An application of nuclear magnetic resonance imaging to study migration rates of oil-related residues in estuarine sediments

Biodegradation - Tập 9 - Trang 443-449 - 1998
J.A. Chudek1, A.D. Reeves2
1Department of Chemistry, UK
2Department of Geography, University of Dundee, Dundee, Scotland, UK

Tóm tắt

Organisations such as the Marine Control Pollution Unit of the Department of Transport are at present testing the suitability of burial and landfarming of oily residues in sandy coastal environments as an alternative to landfill sites. The tendency for oil related compounds to sorb to sediments has been extensively investigated, but this has not permitted the 'observation' or measurement of advection/diffusion processes or the breakdown of these compounds within sediments. MRI, which is a multidimensional technique allowing the position of nuclei (most commonly protons) to be charted within a volume, provides a means of monitoring advection and diffusion of oil within sediments, thus offering a method of assessing the harming potential of oils in near-shore environments. A three dimensional MRI analysis of the movement of oil in an organic substrate and in three related estuarine sediments show that, using appropriate parameters, movement of the oil can be both observed and quantified. The results presented in terms of the % change of oil distribution within each sediment sample, show the great potential of MRI in studying protonated contaminants in these materials.

Tài liệu tham khảo

Amin MHG, Hall LD, Chorely RJ, Carpenter TA, Richards KS & Bache BW (1994) Magnetic resonance imaging of soil-water phenomena. Mag. Res. Imag. 12(2): 319–321 Amin MHG, Richards KS, Chorely RJ, Gibbs SG, Carpenter TA & Hall LD (1996) Studies of soil-water transport by MRI. Mag. Res. Imag. 14(7–8): 879–882 Borgia GC (1994) The many facets of current work in nuclear magnetic resonance for fluids in heterogeneous systems. Mag. Res. Imag. 12(2): 163–165 Callaghan PT (1991) Principles of Nuclear Magnetic Resonance Microscopy. Clarendon Press, Oxford Davies S, Harwick A, Roberts D, Spowage K & Packer KJ (1994). Quantification of oil and water in preserved reservoir rock by NMR spectroscopy and imaging. Mag. Res. Imag. 12: 394–353 Fordham EJ, Gibbs SJ & Hall LD (1994). Partially restricted diffusion in a permeable Harrison T. (1995). Disposal of oil contaminated beach materials in sandy coastal environments, NERC News 33: 31 Means JC, Wood SG, Hasset JJ & Banwart WL (1980) Sorption of PAHs by sediments and soils. Environ. Sci. Technol. 16: 93–98 McDonald PJ, Pritchard T & Roberts SP (1996) Diffusion of water at low saturation into sandstone rock plugs measured by broad-line magnetic-resonance profiling. J. Colloid Interface Sci. 177(2): 439–445 McDonald PJ (1996) The application of broad-line MRI to the study of porous media. Mag. Res. Imag. 14(7–8): 807–810 Mudge, SM & Bebianno, MJ (1997) Sewage contamination following an accidental spillage in the Ria Formossa, Portugal. Mar. Poll. Bull. 34: 61–84 Williams JLA & Taylor DG (1994) Measurements of viscosity and permeability of 2-phase miscible fluid-flow in rock cores. Mag. Res. Imag. 12(2): 317–318