Continuous-Flow Microfluidic Electrochemical Synthesis: Investigating a New Tool for Oxidative Chemistry

Journal of Flow Chemistry - Tập 3 Số 2 - Trang 34-40 - 2013
Gregory P. Roth, Romain Stalder, Toby R. Long, Daryl R. Sauer, Stevan W. Djurić

Tóm tắt

Từ khóa


Tài liệu tham khảo

(a) Bochet, C. G.; Blanc, A. Photolabile Protecting Groups in Organic Synthesis. In <i>Handbook of Synthetic Photochemistry</i>; Albini, A.; Fagnoni, M., Eds.; Wiley-VCH: Weinheim, 2010; 417–447; (b) Yoshida, J.; Kataoka, K.; Horcajada, R.; Nagaki, A. <i>Chem. Rev</i>. <b>2008</b>, <i>108</i>, 2265–2299; (c) Patel, V. K.; Sen, D. J.; Patel, H. U.; Patel, C. N. <i>J. Chem. Pharm. Res</i>. <b>2010</b>, <i>2</i>, 573–580.

(a) Booker-Milburn, K. <i>Nat. Chem.</i><b>2012</b>, <i>4</i>, 433–435; (b) Longstreet, A. R.; McQuade, D. T. <i>Acc. Chem. Res.</i>, Article ASAP, doi:10.1021/ar300144x; (c) Yoshida, J.-I.; Suga, S. <i>Chem. Eur. J.</i><b>2002</b>, <i>8</i>, 2650–2658; (d) Loewe, H.; Ehrfeld, W. <i>Electrochim. Acta</i>, <b>1999</b>, <i>44</i>, 3679–3689.

(a) Pütter, H. <i>Industrial Electroorganic Chemistry</i>, edition 4; Marcel Dekker: New York, 2001; (b) Ziogas, A.; Kolb, G.; O'Connell, M.; Attour, A.; Lapicque, F.; Matlosz, M.; Rode, S. <i>J. Appl. Electrochem.</i><b>2009</b>, <i>39</i>, 2297–2313.

Rode, S.; Lapicque, F. Microstructured Reactors for Electrochemical Synthesis. In <i>Micro Process Engineering, Vol. 1: Fundamentals, Operations, and Catalysts</i>; Hessel, V.; Renken, J. C.; Yoshida, J.-I., Eds.; Wiley-VCH KGaA: Weinheim, 2009.

(a) Hoormann, D.; Kubon, C.; Jörissen, J.; Kröner, L.; Pütter, H. <i>J. Electroanal. Chem</i>. <b>2001</b>, <i>507</i>, 215–225; (b) Horcajada, R.; Okajima, M.; Suga, S.; Yoshida, J.-I. <i>Chem. Commun</i>. <b>2005</b>, 1303–1305; (c) Kataoka, K.; Hagiwara, Y.; Midorikawa, K.; Suga, S.; Yoshida, J.-I. <i>Org. Process Res. Dev</i>. <b>2008</b>, <i>12</i>, 1130–1136; (d) Horii, D.; Atobe, M.; Fuchigami, T.; Marken, F. <i>J. Electrochem. Soc</i>. <b>2006</b>, <i>153</i>, D143–D147; (e) Paddon, C. A.; Pritchard, G. J.; Thiemann, T.; Marken, F. <i>Electrochem. Commun</i>. <b>2002</b>, <i>4</i>, 825–831; (f) Hori, D.; Fuchigami, T.; Atobe, M. <i>J. Am. Chem. Soc.</i><b>2007</b>, <i>129</i>, 11692–11693; (g) Watts, K.; Gattrell, W.; Wirth, T. <i>Beilstein J. Org. Chem</i>. <b>2011</b>, <i>7</i>, 1108–1114; (h) Suga, S.; Okajima, M.; Fujiwara, M.; Yoshida, J. <i>J. Am. Chem. Soc</i>. <b>2001</b>, <i>123</i>, 7941–7942; (i) C. Karakus, C.; Zuman, P. J. <i>J. Electrochem. Soc.</i><b>1995</b>, <i>142</i>, 4018–4025.

For further details on the Flux Module reactor, see <a href="http://www.syrris.com/">www.syrris.com</a> . Syrris Ltd., 27 Jarman Way, Royston, Hertfordshire SG8 5HW, United Kingdom 01763 242555

Utley, J. <i>Chem. Soc. Rev.</i><b>1997</b>, <i>26</i>, 157–167.

Kawabata, J.; Nozawa, K.; Kawai, K.; Nakajima, S. <i>Liebigs Ann. Chem.</i><b>1960</b>, <i>2</i>, 181–183.

Konno, A.; Fuchigami, T. <i>J. Appl. Electrochem</i>. <b>1995</b>, <i>25</i>, 173–175.

Nematollahi, D.; Tammari, E. <i>J. Org. Chem</i>. <b>2005</b>, <i>70</i>, 7769–7772.

Maeda, G.; Ashie, H.; Maki, T.; Ohmori, H. <i>Chem. Pharm. Bull.</i><b>1997</b>, <i>45</i>, 1729–1733.

Hirashima, T.; Nishiguchi, I. <i>J. Org. Chem.</i><b>1985</b>, <i>50</i>, 539–541.

Brinkhaus, K.-H. G.; Steckhan, E. <i>Tetrahedron</i><b>1986</b>, <i>42</i>, 553–560.

(a) Utley, J. H. P.; Rosenberg, G. G. <i>Tetrahedron</i><b>2002</b>, <i>58</i>, 5251–5265; (b) Barba, I.; Alonso, F. <i>J. Org. Chem</i>. <b>1989</b>, <i>54</i>, 4365–4367; (c) Barba, I.; Gómez, C.; Chinchilla, R. <i>J. Org. Chem.</i><b>1990</b>, <i>55</i>, 3272–3273.

Bard, A. J.; Faulkner, L. R. <i>Electrochemical Methods. Fundamentals and Applications</i>, edition 2; Wiley: New York, 2001.

Arnold, D. R.; Du, X.; Henselheit, K. M. <i>Can. J. Chem.</i><b>1991</b>, <i>69</i>, 839–852.

Pavlishchuk, V. V.; Addison, A. W. Addison. <i>Inorg. Chim. Acta</i><b>2000</b>, <i>298</i>, 97–102.

Rees, N. V.; Klymenko, O. V.; Compton, R. G.; Oyama, M. <i>J. Electroanal. Chem.</i><b>2002</b>, <i>531</i>, 33–42.

(a) Hermeling, D.; Harreus, A.; Wild, J.; Goetz, N. U.S. Patent 5,078,838, Jan 7, 1992; (b) Stecker, F.; Griesbach, U.; Bock, M.; Koenigsmann, L. U.S. Patent 2011/0207968 A1, Aug 25, 2011.