Microfluidic rotational flow generated by redox-magnetohydrodynamics (MHD) under laminar conditions using concentric disk and ring microelectrodes

Microfluidics and Nanofluidics - Tập 18 - Trang 159-166 - 2014
V. Sahore1,2, I. Fritsch1
1Department of Chemistry and Biochemistry, University of Arkansas, Fayetteville, USA.
2Microelectronics and Photonics Graduate Program, University of Arkansas, Fayetteville, USA

Tóm tắt

Localized microfluidic rotational flow (Reynolds number < 1) confined to a cylindrical volume element (1,600 µm diameter, 620 µm high) with velocity magnitude ≤14 µm/s was achieved in a small cell (14.3 mm wide × 27.0 mm long × 620 µm high) contained over a chip by redox-magnetohydrodynamics (MHD) pumping. The chip consisted of an insulated silicon substrate patterned with pairs of concentric disk and ring gold microelectrodes. The MHD force (F B  = j × B) was generated with ionic current density, j, from electrochemistry of 0.095 M K3Fe(CN)6 and 0.095 M K4Fe(CN)6 in a supporting electrolyte of 0.095 M KCl, and with an external magnetic field, B, from a 0.36 T NdFeB permanent magnet beneath the chip. Fluid flow was monitored between the edge of the disk (radius 80 µm) and the inner radius (800 µm) of the ring, using video microscopy to track 10-µm polystyrene latex beads in the redox solution. Data analysis was performed by particle image velocimetry software. Fluid speeds decreased approximately proportionally with radial position across the disk-ring gap, consistent with the decline of ionic current density. This behavior was visualized when half the solution over the disk (160 µm radius) and ring (1,600 µm inner radius) contained a red dye, where faster circulation near the disk caused the two solutions to pass through each other to form a spiral pattern, increasing the interfacial length, and improving opportunities for diffusional interchange. These results suggest a means for local mixing without the need for moving parts or sidewalls to guide the flow.

Tài liệu tham khảo

Anderson EC, Weston MC, Fritsch I (2010) Investigations of redox magnetohydrodynamic fluid flow at microelectrode arrays using microbeads. Anal Chem 82(7):2643–2651 Arumugam PU, Fakunle ES, Anderson EC, Evans SR, King KG, Aguilar ZP, Carter CS, Fritsch I (2006) Characterization and pumping—redox magnetohydrodynamics in a microfluidic channel. J Electrochem Soc 153(12):E185–E194 Bard AJ, Faulkner LR (1980) Electrochemical methods: fundamentals and applications. Wiley, New York Bazant MZ, Ben YX (2006) Theoretical prediction of fast 3D AC electro-osmotic pumps. Lab Chip 6(11):1455–1461 Craighead H (2006) Future lab-on-a-chip technologies for interrogating individual molecules. Nature 442(7101):387–393 Dittrich PS, Manz A (2006) Lab-on-a-chip: microfluidics in drug discovery. Nat Rev Drug Discov 5(3):210–218 Erickson D, Li DQ (2004) Integrated microfluidic devices. Anal Chim Acta 507(1):11–26 Gleeson JP, West J (2002) Magnetohydrodynamic micromixing. Modeling and simulation of microsystems. ISBN: 0-9708275-7-1 Gleeson JP, Roche OM, West J, Gelb A (2004) Modelling annular micromixers. Siam J Appl Math 64(4):1294–1310 Haeberle S, Zengerle R (2007) Microfluidic platforms for lab-on-a-chip applications. Lab Chip 7(9):1094–1110 Jang JS, Lee SS (2000) Theoretical and experimental study of MHD (magnetohydrodynamic) micropump. Sens Actuators A Phys 80(1):84–89 Kang HJ, Choi B (2011) Development of the MHD micropump with mixing function. Sens Actuators A Phys 165(2):439–445 Lee CY, Chang CL, Wang YN, Fu LM (2011) Microfluidic mixing: a review. Int J Mol Sci 12(5):3263–3287 Lemoff AV, Lee AP (2000) An AC magnetohydrodynamic micropump. Sens Actuators B Chem 63(3):178–185 Mouradian S (2002) Lab-on-a-chip: applications in proteomics. Curr Opin Chem Biol 6(1):51–56 Pamme N (2006) Magnetism and microfluidics. Lab Chip 6(1):24–38 Qian S, Bau HH (2005) Magneto-hydrodynamic stirrer for stationary and moving fluids. Sens Actuators B Chem 106(2):859–870 Sahore V, Fritsch I (2013) Flat flow profiles achieved with microfluidics generated by redox-magnetohydrodynamics (MHD). Anal Chem 85(24):11809–11816. doi:10.1021/ac402476v Scrape PG, Gerner MD, Weston MC, Fritsch I (2013) Redox-magnetohydrodynamics for microfluidic control: remote from active electrodes and their diffusion layers. J Electrochem Soc 160(6):H338–H343 Sigurdson M, Wang DZ, Meinhart CD (2005) Electrothermal stirring for heterogeneous immunoassays. Lab Chip 5(12):1366–1373 Stenberg M, Nygren H (1988) Kinetics of antigen-antibody reactions at solid-liquid interfaces. J Immunol Methods 113(1):3–15 West J, Gleeson JP, Alderman J, Collins JK, Berney H (2003) Structuring laminar flows using annular magnetohydrodynamic actuation. Sens Actuators B Chem 96(1–2):190–199 Weston MC, Fritsch I (2012) Manipulating fluid flow on a chip through controlled-current redox magnetohydrodynamics. Sens Actuators B Chem 173:935–944 Weston MC, Gerner MD, Fritsch I (2010a) Magnetic fields for fluid motion. Anal Chem 82(9):3411–3418. doi:10.1021/ac901783n Weston MC, Nash CK, Fritsch I (2010b) Redox-magnetohydrodynamic microfluidics without channels and compatible with electrochemical detection under immunoassay conditions. Anal Chem 82(17):7068–7072 Yeh RC, Hyun JK, Boehm AK, Lis JT, Franck C (2005) Improving slide-based assays by stirring: application of liquid-on-liquid mixing to immunofluorescence staining of polytene chromosomes. J Biochem Biophys Methods 64(1):59–68 Yi MQ, Qian SZ, Bau HH (2002) A magnetohydrodynamic chaotic stirrer. J Fluid Mech 468:153–177 Zhao H, Bau HH (2007) Microfluidic chaotic stirrer utilizing induced-charge electro-osmosis. Phys Rev E 75(6):066217-1–066217-8 Zhong JH, Yi MQ, Bau HH (2002) Magneto hydrodynamic (MHD) pump fabricated with ceramic tapes. Sens Actuators A Phys 96(1):59–66