Manganese(II) 9-Molybdomanganate(IV), [Mn(H2O)4]3 · [MnMo9O32] · 2H2O: Synthesis, thermal analysis, IR spectra, and crystal structure
Tóm tắt
The [Mn(H2O)4]3 · [MnMo9O32] · 2H2O complex was synthesized and studied by X-ray diffraction, thermogravimetry, powder X-ray diffraction, and IR spectroscopy. The crystals are trigonal: space group R32, a = 14.811(2) Å, c = 14.232(2) Å, V = 2703.7(8) Å3, M = 1848.5, Z = 3, ρ(calcd.) = 3.419 g/cm3.
Tài liệu tham khảo
Nikitina, E.N., Geteropolisoedineniya (Heteropoly Compounds), Moscow: Goskhimizdat, 1962.
Maksimov, G.V., Usp. Khim., 1995, vol. 64, no. 5, p. 480.
Pop, M.T., Geteropoli-i izopolioksometallaty (Heteropoly- and Isopolyoxometallates), Novosibirsk: Nauka, 1990.
Kozhevnikov, I.V., Usp. Khim., 1987, vol. 56, no. 9, p. 1417.
Misono, M., Catalysis by Acids and Bases, Imelik, B., Ed., Amsterdam: Elsevier, 1985, p. 147.
Sergienko, V.S. and Porai-Koshits, M.A., Itogi Nauki Tekh., Ser. Kristallokhimiya, Moscow: VINITI, 1985, vol. 19, p. 79.
Holguin Quinones, S., Ivanov-Emin, B.N., and Kaziev, G.Z., Zh. Neorg. Khim., 1979, vol. 24, no. 12, p. 3279.
Maksimova, L.G., Torchenkova, E.A., and Kazanskii, L.P., Zh. Neorg. Khim., 1988, vol. 33, no. 9, p. 2278.
Struve, H., J. Prakt. Chem., 1854, vol. 61 P, p. 499.
Pechard, E., Compt. Rend., 1897, vol. 129, p. 29.
Rosenheim, A. and Itzig, H., Z. Anorg. Allg. Chem., 1898, vol. 16, p. 76.
Hall, R.D., J. Am. Chem. Soc., 1907, vol. 29, no. 5, p. 692.
Holguin Quinones, S., Kaziev, G.Z., Oreshkina, A.V., et al., Koord. Khim., 2007, vol. 33, no. 6, p. 422 [Russ. J. Inorg. Chem. (Engl. Transl.), vol. 33, no. 6, p. 412].
Kaziev, G.Z., Dutov, A.A., Holguin Quinones, S., et al., Zh. Neorg. Khim., 2004, vol. 49, no. 5, p. 743 [Russ. J. Inorg. Chem. (Engl. Transl.), vol. 49, no. 5, p. 678].
Sheldrick, G.M., SHELX-97, Göttingen (Germany): Univ. of Göttingen, 1997.
Waugh, T.L.T., Shoemaker, P., and Pauling, L., Acta Crystallogr., 1954, vol. 7, no. 5, p. 438.
Porai-Koshits, M.A. and Atovmyan, L.O., Itogi Nauki Tekh., Ser. Kristallokhimiya, Moscow: VINITI, 1985, vol. 19, p. 3.
Porai-Koshits, M.A. and Atovmyan, L.O., Kristallokhimiya i stereokhimiya koordinatsionnykh soedinenii molibdena (Crystal Chemistry and Stereochemistry of Coordination Compounds of Molybdenum), Moscow: Nauka, 1975, p. 231.
Gavrilova, L.O. and Molchanov, V.N., Koord. Khim., 2005, vol. 31, no. 6, p. 427.
Davydov, A.A. and Goncharova, O.I., Usp. Khim., 1993, vol. 62, no. 2, p. 118.