Effect of Synthesis Conditions on the Structure and Phase Composition of Magnesium Diboride

Inorganic Materials: Applied Research - Tập 10 - Trang 162-167 - 2019
I. M. Abdyukhanov1, A. S. Tsapleva1, A. V. Borisov1, O. A. Krymskaya2, M. G. Isaenkova2, D. K. Figurovskii3
1Bochvar High-Technology Scientific Research Institute for Inorganic Materials, Moscow, Russia
2National Research Nuclear University MEPhI, Moscow, Russia
3Moscow Technological University, Moscow, Russia

Tóm tắt

Abstract—The effect of synthesis conditions exerted on the phase composition of MgB2 samples synthesized in a temperature range from 650 to 900°C and the features of the microstructure thereof are studied. It is shown that the maximum processing level of the initial boron and magnesium mixture into magnesium boride MgB2 with a minimum content of impurity phases of magnesium oxide and higher magnesium borides can be achieved in the samples after annealing in a temperature range from 650 to 750°C for 1 h upon a preliminary compaction pressure amounting to 630–640 MPa.

Tài liệu tham khảo

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