.1016/j.foodchem.2010.06.012

Saraji, 2008, Application of single-drop microextraction combined with in-microvial derivatization for determination of acidic herbicides in water samples by gas chromatography–mass spectrometry, J. Chromatogr. A, 1178, 17, 10.1016/j.chroma.2007.11.056

Saraji, 2005, Determination of phenols in water samples by single-drop microextraction followed by in-syringe derivatization and gas chromatography–mass spectrometric detection, J. Chromatogr. A, 1098, 30, 10.1016/j.chroma.2005.08.063

Saraji, 2009, Single‐drop microextraction followed by in‐syringe derivatization and GC‐MS detection for the determination of parabens in water and cosmetic products, J. Sep. Sci., 32, 988, 10.1002/jssc.200800635

Wakai, 2005, How polar are ionic liquids? determination of the static dielectric constant of an imidazolium-based ionic liquid by microwave dielectric spectroscopy, J. Phys. Chem. B, 109, 17028, 10.1021/jp053946+

Moradi, 2010, Application of surfactant assisted dispersive liquid–liquid microextraction for sample preparation of chlorophenols in water samples, Talanta, 82, 1864, 10.1016/j.talanta.2010.08.002

Ryu, 2012, Determination of endocrine disrupting chemicals in water samples by dispersive liquid–liquid microextraction combined with liquid chromatography–fluorescence detection, J. Pharm. Investig., 42, 77, 10.1007/s40005-012-0010-y

Salgueiro-González, 2012, Determination of alkylphenols and bisphenol A in seawater samples by dispersive liquid–liquid microextraction and liquid chromatography tandem mass spectrometry for compliance with environmental quality standards (Directive 2008/105/EC), J. Chromatogr. A, 1223, 1, 10.1016/j.chroma.2011.12.011

Zhang, 2011, A new device for magnetic stirring-assisted dispersive liquid–liquid microextraction of UV filters in environmental water samples, Talanta, 83, 1711, 10.1016/j.talanta.2010.11.076

Liu, 2010, Application of DLLME to the determination of pyrethroids in aqueous samples, Chromatographia, 72, 1017, 10.1365/s10337-010-1732-5

Fatemi, 2012, Extraction optimization of polycyclic aromatic hydrocarbons by alcoholic‐assisted dispersive liquid–liquid microextraction and their determination by HPLC, J. Sep. Sci., 35, 86, 10.1002/jssc.201100675

Hendriks, 2007, Reconsideration of sample pH adjustment in bioanalytical liquid–liquid extraction of ionisable compounds, J. Chromatogr. B, 853, 234, 10.1016/j.jchromb.2007.03.017

Yazdi, 2008, Separation and determination of amitriptyline and nortriptyline by dispersive liquid–liquid microextraction combined with gas chromatography flame ionization detection, Talanta, 75, 1293, 10.1016/j.talanta.2008.01.039

Farajzadeh, 2010, Use of a capillary tube for collecting an extraction solvent lighter than water after dispersive liquid–liquid microextraction and its application in the determination of parabens in different samples by gas chromatography – flame ionization detection, Talanta, 81, 1360, 10.1016/j.talanta.2010.02.035

Guo, 2010, Temperature-controlled ionic liquid dispersive liquid phase microextraction combined with ultra-high-pressure liquid chromatography for the rapid determination of triclosan, triclocarban and methyl-triclosan in aqueous samples, Sci. China Chem., 53, 2600, 10.1007/s11426-010-3169-y

Matkovich, 1973, Salting-out of acetone from water. Basis of a new solvent extraction system, Anal. Chem., 45, 1915, 10.1021/ac60333a023

1998, 98/83/EC of 3 November 1998 on the quality of water intended for human consumption, Off. J. Eur. Comm., 5, L330

Caldas, 2010, Validation of method for determination of different classes of pesticides in aqueous samples by dispersive liquid–liquid microextraction with liquid chromatography–tandem mass spectrometric detection, Anal. Chim. Acta, 665, 55, 10.1016/j.aca.2010.03.004

Zhao, 2011, Determination of triclosan and triclocarban in environmental water samples with ionic liquid/ionic liquid dispersive liquid-liquid microextraction prior to HPLC–ESI–MS/MS, Microchim. Acta, 174, 145, 10.1007/s00604-011-0607-2

Zgoła-Grześkowiak, 2010, Application of DLLME to isolation and concentration of non-steroidal anti-inflammatory drugs in environmental water samples, Chromatographia, 72, 671, 10.1365/s10337-010-1702-y

Parrilla Vázquez, 2013, Ultrasound-assisted ionic liquid dispersive liquid–liquid microextraction coupled with liquid chromatography-quadrupole-linear ion trap-mass spectrometry for simultaneous analysis of pharmaceuticals in wastewaters, J. Chromatogr. A, 1291, 19, 10.1016/j.chroma.2013.03.066

Margoum, 2013, Stir bar sorptive extraction coupled to liquid chromatography-tandem mass spectrometry for the determination of pesticides in water samples: method validation and measurement uncertainty, Talanta, 116, 1, 10.1016/j.talanta.2013.04.066

Tran, 2013, Simultaneous determination of PPCPs, EDCs, and artificial sweeteners in environmental water samples using a single-step SPE coupled with HPLC–MS/MS and isotope dilution, Talanta, 113, 82, 10.1016/j.talanta.2013.03.072

Fenoll, 2011, Determination of 48 pesticides and their main metabolites in water samples by employing sonication and liquid chromatography–tandem mass spectrometry, Talanta, 85, 975, 10.1016/j.talanta.2011.05.012