Metrological characterization of X-ray diffraction methods for determination of crystallite size in nano-scale materials

Materials Characterization - Tập 58 Số 10 - Trang 883-891 - 2007
Vladimir Uvarov1, Inna Popov1
1The Hebrew University of Jerusalem, The Faculty of Natural Science, The Center for Nanoscience and Nanotechnology, The Unit for Nanoscopic Characterization, E. Safra Campus, Givat Ram, Jerusalem 91904, Israel

Tóm tắt

Từ khóa


Tài liệu tham khảo

Klug, 1974

Mittemeijer, 2004

Delhez, 1982, Determination of crystallite size and lattice distortions through X-ray diffraction line profile analysis. Recipes, methods and comments, J Anal Bioanal Chem, 312, 1

Weibel, 2005, The big problem of small particles: a comparison of methods for determination of particle size in nanocrystalline anatase powders, Chem Mater, 17, 2378, 10.1021/cm0403762

Tian, 1999, Comparison of X-ray analysis methods used to determine the grain size and strain in nanocrystalline materials, Philos Mag, A, 79, 1769, 10.1080/01418619908210391

Balzar, 2004, Size–strain line-broadening analysis of the ceria round-robin sample, J Appl Crystallogr, 37, 911, 10.1107/S0021889804022551

Marinkovic, 2001, A comparison between the Warren–Averbach method and alternate methods for X-ray diffraction microstructure analysis of polycrystalline specimens, Mater Res, 4, 71, 10.1590/S1516-14392001000200005

Santra, 2002, Voigt modeling of size–strain analysis: application to α-Al2O3 prepared by combustion technique, Bull Mater Sci, 25, 251, 10.1007/BF02711163

Scherrer, 1918, Estimation of the size and internal structure of colloidal particles by means of r.ovrddot.ontgen rays, 96

Shull, 1946, The determination of X-ray diffraction line widths, Phys Rev, 70, 679, 10.1103/PhysRev.70.679

Pielaszek, R. Diffraction studies of microstructure of nanocrystals exposed to high pressure, Ph.D. thesis, Warsaw University, Department of Physics, Warsaw, Poland; 2003.

Warren, 1950, The effect of cold-work distortion on X-ray patterns, J Appl Phys, 21, 595, 10.1063/1.1699713

Cheary, RW, Coelho, AA. Software: XFIT-FOURYA, deposited in CCP14 Powder Diffraction Library, Engineering and Physical Sciences Research Council, Daresbury Laboratory, Warrington, England; 1996 (http://www.ccp14.ac.uk/tutorial/xfit-95/xfit.htm).

Kraus, 1996, POWDER CELL — a program for the representation and manipulation of crystal structures and calculation of the resulting X-ray powder patterns, J Appl Crystallogr, 29, 301, 10.1107/S0021889895014920

Roisnel, 2000, WinPLOTR: a Windows tool for powder diffraction patterns analysis, 118

Krumm, 1994, WINFIT 1.0 — a computer program for X-ray diffraction line profile analysis, Acta Univ Carol, Geol, 38, 253

Stewart, 1989, XRAYL: a new powder diffraction profile fitting program, J Appl Crystallogr, 22, 640, 10.1107/S0021889889008770

Cheary, 2004, Fundamental parameters line profile fitting in laboratory diffractometers, J Res Natl Stand Technol, 109, 1, 10.6028/jres.109.002

Lowry, R., Concepts & Applications of inferential statistics, (http://faculty.vassar.edu/lowry/VassarStats.html).

Lee Penn, 1998, Imperfect oriented attachment: dislocation generation in defect-free nanocrystals, Science, 281, 969, 10.1126/science.281.5379.969

Nagaveni, 2004, Solar photocatalytic degradation of dyes: high activity of combustion synthesized nano TiO2, Appl Catal B: Environ, 48, 83, 10.1016/j.apcatb.2003.09.013

Tayade, 2006, Photocatalytic degradation of aqueous nitrobenzene by nanocrystalline TiO2, Ind Eng Chem Res, 45, 922, 10.1021/ie051060m

Sreethawong, 2005, Synthesis, characterization, and photocatalytic activity for hydrogen evolution of nanocrystalline mesoporous titania prepared by surfactant-assisted templating sol–gel process, J Solid State Chem, 178, 329, 10.1016/j.jssc.2004.11.014

Nagaveni, 2004, Synthesis and structure of nanocrystalline TiO2 with lower band gap showing high photocatalytic activity, Langmuir, 20, 2900, 10.1021/la035777v