Alloying behaviour in nanocrystalline materials during mechanical alloying

Bulletin of Materials Science - Tập 22 - Trang 321-327 - 1999
S K Pabi1, I Manna1, B S Murty1
1Department of Metallurgical and Materials Engineering, Indian Institute of Technology, Kharagpur, India

Tóm tắt

The alloying behaviour in a number of systems such as Cu-Ni, Cu-Zn, Cu-Al, Ni-Al, Nb-Al has been studied to understand the mechanism as well as the kinetics of alloying during mechanical alloying (MA). The results show that nanocrystallization is a prerequisite for alloying in all the systems during MA. The mechanism of alloying appears to be a strong function of the enthalpy of formation of the phase and the energy of ordering in case of intermetallic compounds. Solid solutions (Cu-Ni), intermetallic compounds with low ordering energies (such as Ni3Al which forms in a disordered state during MA) and compounds with low enthalpy of formation (Cu-Zn, Al3Nb) form by continuous diffusive mixing. Compounds with high enthalpy of formation and high ordering energies form by a new mechanism christened as discontinuous additive mixing. When the intermetallic gets disordered, its formation mechanism changes from discontinuous additive mixing to continuous diffusive one. A rigorous mathematical model, based on iso-concentration contour migration method, has been developed to predict the kinetics of diffusive intermixing in binary systems during MA. Based on the results of Cu-Ni, Cu-Zn and Cu-Al systems, an effective temperature (T eff) has been proposed that can simulate the observed alloying kinetics. TheT eff for the systems studied is found to lie between 0·42–0·52T 1.

Tài liệu tham khảo

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