Influence of electron beam irradiation on the alloy‐to‐resin bond strength

European Journal of Oral Sciences - Tập 113 Số 5 - Trang 429-435 - 2005
Michaël Behr1, Martin Rosentritt, Klaus Bettermann, Gerhard Handel
1Department of Prosthodontics, University of Regensburg, School of Dentistry, Regensburg, Germany. [email protected]

Tóm tắt

The aim of this study was to investigate whether postcuring using electron beam irradiation had an effect on the bond strength of resin‐to‐base‐metal after priming their surfaces using silicoating methods or functional monomers. Composite cylinders were bonded on a restricted area of 5 mm2 to flat rectangular titanium and cobalt‐chromium specimens. Under investigation were the silicoating system Rocatec, the thiol‐phosphate system Metal Primer II and the phosphate ester SR Link. Tensile strength and shear bond strength were determined for the three test groups in each case: (i) after 24 h, (ii) after electron beam irradiation (100 kGy), and (iii) after irradiation (100 kGy) + 12,000 cycles of thermal cycling (5°/55°C). The bond strength was highly affected by irradiation and the metal priming method used. However, the tribochemical silicoating method and phosphate‐ester group showed no significant statistical change in bond strength. Only the thiol‐phosphate system showed considerably higher tensile and shear bond strengths after irradiation. Thermal cycling did not deteriorate this bond and there was a tendency for higher bond strength on titanium. As a result it was determined that thiol‐phosphate primers in combination with postcuring using electron beam irradiation can considerably improve the bond strength between resins and titanium or cobalt‐chromium alloys.

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Tài liệu tham khảo

10.1016/S0022-3913(03)00261-0

Hansson O, 1993, Evaluation of three silicoating methods for resin‐bonded prostheses, Scand J Dent Res, 101, 243

Peutzfeldt A, 1988, Silicoating: evaluation of a new method of bonding composite resin to metal, Scand J Dent Res, 96, 171

10.1177/00220345900690091601

10.1034/j.1600-0722.2000.108005456.x

Matsumara H, 1988, Adhesive 4‐Meta/MMA‐TBB opaque resin with poly(methyl methacrylate)‐coated titanium dioxide, J Dent Res, 67, 29, 10.1177/00220345880670010501

10.1016/S0022-3913(00)70088-6

10.1016/S0300-5712(02)00082-9

10.1038/171167a0

Sotobayashi H, 1982, Degradation of polymethylmethacrylate by synchroton radiation, Polymer Bull, 7, 95, 10.1007/BF00265458

Wilson JE, 1974, Radiation Chemistry of Monomers. Polymers and Plastics, 10.1063/1.3128702

10.1016/S0969-806X(01)00478-9

10.1002/app.1987.070340316

10.4012/dmj.20.325

1994, Dental materials – Guidance on Testing of Adhesion to Tooth Structure.

Marx R, 1992, Tensile or shear test – which test investigates better the metal/resin interface? [in German], Dtsch Zahnärztl Z, 47, 165

Darvell BW, 2002, Materials Science for Dentistry. Mechanical Testing

10.1080/000163502762667405

10.1038/1711153a0

Schlitz A, 1985, Degradation effects of ion and electron beam in polymers‐modification of the Charlesby's law. Proceedings of the Microcircuit Eng. 84 Conference, 544

Sotobayashi H, 1982, Degradation of polymethylmethacrylate by synchroton radiation, Polymer Bull, 7, 95, 10.1007/BF00265458

10.1016/S0014-3057(01)00011-8

10.1007/s10856-005-5905-y

10.1016/S0022-3913(98)70149-0

10.1016/0022-3913(92)90233-Z

10.1016/j.dental.2005.01.017