Chemical shift assignments of dsRBD1 and linker region of R2D2, a siRNA binding protein in the Drosophila RNAi pathway

Biomolecular NMR Assignments - Tập 17 - Trang 211-215 - 2023
Ramdas Aute1,2, Mandar V. Deshmukh1,2
1CSIR-Centre for Cellular and Molecular Biology, Council of Scientific and Industrial Research, Hyderabad, India
2Academy of Scientific and Innovative Research (AcSIR), Ghaziabad, India

Tóm tắt

In the model organism Drosophila melanogaster, one of the Dicer homologs, Dcr-2, initiates the RNA interference pathway by cleaving long double-stranded RNA into small interfering RNA (siRNA). The Dcr-2:R2D2 heterodimer subsequently binds to the 21-nucleotide siRNA to form the R2D2:Dcr-2 Initiator (RDI) complex, which is critical for initiating the assembly of the RNA-induced silencing complex containing guide siRNA strand. During RDI complex formation, R2D2 senses the stability of the 5′ end of the siRNA and a 5′-phosphate group, although the underlying mechanism of siRNA asymmetry sensing and 5′-phosphate recognition by R2D2 is elusive. In this study, we present nearly complete chemical shift assignments of the backbone and the side chain of a construct that comprises the N-terminus dsRBD1 and linker of R2D2 (~ 10.3 kDa; henceforth: R2D2D1L). Our study would further aid in the structural and functional characterization of R2D2.

Tài liệu tham khảo

Benoit MP, Plevin MJ (2013) Backbone resonance assignments of the micro-RNA precursor binding region of human TRBP. Biomol NMR Ass 7:229–233 Chiliveri SC, Aute R, Rai U, Deshmukh MV (2017) DRB4 dsRBD1 drives dsRNA recognition in Arabidopsis thaliana tasi/siRNA pathway. Nucleic Acids Res 45(14):8551–8563 Curtin SJ, Watson JM, Smith NA, Eamens AL, Blanchard CL, Waterhouse PM (2008) The roles of plant dsRNA-binding proteins in RNAi-like pathways. FEBS Lett 582(18):2753–2760 Fire A, Xu S, Montgomery MK, Kostas SA, Driver SE, Mello CC (1998) Potent and specific genetic interference by double-stranded RNA in Caenorhabditis elegans. Nature 391(6669):806–811 Keller R (2004) The computer aided resonance assignment tutorial. CANTINA Verlag, Reiskirchen Lee HY, Zhou K, Smith AM, Noland CL, Doudna JA (2013) Differential roles of human dicer-binding proteins TRBP and PACT in small RNA processing. Nucleic Acids Res 41(13):6568–6576 Lee W, Tonelli M, Markley JL (2015) NMRFAM-SPARKY: enhanced software for biomolecular NMR spectroscopy. Bioinformatics 31:1325–1327 Liu Q, Rand TA, Kalidas S, Du F, Kim HE, Smith DP, Wang X (2003) R2D2, a bridge between the initiation and effector steps of the Drosophila RNAi pathway. Science 301(5641):1921–1925 Montelione GT, Lyons BA, Emerson SD, Tashiro M (1992) An efficient triple resonance experiment using carbon-13 isotropic mixing for determining sequence-specific resonance assignments of isotopically-enriched proteins. J Am Chem Soc 114(27):10974–10975 Muhandiram DR, Kay LE (1994) Gradient-enhanced triple-resonance three-dimensional NMR experiments with improved sensitivity. J Magn Res 103(3):203–216 Muhandiram DR, Farrow NA, Xu GY, Smallcombe SH, Kay LE (1993) A gradient 13 C NOESY-HSQC experiment for recording NOESY spectra of 13 C-labeled proteins dissolved in H2O. J Magn Res 102(3):317–321 Soares ZG, Gonçalves ANA, de Oliveira KPV, Marques JT (2014) Viral RNA recognition by the Drosophila small interfering RNA pathway. Microbes and Infect 16(12):1013–1021 Tabara H, Yigit E, Siomi H, Mello CC (2002) The dsRNA binding protein RDE-4 interacts with RDE-1, DCR-1, and a DExH-box helicase to direct RNAi in C. elegans. Cell 109(7):861–871 Tants JN, Fesser S, Kern T, Stehle R, Geerlof A, Wunderlich C, Sattler M (2017) Molecular basis for asymmetry sensing of siRNAs by the Drosophila Loqs-PD/Dcr-2 complex in RNA interference. Nucleic Acids Res 45(21):12536–12550 Tomari Y, Matranga C, Haley B, Martinez N, Zamore PD (2004) A protein sensor for siRNA asymmetry. Science 306(5700):1377–1380 Wilson RC, Doudna JA (2013) Molecular mechanisms of RNA interference. Annu Rev Biophys 42:217–239 Wishart DS, Sykes BD (1994) The 13C chemical-shift index: a simple method for the identification of protein secondary structure using 13C chemical-shift data. J Biomol NMR 4:171–180 Wishart DS, Bigam CG, Yao J, Abildgaard F, Dyson HJ, Oldfield E, Sykes BD (1995) 1H, 13 C and 15 N chemical shift referencing in biomolecular NMR. J Biomol NMR 6:135–140 Yamaguchi S, Naganuma M, Nishizawa T, Kusakizako T, Tomari Y, Nishimasu H, Nureki O (2022) Structure of the Dicer-2:R2D2 heterodimer bound to a small RNA duplex. Nature 607(7918):393–398 Zambon RA, Vakharia VN, Wu LP (2006) RNAi is an antiviral immune response against a dsRNA virus in Drosophila melanogaster. Cell Microbiol 8(5):880–889