A review of nonlinear oscillatory shear tests: Analysis and application of large amplitude oscillatory shear (LAOS)

Progress in Polymer Science - Tập 36 - Trang 1697-1753 - 2011
Kyu Hyun1, Manfred Wilhelm2, Christopher O. Klein2, Kwang Soo Cho3, Jung Gun Nam4, Kyung Hyun Ahn4, Seung Jong Lee4, Randy H. Ewoldt5, Gareth H. McKinley6
1School of Chemical and Biomolecular Engineering, Pusan National University, Jangjeon-Dong 30, Busan 609-735, Republic of Korea
2Institute for Chemical Technology and Polymer Chemistry, Karlsruhe Institute of Technology (KIT), Engesserstraße 18, 76128 Karlsruhe, Germany
3Department of Polymer Science and Engineering, Kyungpook National University, Sangyeok-Dong 1370, Daegu 702-701, Republic of Korea
4School of Chemical and Biological Engineering, Seoul National University, Seoul 151-744, Republic of Korea
5Institute for Mathematics and its Applications & Department of Chemical Engineering and Materials Science, University of Minnesota, Minneapolis, MN 55455, USA
6Department of Mechanical Engineering, Massachusetts Institute of Technology (MIT), Cambridge, MA, 02139, USA

Tài liệu tham khảo

Ferry, 1980 Bird, 1987, vol. 1 Tschoegl, 1989 Dealy, 1990 Klein, 2007, Separation of the nonlinear oscillatory response into a superposition of linear, strain hardening, strain softening, and wall slip response, Macromolecules, 40, 4250, 10.1021/ma062441u Hyun, 2006, Large amplitude oscillatory shear behavior of PEO–PPO–PEO triblock copolymer solutions, Rheol Acta, 45, 239, 10.1007/s00397-005-0014-x Yosick, 1997, A kinetic network model for nonlinear flow behavior of molten plastics in both shear and extension, J Non-Newtonian Fluid Mech, 70, 103, 10.1016/S0377-0257(96)01535-2 Giacomin, 1993, Large-amplitude oscillatory shear, 99 Payne, 1962, The dynamic properties of carbon black-loaded natural rubber vulcanizates. Part I, J Appl Polym Sci, 6, 57, 10.1002/app.1962.070061906 Fletcher, 1953, Non-linearity in the dynamic properties of vulcanized rubber compounds, Trans Inst Rubber Ind, 29, 266 Harris, 1965, Response of time-dependent materials to oscillatory motion, Nature, 207, 744, 10.1038/207744a0 Philippoff, 1966, Vibrational measurements with large amplitudes, Trans Soc Rheol, 10, 317, 10.1122/1.549049 MacDonald, 1969, Rheological behavior for large amplitude oscillatory shear motion, Chem Eng Sci, 24, 1615, 10.1016/0009-2509(69)80101-6 Onogi, 1970, Nonlinear behavior of viscoelastic materials. I. Disperse systems of polystyrene solution and carbon black, Trans Soc Rheol, 14, 275, 10.1122/1.549190 Dodge, 1971, Oscillatory shear of nonlinear fluids. I. Preliminary investigation, Trans Soc Rheol, 15, 589, 10.1122/1.549236 Matsumoto, 1973, Nonlinear behavior of viscoelastic materials. II. The method of analysis and temperature dependence of nonlinear viscoelastic functions, Trans Soc Rheol, 17, 47, 10.1122/1.549319 Komatsu, 1973, Nonlinear viscoelastic properties of semisolid emulsions, Trans Soc Rheol, 17, 351, 10.1122/1.549285 Tee, 1975, Nonlinear viscoelasticity of polymer melts, J Rheol, 19, 595 Walters, 1970, Further studies on the usefulness of the Weissenberg rheogoniometer, 337 Pearson, 1982, Behavior of concentrated polystyrene solutions in large-amplitude oscillating shear fields, J Polym Sci Polym Phys Ed, 20, 83, 10.1002/pol.1982.180200107 Helfand, 1982, Calculation of the nonlinear stress of polymers in oscillatory shear fields, J Polym Sci Polym Phys Ed, 20, 1249, 10.1002/pol.1982.180200711 Hatzikiriakos, 1991, Wall slip of molten high density polyethylene. I. Sliding plate rheometer studies, J Rheol, 35, 497, 10.1122/1.550178 Adrian, 1992, The quasi-periodic nature of a polyurethane melt in oscillatory shear, J Rheol, 36, 1227, 10.1122/1.550309 Giacomin, 1993, Validity of separable BKZ model for large amplitude oscillatory shear, J Rheol, 37, 811, 10.1122/1.550396 Adrian, 1994, The transition to quasi-periodicity for molten plastics in large amplitude oscillatory shear, J Eng Mater Technol, 116, 446, 10.1115/1.2904311 Giacomin, 1992, Structural network models for molten plastics evaluated in large-amplitude oscillatory shear, J Rheol, 36, 1529, 10.1122/1.550272 Jeyaseelan, 1993, Best fit for differential constitutive model parameters to nonlinear oscillation data, J Non-Newtonian Fluid Mech, 47, 267, 10.1016/0377-0257(93)80054-F Dealy, 1998, Frequency response of a shear stress transducer installed in a sliding plate rheometer, J Rheol, 42, 833, 10.1122/1.550903 Boukany, 2007, A correlation between velocity profile and molecular weight distribution in sheared entangled polymer solutions, J Rheol, 51, 217, 10.1122/1.2424947 Wilhelm, 1998, Fourier-transform rheology, Rheol Acta, 37, 399, 10.1007/s003970050126 Wilhelm, 1999, High sensitivity Fourier-transform rheology, Rheol Acta, 38, 349, 10.1007/s003970050185 Wilhelm, 2000, The crossover between linear and nonlinear mechanical behaviour in polymer solutions as detected by Fourier-transform rheology, Rheol Acta, 39, 241, 10.1007/s003970000084 Wilhelm, 2002, Fourier-transform rheology, Macromol Mater Eng, 287, 83, 10.1002/1439-2054(20020201)287:2<83::AID-MAME83>3.0.CO;2-B Dusschoten, 2001, Increased torque transducer sensitivity via oversampling, Rheol Acta, 40, 395, 10.1007/s003970000158 Neidhöfer, 2001, Fourier-transform rheology on linear polystyrene melts, Appl Rheol, 11, 126, 10.1515/arh-2001-0007 Fleury, 2004, Non linear rheology for long chain branching characterization, comparison of two methodologies: Fourier transform rheology and relaxation, Rheol Acta, 44, 174, 10.1007/s00397-004-0394-3 Schlatter, 2005, Fourier transform rheology of branched polyethylene: experiments and models for assessing the macromolecular architecture, Macromolecules, 38, 6492, 10.1021/ma0505530 Sugimoto, 2006, Melt rheology of long-chain-branched polypropylenes, Rheol Acta, 46, 33, 10.1007/s00397-005-0065-z Vittorias, 2007, Detection and quantification of industrial polyethylene branching topologies via Fourier-transform rheology. NMR and simulation using the pom-pom model, Rheol Acta, 46, 321, 10.1007/s00397-006-0111-5 Vittorias, 2007, Application of FT-Rheology towards industrial linear and branched polyethylene blends, Macromol Mater Eng, 292, 935, 10.1002/mame.200700120 Hyun, 2006, Degree of branching of polypropylene measured from Fourier-transform rheology, Rheol Acta, 46, 123, 10.1007/s00397-006-0098-y Hyun, 2007, Fourier-transform rheology under medium amplitude oscillatory shear for linear and branched polymer melts, J Rheol, 51, 1319, 10.1122/1.2790072 Hyun, 2009, Establishing a new mechanical nonlinear coefficient Q from FT-Rheology: first investigation on entangled linear and comb polymer model systems, Macromolecules, 42, 411, 10.1021/ma8017266 Neidhöfer, 2003, Fourier-transform rheology experiments and finite-element simulations on linear polystyrene solutions, J Rheol, 47, 1351, 10.1122/1.1608954 Neidhöfer, 2004, Distinguishing linear from star-branched polystyrene solutions with Fourier-transform rheology, Macromol Rapid Commun, 25, 1921, 10.1002/marc.200400295 Carotenuto, 2008, Fourier transform rheology of dilute immiscible polymer blends: a novel procedure to probe blend morphology, Macromolecules, 41, 4492, 10.1021/ma800540n Filipe, 2004, Evolution of morphological properties along the extruder length for blends of a commercial liquid crystalline polymer and polypropylene, Polymer, 45, 2367, 10.1016/j.polymer.2003.12.080 Filipe, 2006, Evolution of the morphological properties along the extruder length for compatibilized blends of a commercial liquid crystalline polymer and polypropylene, J Appl Polym Sci, 99, 347, 10.1002/app.22393 Daniel, 2001, Nonlinear rheology of a face-centered cubic phase in a diblock copolymer gel, Rheol Acta, 40, 39, 10.1007/s003970000124 Oelschlaeger, 2007, Kinetics of shear microphase orientation and reorientation in lamellar diblock and triblock copolymer melts as detected via FT-Rheology and 2D-SAXS, Macromol Chem Phys, 208, 1719, 10.1002/macp.200700150 Kallus, 2001, Characterization of polymer dispersions by Fourier transform rheology, Rheol Acta, 40, 552, 10.1007/s003970100184 Leblanc, 2003, Fourier transform rheometry on gum elastomers, J Appl Polym Sci, 89, 1101, 10.1002/app.12284 Leblanc, 2003, Updating a torsional dynamic rheometer for Fourier transform rheometry on rubber materials, Rubber Chem Technol, 76, 287, 10.5254/1.3547743 Leblanc, 2003, Characterizing gum elastomers by Fourier transform rheometry, Rubber Chem Technol, 76, 979, 10.5254/1.3547786 Leblanc, 2006, Poly(vinyl chloride)-green coconut fiber composite and their nonlinear viscoelastic behavior as examined with Fourier transform rheometry, J Appl Polym Sci, 101, 3638, 10.1002/app.22726 Leblanc, 2006, Fourier transform rheometry on carbon black filled polybutadiene compounds, J Appl Polym Sci, 100, 5102, 10.1002/app.21941 Leblanc, 2005, Investigating the nonlinear viscoelastic behavior of rubber materials through Fourier transform rheometry, J Appl Polym Sci, 95, 90, 10.1002/app.20798 Leblanc, 2005, Investigating the non-linear viscoelastic behavior of filled rubber compounds through Fourier transform rheometry, Rubber Chem Technol, 78, 54, 10.5254/1.3547873 Leblanc, 2008, Large amplitude oscillatory shear experiments to investigate the nonlinear viscoelastic properties of highly loaded carbon black rubber compounds without curatives, J Appl Polym Sci, 109, 1271, 10.1002/app.28196 Leblanc, 2007, Non-linear viscoelastic characterization of natural rubber gum through large amplitude harmonic experiments, J Rubber Res, 10, 63 Leblanc, 2007, Non-linear viscoelastic characterization of molten thermoplastic vulcanizates (TPV) through large amplitude harmonic experiments, Rheol Acta, 46, 1013, 10.1007/s00397-007-0185-8 Debbaut, 2002, Large amplitude oscillatory shear and Fourier-transform rheology for a high-density polyethylene: experiments and numerical simulation, J Rheol, 46, 1155, 10.1122/1.1495493 Hyun, 2002, Large amplitude oscillatory shear as a way to classify the complex fluids, J Non-Newtonian Fluid Mech, 107, 51, 10.1016/S0377-0257(02)00141-6 Kim, 2002, Large amplitude oscillatory shear behavior of the network model for associating polymeric systems, Korea-Aust Rheol J, 14, 49 Sim, 2003, Large amplitude oscillatory shear behavior of complex fluids investigated by a network model: a guideline for classification, J Non-Newtonian Fluid Mech, 112, 237, 10.1016/S0377-0257(03)00102-2 Cho, 2005, A geometrical interpretation of large amplitude oscillatory shear response, J Rheol, 49, 747, 10.1122/1.1895801 Klein, 2008, Rheological discrimination and characterization of carrageenans and starches by Fourier transform-rheology in the non-linear viscous regime, J Non-Newtonian Fluid Mech, 151, 145, 10.1016/j.jnnfm.2008.01.001 Ewoldt, 2008, An ontology for large amplitude oscillatory shear flow, 1135 Ewoldt, 2008, New measures for characterizing nonlinear viscoelasticity in large amplitude oscillatory shear, J Rheol, 52, 1427, 10.1122/1.2970095 Skoog, 1992 Williams, 1984, Organic polymeric and non–polymeric materials with large optical nonlinearities, Angew Chem Int Ed Engl, 23, 690, 10.1002/anie.198406901 Nam, 2008, Prediction of normal stresses under large amplitude oscillatory shear flow, J Non-Newtonian Fluid Mech, 150, 1, 10.1016/j.jnnfm.2007.10.002 Reimers, 1996, Sliding plate rheometer studies of concentrated polystyrene solutions: large amplitude oscillatory shear of a very high molecular weight polymer in diethyl phthalate, J Rheol, 40, 167, 10.1122/1.550738 Graham, 1995, Wall slip and the nonlinear dynamics of large amplitude oscillatory shear flows, J Rheol, 39, 697, 10.1122/1.550652 Larson, 1992, Instabilities in viscoelastic flows, Rheol Acta, 31, 213, 10.1007/BF00366504 Groisman, 2000, Elastic turbulence in a polymer solution flow, Nature, 45, 53, 10.1038/35011019 Atalık, 2004, On the occurrence of even harmonics in the shear stress response of viscoelastic fluids in large amplitude oscillatory shear, J Non-Newtonian Fluid Mech, 122, 107, 10.1016/j.jnnfm.2003.11.012 Tapadia, 2006, Banding in entangled polymer fluids under oscillatory shearing, Phys Rev Lett, 96, 10.1103/PhysRevLett.96.196001 Heymann, 2002, Investigation of the solid–liquid transition of highly concentrated suspensions in oscillatory amplitude sweeps, J Rheol, 46, 93, 10.1122/1.1423314 Wyss, 2007, Strain-rate frequency superposition: a rheological probe of structural relaxation in soft materials, Phys Rev Lett, 98, 10.1103/PhysRevLett.98.238303 Ahn, 1994, A network model predicting the shear-thickening behavior of a poly(vinyl alcohol)/sodium borate aqueous solution, J Non-Newtonian Fluid Mech, 55, 215, 10.1016/0377-0257(94)80071-5 Harrison, 1999, Suspensions and polymers – common links in rheology, Korea-Aust Rheol J, 11, 197, 10.1122/1.550982 Höfl, 2006, Effect of large amplitude oscillatory shear (LAOS) on the dielectric response of 1,4-cis-polyisoprene, Polymer, 47, 7282, 10.1016/j.polymer.2006.03.116 Inoue, 1993, Rheological properties of poly(vinyl alcohol)/sodium borate aqueous solutions, Rheol Acta, 32, 550, 10.1007/BF00369071 Storm, 2005, Nonlinear elasticity in biological gels, Nature, 435, 191, 10.1038/nature03521 Mason, 1995, Elasticity of compressed emulsions, Phys Rev Lett, 75, 2051, 10.1103/PhysRevLett.75.2051 Bower, 1999, The rheological and microstructural characterization of the non-linear flow behavior of concentrated oil-in-water emulsions, Rheol Acta, 38, 145, 10.1007/s003970050164 Mason, 1995, Linear viscoelasticity of colloidal hard sphere suspensions near the glass transition, Phys Rev Lett, 75, 2770, 10.1103/PhysRevLett.75.2770 Bossard, 2007, Linear and nonlinear viscoelastic behavior of very concentrated plate-like kaolin suspensions, J Rheol, 51, 1253, 10.1122/1.2790023 Cloitre, 2000, Rheological aging and rejuvenation in microgel pastes, Phys Rev Lett, 85, 4819, 10.1103/PhysRevLett.85.4819 Sim, 2003, Three-dimensional dynamics simulation of electrorheological fluids under large amplitudes oscillatory shear flow, J Rheol, 47, 879, 10.1122/1.1582854 Tirtaatmadja, 1997, Superposition of oscillations on steady shear flow as a technique for investigating the structure of associative polymers, Macromolecules, 30, 1426, 10.1021/ma960098v Tirtaatmadja, 1997, Rheological properties of model alkali-soluble associative (HASE) polymers: effect of varying hydrophobe chain length, Macromolecules, 30, 3271, 10.1021/ma961202b Tam, 1999, Viscoelastic properties of hydrophobically modified alkali-soluble emulsion in salt solutions, Polymer, 40, 6369, 10.1016/S0032-3861(98)00857-X Hyun, 2003, Nonlinear response of complex fluids under LAOS (large amplitude oscillatory shear) flow, Korea-Aust Rheol J, 15, 97 Raghavan, 1995, Shear induced microstructural changes in flocculated suspensions of fumed silica, J Rheol, 39, 1311, 10.1122/1.550638 Parthasarathy, 1999, Large amplitude oscillatory shear of ER suspensions, J Non-Newtonian Fluid Mech, 81, 83, 10.1016/S0377-0257(98)00096-2 Miller, 1991, Rheology of solid propellant dispersions, J Rheol, 35, 901, 10.1122/1.550162 Ma, 1999, Keratin filament suspensions show unique micromechanical properties, J Biol Chem, 274, 19145, 10.1074/jbc.274.27.19145 Citerne, 2001, Rheological properties of peanut butter, Rheol Acta, 40, 86, 10.1007/s003970000120 Carreau, 1999, Rheological properties of concentrated suspensions, vol. 8, 1299 Rochefort, 1987, Rheology of Xanthan gum: salt, temperature, and strain effects in oscillatory and steady shear experiments, J Rheol, 31, 337, 10.1122/1.549953 Neidhöfer, 2002, FT-rheology and finite-element simulations on polystyrene solutions and melts of various topologies, 463 Chopra, 2000, Nonlinear rheological response of phase separating polymer blends: poly(styrene-co-maleic anhydride)/poly(methyl methacrylate), J Rheol, 44, 27, 10.1122/1.551079 Lim, 1984, Rheology of self-associating concentrated Xanthan solutions, J Rheol, 28, 367, 10.1122/1.549757 Hamley, 1998, Shear-induced orientation of the body-centered-cubic phase in diblock copolymer gel, Phys Rev E, 58, 7620, 10.1103/PhysRevE.58.7620 Okamoto, 1994, Dynamics SAXS studies of sphere-forming block copolymers under large oscillatory shear deformation, Macromolecules, 27, 3753, 10.1021/ma00092a012 Gadala-Maria, 1980, Shear-induced structure in a concentrated suspension of solid spheres, J Rheol, 24, 799, 10.1122/1.549584 Powell, 1995, Application of a nonlinear phenomenological model to the oscillatory behavior of ER materials, J Rheol, 39, 1075, 10.1122/1.550618 Li, 2003, Nonlinear viscoelastic properties of MR fluids under large-amplitude-oscillatory shear, Rheol Acta, 42, 280, 10.1007/s00397-002-0285-4 Ewoldt, 2007, Rheological fingerprinting of gastropod pedal mucus and synthetic complex fluids for biomimicking adhesive locomotion, Soft Matter, 3, 634, 10.1039/b615546d Tariq, 1998, Nonlinear viscoelasticity of cheese, Biorheology, 35, 171, 10.1016/S0006-355X(99)80006-7 Lodge, 1964 Coleman, 1970, A phenomenological theory of streaming birefringence, Arch Rational Mech Anal, 39, 358, 10.1007/BF00251297 Coleman, 1974, Asymptotic relations between shear stresses and normal stresses in general incompressible fluids, J Polym Sci Polym Phys Ed, 12, 2195, 10.1002/pol.1974.180121103 Vrentas, 1991, Finite amplitude oscillations of viscoelastic fluids, J Non-Newtonian Fluid Mech, 40, 1, 10.1016/0377-0257(91)87023-Q Oakley, 1994, A sliding plate normal thrust rheometer for molten plastics, Polym Eng Sci, 34, 580, 10.1002/pen.760340706 Janmey, 2007, Negative normal stress in semiflexible biopolymer gels, Nature Mater, 6, 48, 10.1038/nmat1810 Labiausse, 2007, Shear induced normal stress difference in aqueous foams, J Rheol, 51, 479, 10.1122/1.2715392 Jeyaseelan, 2008, Network theory for polymer solutions in large amplitude oscillatory shear, J Non-Newtonian Fluid Mech, 148, 24, 10.1016/j.jnnfm.2007.04.012 Férec, 2008, Rheological behavior of fiber-filled polymers under large amplitude oscillatory shear flow, J Non-Newtonian Fluid Mech, 151, 89, 10.1016/j.jnnfm.2008.01.002 James, 2009, Boger fluids, Annu Rev Fluid Mech, 41, 129, 10.1146/annurev.fluid.010908.165125 Larson, 1988 Nam, 2008, Analysis of the normal stress differences of viscoelastic fluids under large amplitude oscillatory shear flow, 171 Nam, 2010, First normal stress difference of entangled polymer solutions in large amplitude oscillatory shear flow, J Rheol, 54, 1243, 10.1122/1.3483611 Hilliou, 2004, Increasing the torque sensitivity of an RPA 2000 by a factor 5-10 using advanced data acquisition, Rubber Chem Technol, 77, 192, 10.5254/1.3547811 Liu, 2009, Control on the topological structure of polyolefin elastomer by reactive processing, Polymer, 50, 547, 10.1016/j.polymer.2008.11.030 Kossuth, 1999, Viscoelastic behavior of cubic phases in block copolymer melts, J Rheol, 43, 167, 10.1122/1.550981 Kim, 2003, Electrically activated poly(propylene)/clay nanocomposites, Macromol Rapid Commun, 24, 388, 10.1002/marc.200390055 Yu, 2009, General stress decomposition in nonlinear oscillatory shear flow, J Rheol, 53, 215, 10.1122/1.3037267 Larson, 1999 Macosko, 1994 Hatzikiriakos, 1992, Role of slip and fracture in the oscillating flow of HDPE in a capillary, J Rheol, 36, 845, 10.1122/1.550320 Yoshimura, 1988, Wall slip effects on dynamic oscillatory measurements, J Rheol, 32, 575, 10.1122/1.549982 Yosick, 1998, Fluid inertia in large amplitude oscillatory shear, Rheol Acta, 37, 365, 10.1007/s003970050123 Mas, 1997, Experimental validation of steady shear and dynamic viscosity relation for yield stress fluids, Rheol Acta, 36, 49, 10.1007/BF00366723 Sagis, 2001, Constitutive equations for an elastic material with anisotropic rigid particles, Phys Rev E, 63, 10.1103/PhysRevE.63.051504 Ewoldt, 2007, Rheological fingerprinting of complex fluids using large amplitude oscillatory shear (LAOS) flows, Ann Trans Nordic Soc Rheol, 15, 3 Kim, 2006, Comparison of interpretation methods for large amplitude oscillatory shear response, Korea-Aust Rheol J, 18, 91 Calin, 2008, A new approach to determine the nonlinear parameter of the Giesekus constitutive model, 1372 Ewoldt, 2010, On secondary loops in LAOS via self-intersection of Lissajous-Bowditch curves, Rheol Acta, 49, 213, 10.1007/s00397-009-0408-2 Rogers, 2010, Frieze group analysis of asymmetric response to large-amplitude oscillatory shear, J Rheol, 54, 859, 10.1122/1.3445064 Renou, 2010, Yielding processes in a colloidal glass of soft star-like micelles under large amplitude oscillatory shear (LAOS), J Rheol, 54, 1219, 10.1122/1.3483610 Ganeriwala, 1987, Fourier-transform mechanical analysis for determining the nonlinear viscoelastic properties of polymers, Polym Eng Sci, 27, 165, 10.1002/pen.760270211 Franck, 2008, Non-linear oscillation testing with a separate motor transducer rheometer, 1138 Grosso, 2007, A new methodology for the estimation of drop size distributions of dilute polymer blends based on LAOS flows, J Non-Newtonian Fluid Mech, 143, 48, 10.1016/j.jnnfm.2007.01.005 Yu, 2006, Note on morphology determination in emulsions via rheology, J Non-Newtonian Fluid Mech, 133, 57, 10.1016/j.jnnfm.2005.11.001 Leblanc, 2009, Engineering performance and material viscoelastic analyses along a compounding line for silica-based compounds. Part 2. Nonlinear viscoelastic analysis, J Appl Polym Sci, 112, 1128, 10.1002/app.29515 Langela, 2002, Microphase reorientation in block copolymer melts as detected via FT-Rheology and 2D-SAXS, Macromolecules, 35, 3198, 10.1021/ma0115693 Mortensen, 1993, Structural study on the micelle formation of poly(ethylene oxide)–poly(propylene oxide)–poly(ethylene oxide) triblock copolymer in aqueous solution, Macromolecules, 26, 805, 10.1021/ma00056a035 Denny, 1980, The role of gastropod pedal mucus in locomotion, Nature, 285, 160, 10.1038/285160a0 Ewoldt, 2009, Nonlinear viscoelastic biomaterials: meaningful characterization and engineering inspiration, Integr Comp Biol, 49, 40, 10.1093/icb/icp010 Davis, 1978, Nonlinear dynamic mechanical moduli for polycarbonate and PMMA, J Rheol, 22, 53, 10.1122/1.549500 Papon, 2010, Nonlinear rheology of model filled elastomers, J Polym Sci Part B: Polym Phys, 48, 2490, 10.1002/polb.22151 Ewoldt, 2010, Non-linear viscoelasticity of hagfish slime, Int J Non-linear Mech Ng, 2011, Large amplitude oscillatory shear flow of gluten dough; a model power-law gel, J Rheol, 55, 627, 10.1122/1.3570340 Doi, 1986 Bent, 2003, Neutron-mapping polymer flow: scattering, flow visualization, and molecular theory, Science, 301, 1691, 10.1126/science.1086952 Janeschitz-Krigel, 1983 Fuller, 1995 Safinya, 1991, Nematic to Smectic-A phase transition under shear flow: a nonequilibrium synchrotron X-ray study, Phys Rev Lett, 66, 1986, 10.1103/PhysRevLett.66.1986 Dootz, 2007, Rapid prototyping of X-ray microdiffraction compatible continuous microflow foils, Small, 3, 96, 10.1002/smll.200600288 Chen, 1997, Pathways to macroscale order in nanostructured block copolymers, Science, 277, 1248, 10.1126/science.277.5330.1248 Wiesner, 1997, Lamellar diblock copolymers under large amplitude oscillatory shear flow: order and dynamics, Macromol Chem Phys, 198, 3319, 10.1002/macp.1997.021981101 Hamley, 2001, Structure and flow behaviour of block copolymers, J Phys Condens Matter, 13, R643, 10.1088/0953-8984/13/33/201 Hamley, 2004, Small-angle scattering of block copolymers in the melt, solution and crystal states, Prog Polym Sci, 29, 909 Watanabe, 2003, Rheo-dielectrics in oligomeric and polymeric fluids: a review of recent findings, J Phys Condens Matter, 15, S909, 10.1088/0953-8984/15/11/315 Capaccioli, 2007, Applications of the rheo-dielectric technique, J Non-Cryst Solids, 353, 4267, 10.1016/j.jnoncrysol.2007.02.069 Watanabe, 1998, Rheo-dielectric behavior of low molecular weight liquid crystals. 1. Behavior of nematic 5CB and 7CB, Rheol Acta, 37, 519, 10.1007/s003970050139 Watanabe, 1999, Rheo-dielectric behavior of low molecular weight liquid crystals. 2. Behavior of 8CB in nematic and smectic states, Rheol Acta, 38, 100, 10.1007/s003970050160 Watanabe, 2001, Dielectric relaxation of type-A polymers in melts and solutions, Macromol Rapid Commun, 22, 127, 10.1002/1521-3927(200102)22:3<127::AID-MARC127>3.0.CO;2-S Watanabe, 2005, Dielectric and viscoelastic study of entanglement dynamics: a review of recent findings, Macromol Symp, 228, 51, 10.1002/masy.200551005 Alig, 2008, Destruction and formation of a carbon nanotube network in polymer melts: rheology and conductivity spectroscopy, Polymer, 49, 3524, 10.1016/j.polymer.2008.05.037 Watanabe, 2001, Rheo-dielectric behavior of carbon black suspensions, Nihon Reoroji Gakkaishi, 29, 77, 10.1678/rheology.29.77 Hyun, 2009, The rheo-dielectric setup to measure dielectric spectra of 1,4-cis-polyisoprene under large amplitude oscillatory shear (LAOS), J Non-Newtonian Fluid Mech, 160, 93, 10.1016/j.jnnfm.2009.03.002 Watanabe, 2002, Rheodielectric behavior of entangled cis-polyisoprene under fast shear, Macromolecules, 35, 8802, 10.1021/ma020562y Stockmayer, 1969, Dielectric dispersion in branched polypropylene oxide, Macromolecules, 2, 647, 10.1021/ma60012a017 Adachi, 1993, Dielectric normal mode relaxation, Prog Polym Sci, 18, 585, 10.1016/0079-6700(93)90018-8 Pople, 1998, Orientational ordering of a poly(oxyethylene)–poly(oxybutylene) diblock copolymer gel under steady shear flow, Macromolecules, 31, 2952, 10.1021/ma9716490 Panine, 2003, Combined rheometry and small-angle X-ray scattering, Rev Sci Instrum, 74, 2451, 10.1063/1.1556943 Rathgeber, 2007, Rheooscillations of a bottlebrush polymer solution due to shear-induced phase transitions between a shear molten state and a line hexatic phase, Macromolecules, 40, 7680, 10.1021/ma070479g Polushkin, 2003, In situ radial small angle synchrotron X-ray scattering study of shear-induced macroscopic orientation of hierarchically structured comb-shaped supramolecules, Macromolecules, 36, 1421, 10.1021/ma0257548 Polushkin, 2004, A modified rheometer for in-situ radial and tangential SAXS studies on shear-induced alignment, Rheol Acta, 43, 364, 10.1007/s00397-003-0352-5 Caputo, 2002, Time-resolved small-angle X-ray scattering measurements of a polymer bicontinuous microemulsion structure factor under shear, Phys Rev E, 66, 10.1103/PhysRevE.66.041401 Dingenouts, 2010, New developments for the mechanical characterization of materials, Korea-Aust Rheol J, 22, 317 Struth, 2011, Observation of New States of Liquid Crystal 8CB under Nonlinear Shear Conditions as Observed via a Novel and Unique Rheology/Small-Angle X-ray Scattering Combination, Langmuir, 27, 2880, 10.1021/la103786w Garcia-Gutierrez, 2008, Influence of shear on the templated crystallization of poly(butylene terephthalate)/single wall carbon nanotube nanocomposites, Macromolecules, 41, 844, 10.1021/ma0713512 Calin, 2010, Determination of the non-linear parameter (mobility factor) of the Giesekus constitutive model using LAOS procedure, J Non-Newtonian Fluid Mech, 165, 1564, 10.1016/j.jnnfm.2010.08.008 Brader, 2010, Nonlinear response of dense colloidal suspensions under oscillatory shear: mode-coupling theory and Fourier transform rheology experiments, Phys Rev E, 82, 10.1103/PhysRevE.82.061401 Läuger, 2010, Differences between stress and strain control in the non-linear behavior of complex fluids, Rheol Acta, 49, 909, 10.1007/s00397-010-0450-0 Bejenariu, 2010, Large amplitude oscillatory extension of soft polymeric networks, Rheol Acta, 807, 10.1007/s00397-010-0464-7 Li, 2010, Nonlinear rheological behavior of diphenylmethylvinyl silicone gum: an example of homogeneous shear, Rheol Acta, 49, 89, 10.1007/s00397-009-0389-1 Zhou, 2010, Probing shear-banding transitions of the VCM model for entangled wormlike micellar solutions using large amplitude oscillatory shear (LAOS) deformations, J Non-Newtonian Fluid Mech, 165, 1462, 10.1016/j.jnnfm.2010.07.009