Characterization of a modified silicon-containing arylacetylene resin with POSS functionality

Chinese Journal of Polymer Science - Tập 29 - Trang 726-731 - 2011
Zhen-yu Jiang1, Yan Zhou1, Fa-rong Huang1, Lei Du1
1Key Laboratory of Specially Functional Polymeric Materials of Ministry of Education, School of Material Science and Engineering, East China University of Science and Techology, Shanghai, China

Tóm tắt

A modified silicon-containing arylacetylene resin with a well-defined organic-inorganic POSS functionality was successfully synthesized by Huisgen azide-alkyne 1,3-dipolar cycloaddition. The POSS hybridized resin exhibits excellent thermal properties which were characterized by differential scanning calorimetry (DSC) and thermogravimetric analyses (TGA). Scanning electron microscope (SEM) was used to characterize fracture surface of the hybridized polymer. The results show that phase separation occurs. The POSS moieties are aggregated each other in the polymer to form 200–400 nm domains.

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