Application of rotating disk electrode technique for the preparation of Np, Pu and Am α-sources

Applied Radiation and Isotopes - Tập 52 - Trang 357-364 - 2000
V. Tsoupko-Sitnikov1, F. Dayras1, J. de Sanoit1, D. Filossofov2
1BNM-LPRI, CEA/DAMRI, BP 52, 91193 Gif-sur-Yvette Cedex, France
2LNP-JINR, 141980 Dubna, Russia

Tài liệu tham khảo

Becerril, 1993, An improved rotating disk cathode cell for electrodeposition of actinides. The case of plutonium, Nucl. Instrum. & Methods, A328, 512, 10.1016/0168-9002(93)90668-8 Becerril-Vilchis, 1994, Electrodeposition of americium and physicochemical behaviour of the solution, Radiochim. Acta, 64, 99, 10.1524/ract.1994.64.2.99 Becerril-Vilchis, 1996, A method for preparation of very thin and uniform α-radioactive sources, Nucl. Instrum. & Methods, A369, 613, 10.1016/S0168-9002(96)80062-3 Blurton, 1965, Shapes of practical rotating disk electrodes, J. of Electroanalytical Chemistry, 10, 457, 10.1016/0022-0728(65)80046-8 Da Cruz, 1990, Alpha-source preparation by electrodeposition, Nucl. Instrum. & Methods, A286, 453, 10.1016/0168-9002(90)90896-E Da Cruz, 1998, Mixed alpha sources preparation by electrodeposition, Appl. Radiat. Isot., 49, 1273, 10.1016/S0969-8043(97)10058-6 Ferrero Calabuig, 1998, Semipermeable membrane to retain platinum atoms in the electrodeposition process of alpha spectrometry sources, Appl. Radiat. Isot., 49, 1269, 10.1016/S0969-8043(97)10057-4 Hansen, 1959, The conditions for electrodeposition of insoluble hydroxides at a cathode surface: a theoretical investigation, J. Inorg. Nucl. Chem., 12, 30, 10.1016/0022-1902(59)80089-0 Hansen, 1960, The electrodeposition of insoluble hydroxides: an experimental investigation, J. Inorg. Nucl. Chem., 17, 232, 10.1016/0022-1902(61)80144-9 Koskelo, 1996, An advanced analysis program for alpha-particle spectrometry, Radioact. & Radiochem., 7, 18 Morgan, 1971, Electrodeposition of thorium, uranium and neptunium from ammonium sulphate solution, Radiochim. Acta, 15, 190, 10.1524/ract.1971.15.4.190 Opekar, 1976, Rotating disk electrodes, J. Electroanal. Chem., 69, 1, 10.1016/S0022-0728(76)80129-5 Puphal, 1972, Electrodeposition of alpha-emitting nuclides from a mixed oxalate-chloride electrolyte, Anal. Chem., 44, 284, 10.1021/ac60310a014 Ruellan, 1996, A new spectra processing code applied to the analysis of 235U and 238U in the 60 to 200 keV energy range, Nucl. Instrum. & Methods, A369, 651, 10.1016/S0168-9002(96)80070-2 Sahoo, 1997, Preparation of electrodeposited source of 54Mn, Radiochim. Acta, 76, 185, 10.1524/ract.1997.76.4.185 Talvitie, 1972, Electrodeposition of actinides for alpha spectrometric determination, Anal. Chem., 44, 280, 10.1021/ac60310a013 Truffy, 1991, Mise en point d'une methode d'électrodeposition pour la préparation des sources étalons de rayonnement alpha Vera Tome, 1991, Optimizing the parameters affecting the yield and energy resolution in the electrodeposition of uranium, Appl. Radiat. Isot., 42, 135, 10.1016/0883-2889(91)90062-6 Weber, 1999, On energy resolution of α-sources prepared by electrodeposition of uranium, Nucl. Instrum. & Methods, A423, 468, 10.1016/S0168-9002(98)01310-2