Backscattered electron imaging of cementitious microstructures: understanding and quantification

Cement and Concrete Composites - Tập 26 Số 8 - Trang 935-945 - 2004
Karen Scrivener1
1Laboratory of Construction Materials, IMX, Ecole Polytechnique Fédérale de Lausanne, 1015 Lausanne, Switzerland

Tóm tắt

Từ khóa


Tài liệu tham khảo

Scrivener KL, Pratt PL. Characterisation of Portland cement hydration by electron optical techniques. In: Electron microscopy of materials. Proc Mat Res Soc Symp 1983, vol. 31. p. 351–6

Scrivener KL, Pratt PL. Backscattered electron images of polished cement sections in the scanning electron microscope. In: Proc Sixth Int Conf Cement Microscopy, Albuquerque, 1984. p. 145–55

Tennis, 2000, A model for two types of calcium silicate hydrate in the microstructure of Portland cement pastes, Cem. Concr. Res, 30, 855, 10.1016/S0008-8846(00)00257-X

Taylor, 1997

Diamond S, Bonen D. A re-evaluation of hardened cement paste microstructure based on backscatter SEM investigations. In: Diamond S, Mindess S, Glasser FP, Roberts LW, Skalny JP, Wakeley LD, editors. Microstructure of cement based systems/bonding and interfaces in cementitious materials. Materials Research Society Symposium Proceedings, 1995, vol. 370. p. 13–22

Scrivener KL, Lewis MC. Microstructural and microanalytical study of heat cured mortars and delayed ettringite formation. Paper 4iv062, Proc 10th ICCC, Göteborg, 1997

Famy C, Scrivener KL, Brough AR, Atkinson A, Lachowski E. Characterisation of C–S–H products in expansive and non-expansive heat-cured mortars: an electron microscopy study. Proceeding of the 5th CANMET/ACI International Conference of Concrete Durability, Barcelona, Spain, 20001, vol. 1. p. 385–402

Scrivener, 1992, The effect of heat treatment on inner product C–S–H, Cem. Concr. Res, 22, 1224, 10.1016/0008-8846(92)90051-V

Diamond, 1998, The occurrence of two-tone structures in room temperature cured cement pastes, Cem. Concr. Res, 28, 1237, 10.1016/S0008-8846(98)00099-4

Famy, 2002, What causes differences of C–S–H gel grey levels in backscattered electron images?, Cem. Concr. Res, 32, 1465, 10.1016/S0008-8846(02)00808-6

Scrivener KL, Patel HH, Pratt PL, Parrott LJ. Analysis of phases in cement paste using backscattered electron images, methanol adsorption and thermogravimetric analysis. In: Microstructural Development During the Hydration of Cement. Proc Mat Res Soc Symp 1987, vol. 85. p. 67–76

Mouret, 2001, Image analysis: A tool for the characterisation of cement in concrete––metrological aspects of magnification on measurement, Cem. Concr. Comp, 23, 201, 10.1016/S0958-9465(00)00061-5

Patel HH. PhD Thesis. London, University of London, 1987

Diamond, 2000, Mercury porosimetry: an inappropriate method for the measurement of pore size distributions in cement-based materials, Cem. Concr. Res, 30, 1517, 10.1016/S0008-8846(00)00370-7

Scrivener KL, Pratt P. Characterisation of interfacial microstructures. In: Maso JC, editor. Interfacial transition zone in concrete, State of the Art Report, RILEM Committee 108 ICC. London, F.N. Spon, 1996. p. 3–17

Scrivener KL. Characterisation of the ITZ and its quantification by test methods. State of the Art Report, RILEM Committee TC-ETZ, 1999

Crumbie AK. PhD thesis. London, University of London, 1994