Evaluation of an analytical method for determining phthalate esters in wine samples by solid-phase extraction and gas chromatography coupled with ion-trap mass spectrometer detector

Springer Science and Business Media LLC - Tập 402 Số 3 - Trang 1373-1381 - 2012
Mario Vincenzo Russo1, Ivan Notardonato1, Giuseppe Cinelli1, Pasquale Avino2
1Università del Molise
2Chemical Laboratory, DIPIA, INAIL (ex-ISPESL)

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Staples CA, Peterson DR, Parkerton TF, Adams WJ (1997) The environmental fate of phthalate esters: a literature review. Chemosphere 35:667–749

Stanley MK, Robillard KA, Staples CA (2003) The handbook of environmental chemistry, part Q. Phthalates esters. Springer, Berlin

Gomez-Hens A, Aguilar-Caballos MP (2003) Social and economic interest in the control of phthalic acid esters. Trends Anal Chem 22:847–857

Castle L, Mercer AJ, Startin JR, Gilbert J (1988) Migration from plasticized films into foods 3. Migration of phthalate, sebacate, citrate and phosphate esters from films used for retail food packaging. Food Add Cont 5:9–20

International Agency for Research on Cancer (2000) Di(2-ehylhexyl) phthalate IARC Monograph on the evaluation of carcinogenic risks to humans. Lyon (France)

van Wezel AP, Van Vlaardingen P, Posthumus R, Crommentuijn GH, Sijm DTHM (2000) Environmental risk limits for two phthalates, with special emphasis on endocrine disruptive properties. Ecotoxicol Environ Safety 46:305–321

Gray LE, Ostby J, Furr J, Veeramachaneni DNR, Parks L (2000) Perinatal exposure to the phthalates DEHP, BBP, and DINP, but not DEP, DMP, or DOTP, alters sexual differentiation of the male rat. Toxicol Sci 58:350–365

Petrovic M, Eljarrat E, Lòpez de Alda MJ, Barcelò D (2001) Analysis and environmental levels of endocrine-disrupting compounds in freshwater sediments. Trends Anal Chem 20:637–648

Hauser R, Meeker JD, Duty S, Silva MJ, Calafat AM (2006) Altered semen quality in relation to urinary concentrations of phthalate monoester and oxidative metabolites. Epidemiol 17:682–691

Gunnarsson D, Leffler P, Ekwurtzel E, Martinsson G, Liu K, Selstam G (2008) Mono-(2-ethylhexyl) phthalate stimulates basal steroidogenesis by a cAMP-independent mechanism in mouse gonadal cells of both sexes. Reproduction 135:693–703

Harris CA, Henttu P, Parker MG, Sumpter JP (1997) The estrogenic activity of phthalate esters in vitro. Environ Health Perspect 105:802–811

Paganetto G, Campi F, Varani K, Piffanelli A, Giovannini G, Borea PA (2000) Endocrine disrupting agents on healthy human tissues. Pharmacol Toxicol 86:24–29

Sathyanarayana S, Karr CJ, Lozano P, Brown E, Calafat AM, Liu F, Swan SH (2008) Baby care products: possible sources of infant phthalate exposure. Pediatrics 121:260–268

US Environmental Protection Agency (1999) Introduction to Water Policy Standards. Office of Water, Washington, DC

World Health Organization (WHO) (2003) Chapter 8: Chemical aspects, guidelines for drinking-water quality, 3 rd ed., Geneva. (available at: www.who.int/docstore/ water_sanitation_health/GDWQ/Updating/draftguidel/2003gdwq8.pdf)

Prokupkovà G, Holadovà K, Poustka J, Hajslova J (2002) Development of a solid-phase microextraction method for the determination of phthalic acid esters in water. Anal Chim Acta 457:211–223

Fankhauser-Noti A, Grob K (2007) Blank problems in trace analysis of diethylhexyl and dibutyl phthalate: investigation of the sources, tips and tricks. Anal Chim Acta 582:353–360

Batlle R, Nerìn C (2004) Application of single-drop microextraction to the determination of dialkyl phthalate esters in food simulates. J Chromatogr A 1045:29–35

Polo M, Llompart M, Garcia-Jares C, Cela R (2005) Multivariate optimization of a solid-phase microextraction method for the analysis of phthalate esters in environmental waters. J Chromatogr A 1072:63–72

Jonsson S, Boren H (2002) Analysis of mono- and diesters of o-phthalic acid by solid-phase extractions with polystyrene–divinylbenzene-based polymers. J Chromatogr A 963:393–400

Sablayrolles C, Montréjaud-Vignoles M, Benanou D, Patria L, Treilhou M (2005) Development and validation of methods for trace determination of phthalates in sludges and vegetables. J Chromatogr A 1072:233–242

Shen HY (2005) Simultaneous screening and determination eight phthalates in plastic products for food use by sonication-assisted extraction/GC-MA methods. Talanta 66:734–739

Kotowska UK, Garbowska VI (2006) Distribution coefficients of phthalates between adsorption fiber and water and its using in quantitative analysis. Anal Chim Acta 560:110–117

Del Carlo M, Pepe A, Sacchetti G, Compagnone D, Mastrocola D, Cichelli A (2008) Determination of phthalate esters in wine using solid-phase extraction and gas chromatography–mass spectrometry. Food Chem 111:771–777

Cano JM, Marín ML, Sánchez A, Hernandis ML (2002) Determination of adipate plasticizers in poly(vinyl chloride) by microwave assisted extraction. J Chromatogr A 963:401–409

Peñalver A, Pocurull E, Borrull F, Marcé RM (2001) Comparison of different fibers for the solid-phase microextraction of phthalate esters from water. J Chromatogr A 922:377–384

Brossa L, Marcé RM, Borrull F, Pocurull E (2003) Determination of endocrine-disrupting compounds in water samples by on-line solid-phase extraction-programmed-temperature vaporisation-gas chromatography–mass spectrometry. J Chromatogr A 998:41–50

Holadová K, Prokůpková G, Hajšlová J, Poustka J (2007) Headspace solid-phase microextraction of phthalic acid esters from vegetable oil employing solvent based matrix modification. Anal Chim Acta 582:24–33

Zhu J (2006) Phthalate esters in human milk: concentration variation over a six-month postpartum time. Environ Sci Technol 40:5276–5281

Casajuana N, Lacorte S (2003) Presence and release of phthalic esters and other endocrine disrupting compounds in drinking water. Chromatographia 57:649–655

Carrillo JD, Salazar C, Moreta C, Tena MT (2007) Determination of phthalates in wine by headspace solid-phase microextraction followed by gas chromatography–mass spectrometry: fibre comparison and selection. J Chromatogr A 1164:248–261

Russo MV, Goretti G, Liberti A (1993) Rapid determination of chlorinated pesticides using CN-bonded cartridge followed by GC-ECD. Chromatographia 35:290–294

Russo MV, Goretti G, Nevigato T (1999) Sequential solid-phase extract in with cyanopropil bonded-phase cartridge for trace enrichment of PCB’s chlorinated pesticides for water samples. Chromatographia 50:446–452

Russo MV (2000) Fast solid phase extraction polychlorobiphenylis and chlorinated pesticides residues from mussels using Sep-Pack cartridges. Chromatographia 51:71–76

Russo MV (2000) Diol Sep-Pack cartridges for polychlorobiphenyls and chlorinated pesticides enrichment from water samples; determination by GC-ECD. Chromatographia 53:93–98

Russo MV, Avino P (2001) Determination of 1,2,4- and 1,3,5-trichlorobenzenes in water samples by solid-phase extraction and gas-chromatography coupled to electron capture. Anal Lett 34:1003–1013

Russo MV, Avino P, Notardonato I, Cinelli G (2009) Cyanopropyl bonded-phase cartridges for trace enrichment of dioxins and chlorinated pesticides from water sample. Chromatographia 69:709–717

Russo MV, Avino P, Notardonato I, Cinelli G (2009) Aromatic sulphur compounds enrichment from seawater in crude oil contamination by solid phase extraction. Current Anal Chem 5:339–346

Cartoni GP, Goretti G, Neri B, Russo MV (1989) Evaluation of small diameter capillary columns for gas chromatography. J Chromatogr 475:145–151

Russo MV, Goretti G, Soriero A (1996) Preparation and application of fused-silica capillary microcolumns (25–50 μm I.D.) in gas chromatography. Ann Chim (Rome) 86:115–124

Knoll JK (1985) Estimation of the limit of detection in chromatography. J Chromatogr Sci 23:422–425

Legislative Decree 109/1992 (1992) Attuazione delle direttive 89/395/CEE e 89/396 CEE concernenti l'etichettatura, la presentazione e la pubblicità dei prodotti alimentari. Gazz. Uff. It. 17 February, n. 39.

Kamrin MA (2009) Phthalate risks, phthalate regulation, and public health: a review. J Toxic Environ Health B 12:157–174

Vera P, Aznar M, Mercea P, Nerín C (2011) Study of hotmelt adhesives used in food packaging multilayer laminates. Evaluation of the main factors affecting migration to food. J Mater Chem 21:420–431

Aznar M, Vera P, Canellas E, Nerín C, Mercea P, Störmer A (2011) Composition of the adhesives used in food packaging multilayer materials and migration studies from packaging to food. J Mater Chem 21:4358–4370