Development of novel three-dimensional reconstruction method for porous media for polymer electrolyte fuel cells using focused ion beam-scanning electron microscope tomography

Journal of Power Sources - Tập 347 - Trang 108-113 - 2017
Takeshi Terao1, Gen Inoue2, Motoaki Kawase2, Norio Kubo1, Makoto Yamaguchi1, Kouji Yokoyama1, Tomomi Tokunaga1, Kazuhiko Shinohara1, Yuka Hara3, Toru Hara3
1FC-Cubic Technology Research Association, 2-3-26, Aomi, Koto-ku, Tokyo, 135-0064, Japan
2Department of Chemical Engineering, Faculty of Engineering, Kyoto University, Kyoto-daigaku-katsura, Nishikyo-ku, Kyoto, 615-8510, Japan
3National Institute for Materials Science, 1-2-1, Sengen, Tsukuba, Ibaraki 305-0047, Japan

Tài liệu tham khảo

Mehta, 2003, Review and analysis of PEM fuel cell design and manufacturing, J. Power Sources, 114, 32, 10.1016/S0378-7753(02)00542-6 Costamagna, 2001, Quantum jumps in the PEMFC science and technology from the 1960s to the year 2000 Part II. Engineering, technology development and application aspects, J. Power Sources, 102, 253, 10.1016/S0378-7753(01)00808-4 Hirschenhofer, 1998 Ohma, 2011, Analysis of proton exchange membrane fuel cell catalyst layers for reduction of platinum loading at Nissan, Electrochim. Acta, 56, 10832, 10.1016/j.electacta.2011.04.058 Murata, 2014, Vertically aligned carbon nanotube electrodes for high current density operating proton exchange membrane fuel cells, J. Power Sources, 253, 104, 10.1016/j.jpowsour.2013.11.073 Ostadi, 2010, 3D reconstruction of a gas diffusion layer and a microporous layer, J. Mem. Sci., 351, 69, 10.1016/j.memsci.2010.01.031 Dalasm, 2013, A comparison of laboratory based and synchrotron based nano X-ray CT for PEFC micro porous layer, ECS Trans., 58, 345, 10.1149/05801.0345ecst Epting, 2012, Resolving the three-dimensional microstructure of polymer electrolyte fuel cell electrodes using nanometer-scale X-ray computed tomography, Adv. Funct. Mater, 22, 555, 10.1002/adfm.201101525 Schulenburg, 2011, 3D imaging of catalyst support corrosion in polymer electrolyte fuel cells, J. Phys. Chem. C, 115, 14236, 10.1021/jp203016u Wargo, 2013, Comparison of focused ion beam versus nano-scale X-ray computed tomography for resolving 3-D microstructures of porous fuel cell materials, J. Power Sources, 241, 608, 10.1016/j.jpowsour.2013.04.153 Zils, 2010, 3D visualisation of PEMFC electrode structures using FIB nanotomography, Fuel Cells, 10, 966, 10.1002/fuce.201000133 Thiele, 2011, Nano-morphology of a polymer electrolyte fuel cell catalyst layer—imaging, reconstruction and analysis, Nano Res., 4, 849, 10.1007/s12274-011-0141-x Wilson, 2011, Measurement of three-dimensional microstructure in a LiCoO2 positive electrode, J. Power Sources, 196, 3443, 10.1016/j.jpowsour.2010.04.066 Iwai, 2010, Quantification of SOFC anode microstructure based on dual beam FIB-SEM technique, J. Power Sources, 195, 955, 10.1016/j.jpowsour.2009.09.005 Vierrath, 2015, Enhancing the quality of the tomography of nanoporous materials for better understanding of polymer electrolyte fuel cell materials, J. Power Sources, 285, 413, 10.1016/j.jpowsour.2015.03.110 Zielke, 2016, Three-dimensional morphology of the interface between micro porous layer and catalyst layer in a polymer electrolyte membrane fuel cell, RSC Adv., 6, 80700, 10.1039/C6RA16560E Salzer, 2012, A two-stage approach to the segmentation of FIB-SEM images of highly porous materials, Mater. Charact., 69, 115, 10.1016/j.matchar.2012.04.003 Salzer, 2014, On the importance of FIB-SEM specific segmentation algorithms for porous media, Mater. Charact., 95, 36, 10.1016/j.matchar.2014.05.014 Hara, 2013, Application of orthogonally arranged FIB–SEM for precise microstructure analysis of materials, J. Alloys Compd., 577S, S717, 10.1016/j.jallcom.2012.02.019 Inoue, 2008, Development of simulated gas diffusion layer of polymer electrolyte fuel cells and evaluation of its structure, J. Power Sources, 175, 145, 10.1016/j.jpowsour.2007.09.014 Inoue, 2008, Development of simulated gas diffusion layer of polymer electrolyte fuel cells and evaluation of its structure, J. Power Sources, 175, 145, 10.1016/j.jpowsour.2007.09.014 Watanabe, 2002, RW3D.m: three-dimensional random walk program for the calculation of the diffusivities in porous media, Comput. Geosci., 28, 583, 10.1016/S0098-3004(01)00057-7 Yokoyama, 2014, 145 Otsu, 1979, A threshold selection method from gray-level histograms, IEEE Trans. Syst. Man Cybern., 9, 10.1109/TSMC.1979.4310076