Investigation of magnesium phosphate cement hydration in diluted suspension and its retardation by boric acid

Cement and Concrete Research - Tập 87 - Trang 77-86 - 2016
Hugo Lahalle1, Céline Cau Dit Coumes1, Adel Mesbah2, David Lambertin1, Céline Cannes3, Sylvie Delpech3, Sandrine Gauffinet4
1CEA, DEN, DTCD, SPDE, F-30207 Bagnols-sur-Cèze cedex, France
2ICSM, UMR 5257 CEA/CNRS/UM/ENSCM, Site de Marcoule—Bât. 426, BP 17171, 30207 Bagnols-sur-Cèze cedex, France
3Institut de Physique Nucléaire, CNRS, Univ. Paris-Sud 11, 91406 Orsay Cedex, France
4UMR6303 Laboratoire Interdisciplinaire Carnot de Bourgogne, Université de Bourgogne Dijon, Faculté des Sciences Mirande, 9 Avenue Alain Savary, BP 47870, 21078 Dijon Cedex, France

Tài liệu tham khảo

Bensted, 1994, Rapid setting magnesium phosphate cement for quick repair of concrete pavements – characterization and durability aspects – discussion, Cem. Concr. Res., 24, 595, 10.1016/0008-8846(94)90150-3 Yang, 2000, Characteristics and durability test of magnesium phosphate cement-based material for rapid repair of concrete, Mater. Struct., 33, 229, 10.1007/BF02479332 Qiao, 2010, Property evaluation of magnesium phosphate cement mortar as patch repair material, Constr. Build. Mater., 24, 695, 10.1016/j.conbuildmat.2009.10.039 Wagh, 1997, Ceramicrete stabilization of low-level mixed wastes, a complete story Covill, 2011, Development of magnesium phosphate cements for radioactive waste, Adv. Appl. Ceram., 110, 151, 10.1179/1743676110Y.0000000008 Stefanko, 2010 Langton, 2011, Use of cementitious materials for SRS reactor facility in-situ decommissioning Cau Dit Coumes, 2014, Selection of a mineral binder with potentialities for the stabilization/solidification of aluminum metal, J. Nucl. Mater., 453, 31, 10.1016/j.jnucmat.2014.06.032 Singh, 1998, Phosphate ceramic process for macroencapsulation and stabilization of low-level debris wastes, Waste Manag., 18, 135, 10.1016/S0956-053X(98)00018-X Weill, 1988 Odler, 2000, 216 Soudée, 2000, Mechanism of setting reaction in magnesia-phosphate cements, Cem. Concr. Res., 30, 315, 10.1016/S0008-8846(99)00254-9 Wagh, 1997, Stabilization of contaminated soil and wastewater with chemically bonded phosphate ceramics Chau, 2012, Potentiometric study of the formation of magnesium potassium phosphate hexahydrate, J. Mater. Civ. Eng., 24, 586, 10.1061/(ASCE)MT.1943-5533.0000410 Le Rouzic, 2014, Conditions of K-struvite formation in magnesium phosphate cements Gardner, 2015, Characterization of magnesium potassium phosphate cements blended with fly ash and ground granulated blastfurnace slag, Cem. Concr. Res., 74, 78, 10.1016/j.cemconres.2015.01.015 Hall, 2001, The effect of retarders on the microstructure and mechanical properties of magnesia–phosphate cement mortar, Cem. Concr. Res., 31, 455, 10.1016/S0008-8846(00)00501-9 Yang, 2010, Effect of borax on hydration and hardening properties of magnesium and potassium phosphate cement pastes, J. Wuhan Univ. Tech. Mater. Sci. Ed, 25, 613, 10.1007/s11595-010-0055-6 Wagh, 1995, Stabilization of hazardous ash waste with newberyite-rich chemically bonded magnesium phosphate ceramic, J. Mater. Res., 29 Soudée, 1999 Bénard, 2008, Influence of orthophosphate ions on the dissolution of tricalcium silicate, Cem. Concr. Res., 38, 1137, 10.1016/j.cemconres.2008.03.019 Nicoleau, 2014, Ion specific effects influencing the dissolution of tricalcium silicate, Cem. Concr. Res., 59, 118, 10.1016/j.cemconres.2014.02.006 Young, 1972, A review of the mechanisms of set retardation in Portland cement pastes containing organic admixtures, Cem. Concr. Res., 2, 415, 10.1016/0008-8846(72)90057-9 Benard, 2005, Hydration process and rheological properties of cement pastes modified by ortho-phosphate addition, J. Eur. Ceram. Soc., 25, 1877, 10.1016/j.jeurceramsoc.2004.06.017 Frontera, 2003, FullProf as a new tool for flipping ratio analysis, Physica B, 335, 219, 10.1016/S0921-4526(03)00241-2 Kiehl, 1933, The dissociation pressures of magnesium ammonium phosphate hexahydrate and some related substances VII, J. Am. Chem. Soc., 55, 605, 10.1021/ja01329a022 Van der Lee, 1998 Manov, 1946, Effect of sodium chloride on the apparent ionization constant of boric acid and the pH values of borate solutions, J. Res. Natl. Bur. Stand., 36, 543, 10.6028/jres.036.033 Owen, 1934, The dissociation constant of boric acid from 10 to 50°C, J. Am. Chem. Soc., 56, 1695, 10.1021/ja01323a014 Owen, 1943, The effect of sodium chloride upon the ionization of boric acid at various temperatures, J. Am. Chem. Soc., 65, 1612, 10.1021/ja01248a046 Baes, 1981, The thermodynamics of cation hydrolysis, Am. J. Sci., 281, 935, 10.2475/ajs.281.7.935 Ingri, 1962, Equilibrium studies of polyanions. 8. On the first equilibrium steps in the hydrolysis of boric acid, a comparison between equilibria in 0.1M and 3.0M NaClO4, Acta Chem. Scand., 16, 439, 10.3891/acta.chem.scand.16-0439 Champenois, 2012 Momii, 1967, Nuclear magnetic resonance study of borate-polyborate equilibria in aqueous solution, Inorg. Chem., 6, 1189, 10.1021/ic50052a026 Ingri, 1963, Equilibrium studies of polyanions. 10. On first equilibrium steps in acidification of B(OH)4, an application of self-medium method, Acta Chem. Scand., 17, 573, 10.3891/acta.chem.scand.17-0573 Ingri, 1963, Equilibrium studies of polyanions. 11. Polyborates in 3.0M NaBr, 3.0M LiBr and 3.0M KBr, a comparison with data obtained in 3.0M NaClO4, Acta Chem. Scand., 17, 581, 10.3891/acta.chem.scand.17-0581 Maya, 1976, Identification of polyborate and fluoropolyborate ions in solution by Raman spectroscopy, Inorg. Chem., 15, 2179, 10.1021/ic50163a036 Reardon, 1976, Dissociation constants for alkali earth and sodium borate ion pairs from 10 to 50°C, Chem. Geol., 18, 309, 10.1016/0009-2541(76)90013-9 Dryssen, 1973, Ionic medium effects in seawater, Mar. Chem., 1, 137 Byrne, 1974, Inorganic speciation of boron in seawater, J. Mar. Res., 32, 119 Bassett, 1980, A critical evaluation of the thermodynamic data for boron ions, ion pairs, complexes and polyanions in aqueous solution at 298.15K and 1bar, Geochim. Cosmochim. Acta, 44, 1151, 10.1016/0016-7037(80)90069-1 Wagh, 2004, 264