Evaluation of hydrogen dissolved in rubber materials under high-pressure exposure using nuclear magnetic resonance
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Conner, W. C., Weist, E. L., Ito, T. & Fraissard, J. Characterization of the porous structure of agglomerated microspheres by xenon-129 NMR spectroscopy. J. Phys. Chem. 93, 4138–4142 (1989).
Nagano, J., Eguchi, T., Asanuma, T., Masui, H., Nakayama, H., Nakamura, N. & Derouane, E. G. 1H and 129Xe NMR investigation of the microporous structure of dealuminated H-mordenite probed by methane and xenon. Micro. Meso. Mater. 33, 249–256 (1999).
Miyoshi, T., Takegoshi, K. & Terao, T. 129Xe NMR study of free volume and phase separation of the polystyrene/poly(vinyl methyl ether) blend. Polymer 38, 5475–5480 (1997).
Suzuki, T., Yoshimizu, H. & Tsujita, Y. Analysis of gas transport properties of PPO/PS blends by 129Xe NMR spectroscopy. Polymer 44, 2975–2982 (2003).
Yoshimizu, H., Suzuki, T. & Tsujita, Y. Characterization of polymer in the solid state by 129Xe NMR spectroscopy. Seni Gakkaishi 60, 26–31 (2004).
Yoshimizu, H., Tsukahara, M., Suzuki, T., Toida, J., Ando, A., Watanabe, J. & Tsujita, Y. Layered structure and, Xe sorption and diffusion properties of low-density liquid-crystalline polyesters with n-alkyl side chains. J. mol. Struct. 739, 19–26 (2005).
Parker, W. O., Ferrando, A., Ferri, D. & Canepari, V. Cross-link density of a dispersed rubber measured by 129Xe chemical shift. Macromolecules 40, 5787–5790 (2007).
Murata, M., Murata, Y. & Komatsu, K. Synthesis and properties of endohedral C60 encapsulating molecular hydrogen. J. Am. Chem. Soc. 128, 8024–8033 (2006).
Shen, K. & Pietrass, T. NMR spectroscopy of hydrogen adsorption on single-walled carbon nanotubes after exposure to hight pressure. Solid State Nucl. Magn. Reson. 29, 125–131 (2006).
Nishimura, S. & Fujiwara, H. Detection of hydrogen dissolved in acrylonitrile butadiene rubber by 1H nuclear magnetic resonance. Chem. Phys. Lett. 522, 43–45 (2012).
Briscoe, B. J., Savvas, T. & Kelly, C. T. Explosive decompression failure of rubber. Rubber Chem. Technol. 67, 384–416 (1994).
Yamabe, J., Nakao, M., Fujiwara, H. & Nishimura, S. In: Hydrogen Conference, (Jackson Lake Lodge, USA, 2008).
Yamabe, J., Nakao, M., Fujiwara, H. & Nishimura, S. Influence of fillers on hydrogen penetration properties and blister fracture of EPDM composites exposed to 10 MPa hydrogen gas. Transact. Jpn Soc. Mech. Eng. 74, 971–981 (2008).
Yamabe, J., Koga, A. & Nishimura, S. Durability and hydrogen permeation properties of sealing rubber under high pressure hydrogen gas. Nippon. Gomu. Kyokaishi 83, 159–166 (2010).
Yamabe, J. & Nishimura, S. Influence of fillers on hydrogen penetration properties and blister fracture of rubber composites for O-ring exposed to high-pressure hydrogen gas. Int. J. Hydrogen Energy 34, 1977–1989 (2009).
Fujiwara, H., Yamabe, J. & Nishimura, S. Evaluation of the change in chemical structure of acrylonitrile butadiene rubber after high-pressure hydrogen exposure. Int. J. Hydrogen Energy 37, 8729–8733 (2012).
Fujiwara, H., Yamabe, J. & Nishimura, S. Determination of chemical structure of vulcanized NBR with solid state 1H, 13C NMR spectroscopy. Kobunshi Ronbunshu 66, 363–372 (2009).
Fujiwara, H., Yamabe, J. & Nishimura, S. Determination of chemical shift of gas-phase hydrogen molecules by 1H nuclear magnetic resonance. Chem. Phys. Lett. 498, 42–44 (2010).
Fujiwara, H. & Nishimura, S. Pressure and temperature dependency for chemical shift in 1H nuclear magnetic resonance spectra of gaseous phase hydrogen. Chem. Phys. Lett (in press).
Van Geet, A. L. Calibration of methanol nuclear magnetic resonance thermometer at low temperature. Anal. Chem. 42, 679–680 (1970).
Raidford, D. S., Fisk, C. L. & Becker, E. D. Calibration of methanol and ethylene glycol nuclear magnetic resonance thermometers. Anal. Chem. 51, 2050–2051 (1979).
Matsumoto, M. & Espenson, J. H. Kinetics of the interconversion of parahydrogen and orthohydrogen catalyzed by paramagnetic complex ions. J. Am. Chem. Soc. 127, 11447–11453 (2005).
Züttel, A., Borgschutle, A. & Schlapbach, L. Hydrogen as a Future Energy Carrier, (Wiley-VCH Verlag GmbH & Co. KGaA, Weinheim, Germany, 2008).