Measurement Uncertainty Assessment for Determination of Allura Red in Puffed Food by HPLC

Springer Science and Business Media LLC - Tập 38 - Trang 324-328 - 2018
Ying Chen1,2, Yun Zhao3, Hua-Ming Wang1, Qing Wang4, Xi Chen4, Dong-qun Xu4, Tao Li2, Feng Yu2, Xiao-yong Wang2, Jia-fa Liu1
1Institute of Health Inspection and Testing, Hubei Provincial Center for Disease Control and Prevention, Wuhan, China
2Public Hospital Administration of Hubei Province, Health And Family Planning Commission of Hubei Province, Wuhan, China
3Department of Obsterics, Maternal and Child Health Hospital of Hubei Province, Wuhan, China
4Institute for Environmental Health and Related Product Safety, Chinese Center for Disease Control and Prevention, Beijing, China

Tóm tắt

This study aimed to assess the measurement uncertainty of a new method for determination of allura redin food by high performance liquid chromatography (HPLC). The uncertainty of mathematical model of allura red is based on Europe for Analytical Chemistry(EURACHEM) guidelines. The sources and components of uncertainty were calculated, including recovery, working solution, sample mass, final volume, response of standard solution, response of sample solution. The expanded uncertainty was 0.0024 (k=2). Uncertainty of working solution was the most significant factor contributing to the total uncertainty, accounting for 86.2%. The uncertainty of volume accounted for the minimum at 0.025%. The developed method is simple and accurate, which can be used for the determination of allura redin puffed samples.

Tài liệu tham khảo

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